Filipović, Vladimir M.

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orcid::0000-0002-7081-8217
  • Filipović, Vladimir M. (4)
  • Filipović, Vladimir (3)
Projects

Author's Bibliography

Prediction of the Impact of Land Use and Soil Type on Concentrations of Heavy Metals and Phthalates in Soil Based on Model Simulation

Stojić, Nataša; Pezo, Lato; Lončar, Biljana; Pucarević, Mira; Filipović, Vladimir; Prokić, Dunja; Ćurčić, Ljiljana; Štrbac, Snežana

(MDPI, 2023)

TY  - JOUR
AU  - Stojić, Nataša
AU  - Pezo, Lato
AU  - Lončar, Biljana
AU  - Pucarević, Mira
AU  - Filipović, Vladimir
AU  - Prokić, Dunja
AU  - Ćurčić, Ljiljana
AU  - Štrbac, Snežana
PY  - 2023
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/7193
AB  - The main objective of this study is to determine the possibility of predicting the impact of land use and soil type on concentrations of heavy metals (HMs) and phthalates (PAEs) in soil based on an artificial neural network model (ANN). Qualitative analysis of HMs was performed with inductively coupled plasma-optical emission spectrometry (ICP/OES) and Direct Mercury Analyzer. Determination of PAEs was performed with gas chromatography (GC) coupled with a single quadrupole mass spectrometry (MS). An ANN, based on the Broyden-Fletcher-Goldfarb-Shanno (BFGS) iterative algorithm, for the prediction of HM and PAE concentrations, based on land use and soil type parameters, showed good prediction capabilities (the coefficient of determination (r(2)) values during the training cycle for HM concentration variables were 0.895, 0.927, 0.885, 0.813, 0.883, 0.917, 0.931, and 0.883, respectively, and for PAEs, the concentration variables were 0.950, 0.974, 0.958, 0.974, and 0.943, respectively). The results of this study indicate that HM and PAE concentrations, based on land use and soil type, can be predicted using ANN.
PB  - MDPI
T2  - Toxics
T1  - Prediction of the Impact of Land Use and Soil Type on Concentrations of Heavy Metals and Phthalates in Soil Based on Model Simulation
VL  - 11
IS  - 3
DO  - 10.3390/toxics11030269
UR  - conv_1093
ER  - 
@article{
author = "Stojić, Nataša and Pezo, Lato and Lončar, Biljana and Pucarević, Mira and Filipović, Vladimir and Prokić, Dunja and Ćurčić, Ljiljana and Štrbac, Snežana",
year = "2023",
abstract = "The main objective of this study is to determine the possibility of predicting the impact of land use and soil type on concentrations of heavy metals (HMs) and phthalates (PAEs) in soil based on an artificial neural network model (ANN). Qualitative analysis of HMs was performed with inductively coupled plasma-optical emission spectrometry (ICP/OES) and Direct Mercury Analyzer. Determination of PAEs was performed with gas chromatography (GC) coupled with a single quadrupole mass spectrometry (MS). An ANN, based on the Broyden-Fletcher-Goldfarb-Shanno (BFGS) iterative algorithm, for the prediction of HM and PAE concentrations, based on land use and soil type parameters, showed good prediction capabilities (the coefficient of determination (r(2)) values during the training cycle for HM concentration variables were 0.895, 0.927, 0.885, 0.813, 0.883, 0.917, 0.931, and 0.883, respectively, and for PAEs, the concentration variables were 0.950, 0.974, 0.958, 0.974, and 0.943, respectively). The results of this study indicate that HM and PAE concentrations, based on land use and soil type, can be predicted using ANN.",
publisher = "MDPI",
journal = "Toxics",
title = "Prediction of the Impact of Land Use and Soil Type on Concentrations of Heavy Metals and Phthalates in Soil Based on Model Simulation",
volume = "11",
number = "3",
doi = "10.3390/toxics11030269",
url = "conv_1093"
}
Stojić, N., Pezo, L., Lončar, B., Pucarević, M., Filipović, V., Prokić, D., Ćurčić, L.,& Štrbac, S.. (2023). Prediction of the Impact of Land Use and Soil Type on Concentrations of Heavy Metals and Phthalates in Soil Based on Model Simulation. in Toxics
MDPI., 11(3).
https://doi.org/10.3390/toxics11030269
conv_1093
Stojić N, Pezo L, Lončar B, Pucarević M, Filipović V, Prokić D, Ćurčić L, Štrbac S. Prediction of the Impact of Land Use and Soil Type on Concentrations of Heavy Metals and Phthalates in Soil Based on Model Simulation. in Toxics. 2023;11(3).
doi:10.3390/toxics11030269
conv_1093 .
Stojić, Nataša, Pezo, Lato, Lončar, Biljana, Pucarević, Mira, Filipović, Vladimir, Prokić, Dunja, Ćurčić, Ljiljana, Štrbac, Snežana, "Prediction of the Impact of Land Use and Soil Type on Concentrations of Heavy Metals and Phthalates in Soil Based on Model Simulation" in Toxics, 11, no. 3 (2023),
https://doi.org/10.3390/toxics11030269 .,
conv_1093 .
4
3

In vitro evaluation of antioxidative activities of the extracts of petals of Paeonia lactiflora and Calendula officinalis incorporated in the new forms of biobased carriers

Batinić, Petar; Milošević, Milena; Lukić, Milan; Prijić, Željana; Gordanić, Stefan; Filipović, Vladimir; Marinković, Aleksandar; Bugarski, Branko; Marković, Tatjana

