A Voltammetric Method for the Quantitative Determination of Midecamycin Compared to Its Simultaneous HPLC Determination
Само за регистроване кориснике
2011
Аутори
Drljevic-Djuric, K. M.Avramov Ivić, Milka
Petrović, Slobodan D.
Mijin, Dušan
Jadranin, Milka
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The aim of this study was to present the quantitative determination of midecamycin at a gold electrode in 0.05 M NaHCO(3) using cyclic linear sweep voltammetry. It was found that the value of the oxidative peak of pure midecamycin at 0.85 V vs. SCE at a scan rate of 50 mV s(-1) is a linear function of the concentration in the range 0.1693-0.3289 mg cm(-3). The value of its reductive peak at 0.3 V vs. SCE is a linear function of the concentration in the range 0.11396-0.3802 mg cm(-3). HPLC analysis of the bulk of electrolyte confirmed the data obtained by analysis of the current peak values concerning the correlation with each investigated concentration of midecamycin. By MS spectrometry no degradation products were found in electrolyte during its quantitative determination.
Кључне речи:
midecamycin / gold electrode / quantitative determination / HPLC / MS spectrometryИзвор:
Russian Journal of Electrochemistry, 2011, 47, 7, 781-786Издавач:
- Maik Nauka/Interperiodica/Springer, New York
Финансирање / пројекти:
- Проучавање синтезе, структуре и активности органских једињења природног и синтетског порекла (RS-172013)
DOI: 10.1134/S1023193511070056
ISSN: 1023-1935
WoS: 000295530300003
Scopus: 2-s2.0-80052644417
Институција/група
IHTMTY - JOUR AU - Drljevic-Djuric, K. M. AU - Avramov Ivić, Milka AU - Petrović, Slobodan D. AU - Mijin, Dušan AU - Jadranin, Milka PY - 2011 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/848 AB - The aim of this study was to present the quantitative determination of midecamycin at a gold electrode in 0.05 M NaHCO(3) using cyclic linear sweep voltammetry. It was found that the value of the oxidative peak of pure midecamycin at 0.85 V vs. SCE at a scan rate of 50 mV s(-1) is a linear function of the concentration in the range 0.1693-0.3289 mg cm(-3). The value of its reductive peak at 0.3 V vs. SCE is a linear function of the concentration in the range 0.11396-0.3802 mg cm(-3). HPLC analysis of the bulk of electrolyte confirmed the data obtained by analysis of the current peak values concerning the correlation with each investigated concentration of midecamycin. By MS spectrometry no degradation products were found in electrolyte during its quantitative determination. PB - Maik Nauka/Interperiodica/Springer, New York T2 - Russian Journal of Electrochemistry T1 - A Voltammetric Method for the Quantitative Determination of Midecamycin Compared to Its Simultaneous HPLC Determination VL - 47 IS - 7 SP - 781 EP - 786 DO - 10.1134/S1023193511070056 ER -
@article{ author = "Drljevic-Djuric, K. M. and Avramov Ivić, Milka and Petrović, Slobodan D. and Mijin, Dušan and Jadranin, Milka", year = "2011", abstract = "The aim of this study was to present the quantitative determination of midecamycin at a gold electrode in 0.05 M NaHCO(3) using cyclic linear sweep voltammetry. It was found that the value of the oxidative peak of pure midecamycin at 0.85 V vs. SCE at a scan rate of 50 mV s(-1) is a linear function of the concentration in the range 0.1693-0.3289 mg cm(-3). The value of its reductive peak at 0.3 V vs. SCE is a linear function of the concentration in the range 0.11396-0.3802 mg cm(-3). HPLC analysis of the bulk of electrolyte confirmed the data obtained by analysis of the current peak values concerning the correlation with each investigated concentration of midecamycin. By MS spectrometry no degradation products were found in electrolyte during its quantitative determination.", publisher = "Maik Nauka/Interperiodica/Springer, New York", journal = "Russian Journal of Electrochemistry", title = "A Voltammetric Method for the Quantitative Determination of Midecamycin Compared to Its Simultaneous HPLC Determination", volume = "47", number = "7", pages = "781-786", doi = "10.1134/S1023193511070056" }
Drljevic-Djuric, K. M., Avramov Ivić, M., Petrović, S. D., Mijin, D.,& Jadranin, M.. (2011). A Voltammetric Method for the Quantitative Determination of Midecamycin Compared to Its Simultaneous HPLC Determination. in Russian Journal of Electrochemistry Maik Nauka/Interperiodica/Springer, New York., 47(7), 781-786. https://doi.org/10.1134/S1023193511070056
Drljevic-Djuric KM, Avramov Ivić M, Petrović SD, Mijin D, Jadranin M. A Voltammetric Method for the Quantitative Determination of Midecamycin Compared to Its Simultaneous HPLC Determination. in Russian Journal of Electrochemistry. 2011;47(7):781-786. doi:10.1134/S1023193511070056 .
Drljevic-Djuric, K. M., Avramov Ivić, Milka, Petrović, Slobodan D., Mijin, Dušan, Jadranin, Milka, "A Voltammetric Method for the Quantitative Determination of Midecamycin Compared to Its Simultaneous HPLC Determination" in Russian Journal of Electrochemistry, 47, no. 7 (2011):781-786, https://doi.org/10.1134/S1023193511070056 . .