(Novi Sad : Univerzitet u Novom Sadu - Naučni institut za prehrambene tehnologije, 2022)

TY  - JOUR
AU  - Batinić, Petar
AU  - Milošević, Milena
AU  - Lukić, Milan
AU  - Prijić, Željana
AU  - Gordanić, Stefan
AU  - Filipović, Vladimir
AU  - Marinković, Aleksandar
AU  - Bugarski, Branko
AU  - Marković, Tatjana
PY  - 2022
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/5610
AB  - U ovom radu prikazana je ekstrakcija latica hibrida Paeonia lactiflora "Činija lepote" i Calendula officinalis L. pomoću mikrotalasnog reaktora i ultarazvuka u sistemu etanol-voda, kao i izolacija etarskog ulja latica Calendula officinalis L. hidrodestilacijom. Određen je ukupan sadržaj fenola i flavonoida u ekstraktima i ulju, i procenjena je antioksidativna aktivnost. Antioksidativna aktivnost je određena korišćenjem standardnih, antioksidativnih in vitro DPPH • i ABTS •+ testova. Najveći ukupni sadržaj fenola utvrđen je kod ekstrakata P. lactiflora i C. officinalis L. dobijenih ultrazvučnom ekstrakcijom (83,16 i 114,47 mg GA/g, redom), dok je najveći sadržaj flavonoida dobijen ekstrakcijom uz pomoć mikrotalasnog reaktora (123,48 i 65,29 mg QE/g, redom). Najveća antioksidativna aktivnost za ekstrakt hibrida Paeonia lactiflora "Činija lepote" dobijena je mikrotalasnom ekstrakcijom (79% i 83%), dok je za ekstrakt Calendula officinalis L. dobijena ultrazvučnom ekstrakcijom (45% i 49%) u DPPH • i ABTS •+ , redom. U cilju poboljšanja antioksidativne aktivnosti oba tipa ispitivanih analita (ekstrakta i etarskog ulja), pektinski biopolimerni film, (u formi nosača), u procesu enzimski potpomognute katalize, je pripremljen. Za karakterizaciju dobijenih filmova korišćena je optička mikroskopija i FTIR spektroskopija. Filmovi sa esencijalnim uljem C. officinalis L. i galnom kiselinom, pokazali su značajno povećan procenat inhibicije u DPPH • i ABTS •+ testu (91% i 95%, redom) nakon 10 minuta. Rezultati su, takođe, pokazali da se sve formulacije pektinskog biopolimernog filma, modifikovanog galnom kiselinom, mogu uspešno primenjivati kao nosač za oba tipa ingredijenata.
AB  - In this study, the petals collected from peony hybrid Paeonia lactiflora "Bowl of Beauty" and Calendula officinalis L. were extracted using an ethanol-water mixture assisted with microwave and ultrasonic treatment. The isolation of Calendula officinalis L. essential oil was done by hydrodistillation as well. The total phenolic and flavonoids content in the extracts and oil were determined and their antioxidant activity was evaluated. The highest total phenolic content was found for the extracts of hybrid Paeonia lactiflora and Calendula officinalis L. obtained by ultrasound extraction (83.16 and 114.47 mg GA/g, respectively), while the flavonoid content obtained by microwave-assisted extraction was relatively high (123.48 and 65.29 mg QE/g, respectively). The highest antioxidant activity was obtained in DPPH • and ABTS •+ assay for the microwave-assisted extraction of hybrid P. lactiflora (79% and 83%) and ultrasound-assisted extraction of C. officinalis L. (45% and 49%), respectively. To improve antioxidant activity of both types of examined analytes (extracts and essential oil), the pectin biopolymer film (as a carrier) was prepared in the process of enzymatically assisted catalysis. Optical microscopy and FTIR spectroscopy were used for the characterization of obtained materials. The films, with essential oil of C. officinalis L. and gallic acid, showed significantly increased percentage inhibition in DPPH • and ABTS •+ test (91% and 95%, respectively) after 10 minutes. The results, also, showed that all formulations of pectin biopolymer film, modified with gallic acid, can be successfully applied as a carrier for both types of ingredients.
PB  - Novi Sad : Univerzitet u Novom Sadu - Naučni institut za prehrambene tehnologije
T2  - Food and Feed Research
T1  - In vitro evaluation of antioxidative activities of the extracts of petals of Paeonia lactiflora and Calendula officinalis incorporated in the new forms of biobased carriers
T1  - In vitro procena antioksidativne aktivnosti ekstrakta latica Paeonia lactiflora i Calendula officinalis ugrađenih u nove forme nosača na biobazi
DO  - 10.5937/ffr0-36381
ER  - 
@article{
author = "Batinić, Petar and Milošević, Milena and Lukić, Milan and Prijić, Željana and Gordanić, Stefan and Filipović, Vladimir and Marinković, Aleksandar and Bugarski, Branko and Marković, Tatjana",
year = "2022",
abstract = "U ovom radu prikazana je ekstrakcija latica hibrida Paeonia lactiflora "Činija lepote" i Calendula officinalis L. pomoću mikrotalasnog reaktora i ultarazvuka u sistemu etanol-voda, kao i izolacija etarskog ulja latica Calendula officinalis L. hidrodestilacijom. Određen je ukupan sadržaj fenola i flavonoida u ekstraktima i ulju, i procenjena je antioksidativna aktivnost. Antioksidativna aktivnost je određena korišćenjem standardnih, antioksidativnih in vitro DPPH • i ABTS •+ testova. Najveći ukupni sadržaj fenola utvrđen je kod ekstrakata P. lactiflora i C. officinalis L. dobijenih ultrazvučnom ekstrakcijom (83,16 i 114,47 mg GA/g, redom), dok je najveći sadržaj flavonoida dobijen ekstrakcijom uz pomoć mikrotalasnog reaktora (123,48 i 65,29 mg QE/g, redom). Najveća antioksidativna aktivnost za ekstrakt hibrida Paeonia lactiflora "Činija lepote" dobijena je mikrotalasnom ekstrakcijom (79% i 83%), dok je za ekstrakt Calendula officinalis L. dobijena ultrazvučnom ekstrakcijom (45% i 49%) u DPPH • i ABTS •+ , redom. U cilju poboljšanja antioksidativne aktivnosti oba tipa ispitivanih analita (ekstrakta i etarskog ulja), pektinski biopolimerni film, (u formi nosača), u procesu enzimski potpomognute katalize, je pripremljen. Za karakterizaciju dobijenih filmova korišćena je optička mikroskopija i FTIR spektroskopija. Filmovi sa esencijalnim uljem C. officinalis L. i galnom kiselinom, pokazali su značajno povećan procenat inhibicije u DPPH • i ABTS •+ testu (91% i 95%, redom) nakon 10 minuta. Rezultati su, takođe, pokazali da se sve formulacije pektinskog biopolimernog filma, modifikovanog galnom kiselinom, mogu uspešno primenjivati kao nosač za oba tipa ingredijenata., In this study, the petals collected from peony hybrid Paeonia lactiflora "Bowl of Beauty" and Calendula officinalis L. were extracted using an ethanol-water mixture assisted with microwave and ultrasonic treatment. The isolation of Calendula officinalis L. essential oil was done by hydrodistillation as well. The total phenolic and flavonoids content in the extracts and oil were determined and their antioxidant activity was evaluated. The highest total phenolic content was found for the extracts of hybrid Paeonia lactiflora and Calendula officinalis L. obtained by ultrasound extraction (83.16 and 114.47 mg GA/g, respectively), while the flavonoid content obtained by microwave-assisted extraction was relatively high (123.48 and 65.29 mg QE/g, respectively). The highest antioxidant activity was obtained in DPPH • and ABTS •+ assay for the microwave-assisted extraction of hybrid P. lactiflora (79% and 83%) and ultrasound-assisted extraction of C. officinalis L. (45% and 49%), respectively. To improve antioxidant activity of both types of examined analytes (extracts and essential oil), the pectin biopolymer film (as a carrier) was prepared in the process of enzymatically assisted catalysis. Optical microscopy and FTIR spectroscopy were used for the characterization of obtained materials. The films, with essential oil of C. officinalis L. and gallic acid, showed significantly increased percentage inhibition in DPPH • and ABTS •+ test (91% and 95%, respectively) after 10 minutes. The results, also, showed that all formulations of pectin biopolymer film, modified with gallic acid, can be successfully applied as a carrier for both types of ingredients.",
publisher = "Novi Sad : Univerzitet u Novom Sadu - Naučni institut za prehrambene tehnologije",
journal = "Food and Feed Research",
title = "In vitro evaluation of antioxidative activities of the extracts of petals of Paeonia lactiflora and Calendula officinalis incorporated in the new forms of biobased carriers, In vitro procena antioksidativne aktivnosti ekstrakta latica Paeonia lactiflora i Calendula officinalis ugrađenih u nove forme nosača na biobazi",
doi = "10.5937/ffr0-36381"
}
Batinić, P., Milošević, M., Lukić, M., Prijić, Ž., Gordanić, S., Filipović, V., Marinković, A., Bugarski, B.,& Marković, T.. (2022). In vitro evaluation of antioxidative activities of the extracts of petals of Paeonia lactiflora and Calendula officinalis incorporated in the new forms of biobased carriers. in Food and Feed Research
Novi Sad : Univerzitet u Novom Sadu - Naučni institut za prehrambene tehnologije..
https://doi.org/10.5937/ffr0-36381
Batinić P, Milošević M, Lukić M, Prijić Ž, Gordanić S, Filipović V, Marinković A, Bugarski B, Marković T. In vitro evaluation of antioxidative activities of the extracts of petals of Paeonia lactiflora and Calendula officinalis incorporated in the new forms of biobased carriers. in Food and Feed Research. 2022;.
doi:10.5937/ffr0-36381 .
Batinić, Petar, Milošević, Milena, Lukić, Milan, Prijić, Željana, Gordanić, Stefan, Filipović, Vladimir, Marinković, Aleksandar, Bugarski, Branko, Marković, Tatjana, "In vitro evaluation of antioxidative activities of the extracts of petals of Paeonia lactiflora and Calendula officinalis incorporated in the new forms of biobased carriers" in Food and Feed Research (2022),
https://doi.org/10.5937/ffr0-36381 . .
4

Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses

Nićetin, Milica; Pezo, Lato; Pergal, Marija; Lončar, Biljana; Filipović, Vladimir; Knežević, Violeta; Demir, Hande; Filipović, Jelena; Manojlović, Dragan

(MDPI, 2022)

TY  - JOUR
AU  - Nićetin, Milica
AU  - Pezo, Lato
AU  - Pergal, Marija
AU  - Lončar, Biljana
AU  - Filipović, Vladimir
AU  - Knežević, Violeta
AU  - Demir, Hande
AU  - Filipović, Jelena
AU  - Manojlović, Dragan
PY  - 2022
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/5582
AB  - The osmotic dehydration (OD) of celery root in sugar beet molasses was studied at three temperatures (20, 35, and 50 °C) and three immersion periods (1, 3, and 5 h) in order to examine the changes in antioxidant potential and phenolic profile of celery root throughout the process. The antioxidant capacity (AOC) of dehydrated samples was evaluated by spectrophotometric and polarographic assays, the total phenolic content by the Folin-Ciocalteu method, and the individual phenolic compounds by HPLC-DAD. As a result of OD in molasses, the AOC and phenols content in samples increased proportionally to the augmentation of temperature and the immersion time. Vanillic acid, syringic acid, and catechin were detected in dehydrated samples as a result of transfer from molasses. Compared to fresh celery root, the content of identified phenols in osmodehydrated samples was improved from 1.5 to 6.2 times. Strong correlations between applied assays were obtained, except for the DPPH. Based on the correlation analysis chlorogenic acid, gallic acid, chrysin, catechin, and kaempferol showed the greatest contribution to the overall AOC of osmodehydrated celery root. Molasses, an agro-industrial waste from sugar production, could be valorized as a valuable osmotic solution.
PB  - MDPI
T2  - Foods
T1  - Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses
VL  - 11
IS  - 13
SP  - 1945
DO  - 10.3390/foods11131945
ER  - 
@article{
author = "Nićetin, Milica and Pezo, Lato and Pergal, Marija and Lončar, Biljana and Filipović, Vladimir and Knežević, Violeta and Demir, Hande and Filipović, Jelena and Manojlović, Dragan",
year = "2022",
abstract = "The osmotic dehydration (OD) of celery root in sugar beet molasses was studied at three temperatures (20, 35, and 50 °C) and three immersion periods (1, 3, and 5 h) in order to examine the changes in antioxidant potential and phenolic profile of celery root throughout the process. The antioxidant capacity (AOC) of dehydrated samples was evaluated by spectrophotometric and polarographic assays, the total phenolic content by the Folin-Ciocalteu method, and the individual phenolic compounds by HPLC-DAD. As a result of OD in molasses, the AOC and phenols content in samples increased proportionally to the augmentation of temperature and the immersion time. Vanillic acid, syringic acid, and catechin were detected in dehydrated samples as a result of transfer from molasses. Compared to fresh celery root, the content of identified phenols in osmodehydrated samples was improved from 1.5 to 6.2 times. Strong correlations between applied assays were obtained, except for the DPPH. Based on the correlation analysis chlorogenic acid, gallic acid, chrysin, catechin, and kaempferol showed the greatest contribution to the overall AOC of osmodehydrated celery root. Molasses, an agro-industrial waste from sugar production, could be valorized as a valuable osmotic solution.",
publisher = "MDPI",
journal = "Foods",
title = "Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses",
volume = "11",
number = "13",
pages = "1945",
doi = "10.3390/foods11131945"
}
Nićetin, M., Pezo, L., Pergal, M., Lončar, B., Filipović, V., Knežević, V., Demir, H., Filipović, J.,& Manojlović, D.. (2022). Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses. in Foods
MDPI., 11(13), 1945.
https://doi.org/10.3390/foods11131945
Nićetin M, Pezo L, Pergal M, Lončar B, Filipović V, Knežević V, Demir H, Filipović J, Manojlović D. Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses. in Foods. 2022;11(13):1945.
doi:10.3390/foods11131945 .
Nićetin, Milica, Pezo, Lato, Pergal, Marija, Lončar, Biljana, Filipović, Vladimir, Knežević, Violeta, Demir, Hande, Filipović, Jelena, Manojlović, Dragan, "Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses" in Foods, 11, no. 13 (2022):1945,
https://doi.org/10.3390/foods11131945 . .
5
3

Chemical Composition and Antibacterial Activity of Angelica archangelica Root Essential Oil

Aćimović, Milica; Pavlovic, Snezana D.; Varga, Ana; Filipović, Vladimir M.; Cvetković, Mirjana; Stanković, Jovana; Čabarkapa, Ivana

(Natural Product Incorporation, 2017)

TY  - JOUR
AU  - Aćimović, Milica
AU  - Pavlovic, Snezana D.
AU  - Varga, Ana
AU  - Filipović, Vladimir M.
AU  - Cvetković, Mirjana
AU  - Stanković, Jovana
AU  - Čabarkapa, Ivana
PY  - 2017
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/2192
AB  - Roots of wild growing Angelica archangelica L. from Mt. Ozren (Serbia) were subjected to hydrodistillation and GC-MS analysis. The roots contained 0.10% of essential oil with alpha-pinene (29.7%), delta-3-carene (14.2%), and a mixture of beta-phellandrene and limonene (13.2%) as main compounds. The modified resazurin microtiter-plate assay was used to evaluate the antibacterial activity of the essential oil against Staphylococcus aureus and Escherichia coli. The minimum inhibitory concentration (MIC) values were 14.2 mu L/mL for S. aureus and 28.4 mu L/mL for E. coli, while the minimum bactericidal concentrations (MBC) were 56.8 mu L/mL and 113.6 mu L/mL, respectively. According to the obtained results, the angelica root essential oil can be applied as a natural preservative in food and as a natural antibiotic for the treatment of several infectious diseases caused by these two bacteria.
PB  - Natural Product Incorporation
T2  - Natural Product Communications
T1  - Chemical Composition and Antibacterial Activity of Angelica archangelica Root Essential Oil
VL  - 12
IS  - 2
SP  - 205
EP  - 206
UR  - https://hdl.handle.net/21.15107/rcub_cer_2192
ER  - 
@article{
author = "Aćimović, Milica and Pavlovic, Snezana D. and Varga, Ana and Filipović, Vladimir M. and Cvetković, Mirjana and Stanković, Jovana and Čabarkapa, Ivana",
year = "2017",
abstract = "Roots of wild growing Angelica archangelica L. from Mt. Ozren (Serbia) were subjected to hydrodistillation and GC-MS analysis. The roots contained 0.10% of essential oil with alpha-pinene (29.7%), delta-3-carene (14.2%), and a mixture of beta-phellandrene and limonene (13.2%) as main compounds. The modified resazurin microtiter-plate assay was used to evaluate the antibacterial activity of the essential oil against Staphylococcus aureus and Escherichia coli. The minimum inhibitory concentration (MIC) values were 14.2 mu L/mL for S. aureus and 28.4 mu L/mL for E. coli, while the minimum bactericidal concentrations (MBC) were 56.8 mu L/mL and 113.6 mu L/mL, respectively. According to the obtained results, the angelica root essential oil can be applied as a natural preservative in food and as a natural antibiotic for the treatment of several infectious diseases caused by these two bacteria.",
publisher = "Natural Product Incorporation",
journal = "Natural Product Communications",
title = "Chemical Composition and Antibacterial Activity of Angelica archangelica Root Essential Oil",
volume = "12",
number = "2",
pages = "205-206",
url = "https://hdl.handle.net/21.15107/rcub_cer_2192"
}
Aćimović, M., Pavlovic, S. D., Varga, A., Filipović, V. M., Cvetković, M., Stanković, J.,& Čabarkapa, I.. (2017). Chemical Composition and Antibacterial Activity of Angelica archangelica Root Essential Oil. in Natural Product Communications
Natural Product Incorporation., 12(2), 205-206.
https://hdl.handle.net/21.15107/rcub_cer_2192
Aćimović M, Pavlovic SD, Varga A, Filipović VM, Cvetković M, Stanković J, Čabarkapa I. Chemical Composition and Antibacterial Activity of Angelica archangelica Root Essential Oil. in Natural Product Communications. 2017;12(2):205-206.
https://hdl.handle.net/21.15107/rcub_cer_2192 .
Aćimović, Milica, Pavlovic, Snezana D., Varga, Ana, Filipović, Vladimir M., Cvetković, Mirjana, Stanković, Jovana, Čabarkapa, Ivana, "Chemical Composition and Antibacterial Activity of Angelica archangelica Root Essential Oil" in Natural Product Communications, 12, no. 2 (2017):205-206,
https://hdl.handle.net/21.15107/rcub_cer_2192 .
6
15

The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material

Aćimović, Milica; Tešević, Vele; Mara, Dimitrije; Cvetković, Mirjana; Stanković, Jovana; Filipović, Vladimir M.

(Tehnološki fakultet, Leskovac, 2016)

TY  - JOUR
AU  - Aćimović, Milica
AU  - Tešević, Vele
AU  - Mara, Dimitrije
AU  - Cvetković, Mirjana
AU  - Stanković, Jovana
AU  - Filipović, Vladimir M.
PY  - 2016
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/1995
AB  - The essential oil content in cumin samples from Serbian market ranged between 2.0 and 4.0%, with 22 identified compounds, among which the most abundant were cumin aldehyde, β-pinene, γ-terpinene, γ-terpinene-7-al and p-cymene. Postdistillation cumin seeds waste material that remained after the essential oil extraction contains total polyphenols of between 30.1 and 47.5 mg GAE/g dry extract, as estimated by the Folin-Ciocalteu method. Hydroxybenzoic and hydroxycinnamic acids, as well as glycosides of flavonones and flavonoles, are the dominant polyphenols. However, according to DPPH method, the antioxidative potential of cumin postdistillation seeds waste was poor and it ranged between 0.02 and 0.04 mM TE/g. Further research will be focused on agro-food implementation of postdistillation waste material of cumin and other plants which are used for the essential oil production.
AB  - Sadržaj etarskog ulja u plodovima kumina prisutnog na Srpskom tržištu kreće se između 2.0 i 4.0%. Primenom GC/MS identifikovane je ukupno 22 komponente u etarskim uljima kumina, među kojima su najzastupljenije: kumin aldehid, β-pinen, γ-terpinen, γ-terpinen-7-al i p-cimen. Međutim, kako je sadržaj etarskog ulja u plodovima kumina mali (ispod 5%), veliki deo biljnog materijala ostaje neiskorišćen. Primenom tzv. Folin-Ciocalteu metoda, ustanovljeno je da ostaci nakon destilacije etarskog ulja iz plodova kumina sadrže između 30.1 i 47.5 mg GAE/g suvog ekstrakta ukupnih polifenola. Hidroksibenzoeva i hidroksicimetna kiselina, kao i glikozidi flavonona i flavonola, su najzastupljeniji polifenoli. Na osnovu DPPH-metoda antioksidativni potencijal ostataka nakon destilacije plodova kumina je slab i kreće se između 0.02 i 0.04 mM TE/g. Dalja istraživanja bi trebalo usmeriti ka primeni ostataka nakon destilacije plodova kumina i drugih biljaka koje se koriste za destilaciju etarskih ulja u prehrambenoj industriji i poljoprivredi.
PB  - Tehnološki fakultet, Leskovac
T2  - Advanced Technologies
T1  - The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material
T1  - Analiza etarskog ulja plodova kumina i ukupnih polifenola u ostacima nakon destilacije
VL  - 5
IS  - 1
SP  - 23
EP  - 30
DO  - 10.5937/savteh1601023A
ER  - 
@article{
author = "Aćimović, Milica and Tešević, Vele and Mara, Dimitrije and Cvetković, Mirjana and Stanković, Jovana and Filipović, Vladimir M.",
year = "2016",
abstract = "The essential oil content in cumin samples from Serbian market ranged between 2.0 and 4.0%, with 22 identified compounds, among which the most abundant were cumin aldehyde, β-pinene, γ-terpinene, γ-terpinene-7-al and p-cymene. Postdistillation cumin seeds waste material that remained after the essential oil extraction contains total polyphenols of between 30.1 and 47.5 mg GAE/g dry extract, as estimated by the Folin-Ciocalteu method. Hydroxybenzoic and hydroxycinnamic acids, as well as glycosides of flavonones and flavonoles, are the dominant polyphenols. However, according to DPPH method, the antioxidative potential of cumin postdistillation seeds waste was poor and it ranged between 0.02 and 0.04 mM TE/g. Further research will be focused on agro-food implementation of postdistillation waste material of cumin and other plants which are used for the essential oil production., Sadržaj etarskog ulja u plodovima kumina prisutnog na Srpskom tržištu kreće se između 2.0 i 4.0%. Primenom GC/MS identifikovane je ukupno 22 komponente u etarskim uljima kumina, među kojima su najzastupljenije: kumin aldehid, β-pinen, γ-terpinen, γ-terpinen-7-al i p-cimen. Međutim, kako je sadržaj etarskog ulja u plodovima kumina mali (ispod 5%), veliki deo biljnog materijala ostaje neiskorišćen. Primenom tzv. Folin-Ciocalteu metoda, ustanovljeno je da ostaci nakon destilacije etarskog ulja iz plodova kumina sadrže između 30.1 i 47.5 mg GAE/g suvog ekstrakta ukupnih polifenola. Hidroksibenzoeva i hidroksicimetna kiselina, kao i glikozidi flavonona i flavonola, su najzastupljeniji polifenoli. Na osnovu DPPH-metoda antioksidativni potencijal ostataka nakon destilacije plodova kumina je slab i kreće se između 0.02 i 0.04 mM TE/g. Dalja istraživanja bi trebalo usmeriti ka primeni ostataka nakon destilacije plodova kumina i drugih biljaka koje se koriste za destilaciju etarskih ulja u prehrambenoj industriji i poljoprivredi.",
publisher = "Tehnološki fakultet, Leskovac",
journal = "Advanced Technologies",
title = "The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material, Analiza etarskog ulja plodova kumina i ukupnih polifenola u ostacima nakon destilacije",
volume = "5",
number = "1",
pages = "23-30",
doi = "10.5937/savteh1601023A"
}
Aćimović, M., Tešević, V., Mara, D., Cvetković, M., Stanković, J.,& Filipović, V. M.. (2016). The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material. in Advanced Technologies
Tehnološki fakultet, Leskovac., 5(1), 23-30.
https://doi.org/10.5937/savteh1601023A
Aćimović M, Tešević V, Mara D, Cvetković M, Stanković J, Filipović VM. The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material. in Advanced Technologies. 2016;5(1):23-30.
doi:10.5937/savteh1601023A .
Aćimović, Milica, Tešević, Vele, Mara, Dimitrije, Cvetković, Mirjana, Stanković, Jovana, Filipović, Vladimir M., "The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material" in Advanced Technologies, 5, no. 1 (2016):23-30,
https://doi.org/10.5937/savteh1601023A . .
8

The influence of environmental conditions on Carum carvi L. var. annum seed quality

Aćimović, Milica; Filipović, Vladimir M.; Stanković, Jovana; Cvetković, Mirjana; Đukanović, Lana

(Institute of field and vegetable crops, Novi Sad, 2015)

TY  - JOUR
AU  - Aćimović, Milica
AU  - Filipović, Vladimir M.
AU  - Stanković, Jovana
AU  - Cvetković, Mirjana
AU  - Đukanović, Lana
PY  - 2015
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/1778
AB  - Field experiments were carried out during two growing seasons with annual caraway, at three localities, in order to determine the effect of different environmental conditions on the quality of seed as reproductive material. During the experiment, it was found that the quality of caraway seed was significantly lower in the hotter and drier year in comparison to the year with moderate conditions. Unfavourable weather conditions caused premature ripening and consequently thousand seed weight was low and lower amounts of essential oils were stored in the seed. By applying the linear regressions method it was established that the total variability of both thousand seed weight and the amount of essential oil per seed were due to its association with harvest index. Because of better characteristics of seed during the moderate year, the germination energy and total germination were significantly higher, and reproductive material was of good quality.
AB  - Poljski ogled izveden tokom dve godine sa jednogodišnjim kimom na tri lokaliteta imao je za cilj determinaciju uticaja različitih ekoloških uslova na kvalitet semenskog materijala ove biljke. Utvrđeno je da je kvalitet semena kima značajno lošiji u godini koja je bila sušna i praćena visokim temperaturama u poređenju sa godinom sa umerenim vrednostima klimatskih parametara. Nepovoljni vremenski uslovi uzrokovali su prevremeno zrenje i kao posledica toga došlo je do obrazovanja male mase hiljadu semena i akumulacije manje količine etarskog ulja u semenu. Primenom modela linearne regresije ustanovljeno je da su varijabilnost mase hiljadu semena i količina etarskog ulja u semenu u direktnoj vezi sa žetvenim indeksom. Zbog boljih karakteristika semena formiranog u uslovima umerene godine, energija klijanja i ukupna klijavost su značajno veće, što je dovelo do toga da reproduktivni materijal iz te godine ima bolji kvalitet.
PB  - Institute of field and vegetable crops, Novi Sad
T2  - Ratarstvo i povrtarstvo
T1  - The influence of environmental conditions on Carum carvi L. var. annum seed quality
T1  - Uticaj ekoloških faktora na kvalitet semena Carum carvi L. var. annum
VL  - 52
IS  - 3
SP  - 91
EP  - 96
DO  - 10.5937/ratpov52-8022
ER  - 
@article{
author = "Aćimović, Milica and Filipović, Vladimir M. and Stanković, Jovana and Cvetković, Mirjana and Đukanović, Lana",
year = "2015",
abstract = "Field experiments were carried out during two growing seasons with annual caraway, at three localities, in order to determine the effect of different environmental conditions on the quality of seed as reproductive material. During the experiment, it was found that the quality of caraway seed was significantly lower in the hotter and drier year in comparison to the year with moderate conditions. Unfavourable weather conditions caused premature ripening and consequently thousand seed weight was low and lower amounts of essential oils were stored in the seed. By applying the linear regressions method it was established that the total variability of both thousand seed weight and the amount of essential oil per seed were due to its association with harvest index. Because of better characteristics of seed during the moderate year, the germination energy and total germination were significantly higher, and reproductive material was of good quality., Poljski ogled izveden tokom dve godine sa jednogodišnjim kimom na tri lokaliteta imao je za cilj determinaciju uticaja različitih ekoloških uslova na kvalitet semenskog materijala ove biljke. Utvrđeno je da je kvalitet semena kima značajno lošiji u godini koja je bila sušna i praćena visokim temperaturama u poređenju sa godinom sa umerenim vrednostima klimatskih parametara. Nepovoljni vremenski uslovi uzrokovali su prevremeno zrenje i kao posledica toga došlo je do obrazovanja male mase hiljadu semena i akumulacije manje količine etarskog ulja u semenu. Primenom modela linearne regresije ustanovljeno je da su varijabilnost mase hiljadu semena i količina etarskog ulja u semenu u direktnoj vezi sa žetvenim indeksom. Zbog boljih karakteristika semena formiranog u uslovima umerene godine, energija klijanja i ukupna klijavost su značajno veće, što je dovelo do toga da reproduktivni materijal iz te godine ima bolji kvalitet.",
publisher = "Institute of field and vegetable crops, Novi Sad",
journal = "Ratarstvo i povrtarstvo",
title = "The influence of environmental conditions on Carum carvi L. var. annum seed quality, Uticaj ekoloških faktora na kvalitet semena Carum carvi L. var. annum",
volume = "52",
number = "3",
pages = "91-96",
doi = "10.5937/ratpov52-8022"
}
Aćimović, M., Filipović, V. M., Stanković, J., Cvetković, M.,& Đukanović, L.. (2015). The influence of environmental conditions on Carum carvi L. var. annum seed quality. in Ratarstvo i povrtarstvo
Institute of field and vegetable crops, Novi Sad., 52(3), 91-96.
https://doi.org/10.5937/ratpov52-8022
Aćimović M, Filipović VM, Stanković J, Cvetković M, Đukanović L. The influence of environmental conditions on Carum carvi L. var. annum seed quality. in Ratarstvo i povrtarstvo. 2015;52(3):91-96.
doi:10.5937/ratpov52-8022 .
Aćimović, Milica, Filipović, Vladimir M., Stanković, Jovana, Cvetković, Mirjana, Đukanović, Lana, "The influence of environmental conditions on Carum carvi L. var. annum seed quality" in Ratarstvo i povrtarstvo, 52, no. 3 (2015):91-96,
https://doi.org/10.5937/ratpov52-8022 . .
6

Essential oil composition from sweet and bitter fennel fruits from Serbia

Aćimović, Milica; Kostadinović, Ljiljana; Stanković, Jovana; Cvetković, Mirjana; Filipović, Vladimir M.

(Institute for Medicinal Plants Research "Dr. Josif Pancic", 2015)

TY  - JOUR
AU  - Aćimović, Milica
AU  - Kostadinović, Ljiljana
AU  - Stanković, Jovana
AU  - Cvetković, Mirjana
AU  - Filipović, Vladimir M.
PY  - 2015
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/1790
AB  - Fennel (Foeniculum vulgare Mill.) is aromatic plant from Apiaceae family. There are two types that have commercial importance, sweet fennel Foeniculum vulgare var. dulce, and bitter fennel - Foeniculum vulgare var. vulgare. The aim of this study was to examine the quality of essential oil of the fruits of these two varieties. Plants were grown in the experimental field in Mošorin for two years and from the produced fruits, essential oil was obtained by hydrodistillation method according to Clevenger apparatus, while the essential oil components were determined through GC/MS.Sweet fennel (variety 'Fino', Austrosaat AG, Austria) and bitter fennel (variety 'Vojvođanski', Dr Josif Pančić, Serbia) grown in Serbia, as most abundant compound of the essential oil had trans-anethole. In the var. dulceits part was from 77.2-80.0%, while the content of methyl-chavicol was 2.2- 2.7 %, and fenchone 3.9-5.1%. The var. vulgarehad 61.1-67.1 % trans-anethole and fenchone 22.6-26.6 % depended on the year.
AB  - Komorač (Foeniculum vulgare Mill.) je aromatična biljka iz familije Apiaceae. Postoje dva varijeteta od komercijalnog značaja: slatki komorač Foeniculum vulgare Mill. subsp. vulgare var. dulce (Mill.) i gorki komorač - Foeniculum vulgare Mill. subsp. vulgare var. vulgare. Cilj ovog istraživanja bio je da se ispita kvalitet etarskog ulja plodovaova dva varijeteta. Biljke su gajene na oglednom polju u Mošorinu tokom dve godine, a iz dobijenih plodova etarsko ulje je dobijeno postupkom hidrodestilacije na aparaturi po Clevenger-u, a određivanje komponenata atarskog ulja putem GC/MS.Slatki komorač (sorta 'Fino', Austrosaat AG, Austrija) i gorki komorač (sorta 'Vojvođanski', Dr Josif Pančić, Srbija) u etarskom ulju kao najzastupljeniju komponentu je imali su trans-anetol. U varijetetu dulce njegov udeo je bio od 77,2 - 80,0 %, dok je sadržaj metil kavikola bio 2,2-2,7 %, a fenhona 3,9 - 5,1 %. Varijetet vulgare je imao 61,1 - 67,1 % trans-anetola a fenhona 22,6-26,6 % u zavisnosti od godine.
PB  - Institute for Medicinal Plants Research "Dr. Josif Pancic"
T2  - Lekovite sirovine
T1  - Essential oil composition from sweet and bitter fennel fruits from Serbia
T1  - Hemijski sastav etarskog ulja plodova slatkog i gorkog komorača iz Srbije
IS  - 35
SP  - 121
EP  - 129
DO  - 10.5937/leksir1535121A
ER  - 
@article{
author = "Aćimović, Milica and Kostadinović, Ljiljana and Stanković, Jovana and Cvetković, Mirjana and Filipović, Vladimir M.",
year = "2015",
abstract = "Fennel (Foeniculum vulgare Mill.) is aromatic plant from Apiaceae family. There are two types that have commercial importance, sweet fennel Foeniculum vulgare var. dulce, and bitter fennel - Foeniculum vulgare var. vulgare. The aim of this study was to examine the quality of essential oil of the fruits of these two varieties. Plants were grown in the experimental field in Mošorin for two years and from the produced fruits, essential oil was obtained by hydrodistillation method according to Clevenger apparatus, while the essential oil components were determined through GC/MS.Sweet fennel (variety 'Fino', Austrosaat AG, Austria) and bitter fennel (variety 'Vojvođanski', Dr Josif Pančić, Serbia) grown in Serbia, as most abundant compound of the essential oil had trans-anethole. In the var. dulceits part was from 77.2-80.0%, while the content of methyl-chavicol was 2.2- 2.7 %, and fenchone 3.9-5.1%. The var. vulgarehad 61.1-67.1 % trans-anethole and fenchone 22.6-26.6 % depended on the year., Komorač (Foeniculum vulgare Mill.) je aromatična biljka iz familije Apiaceae. Postoje dva varijeteta od komercijalnog značaja: slatki komorač Foeniculum vulgare Mill. subsp. vulgare var. dulce (Mill.) i gorki komorač - Foeniculum vulgare Mill. subsp. vulgare var. vulgare. Cilj ovog istraživanja bio je da se ispita kvalitet etarskog ulja plodovaova dva varijeteta. Biljke su gajene na oglednom polju u Mošorinu tokom dve godine, a iz dobijenih plodova etarsko ulje je dobijeno postupkom hidrodestilacije na aparaturi po Clevenger-u, a određivanje komponenata atarskog ulja putem GC/MS.Slatki komorač (sorta 'Fino', Austrosaat AG, Austrija) i gorki komorač (sorta 'Vojvođanski', Dr Josif Pančić, Srbija) u etarskom ulju kao najzastupljeniju komponentu je imali su trans-anetol. U varijetetu dulce njegov udeo je bio od 77,2 - 80,0 %, dok je sadržaj metil kavikola bio 2,2-2,7 %, a fenhona 3,9 - 5,1 %. Varijetet vulgare je imao 61,1 - 67,1 % trans-anetola a fenhona 22,6-26,6 % u zavisnosti od godine.",
publisher = "Institute for Medicinal Plants Research "Dr. Josif Pancic"",
journal = "Lekovite sirovine",
title = "Essential oil composition from sweet and bitter fennel fruits from Serbia, Hemijski sastav etarskog ulja plodova slatkog i gorkog komorača iz Srbije",
number = "35",
pages = "121-129",
doi = "10.5937/leksir1535121A"
}
Aćimović, M., Kostadinović, L., Stanković, J., Cvetković, M.,& Filipović, V. M.. (2015). Essential oil composition from sweet and bitter fennel fruits from Serbia. in Lekovite sirovine
Institute for Medicinal Plants Research "Dr. Josif Pancic".(35), 121-129.
https://doi.org/10.5937/leksir1535121A
Aćimović M, Kostadinović L, Stanković J, Cvetković M, Filipović VM. Essential oil composition from sweet and bitter fennel fruits from Serbia. in Lekovite sirovine. 2015;(35):121-129.
doi:10.5937/leksir1535121A .
Aćimović, Milica, Kostadinović, Ljiljana, Stanković, Jovana, Cvetković, Mirjana, Filipović, Vladimir M., "Essential oil composition from sweet and bitter fennel fruits from Serbia" in Lekovite sirovine, no. 35 (2015):121-129,
https://doi.org/10.5937/leksir1535121A . .
3