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Synthesis of submicron carbon spheres by the ultrasonic spray pyrolysis method

Authorized Users Only
2010
Authors
Jokić, Bojan
Drmanić, Saša Ž.
Radetić, Tamara
Krstić, Jugoslav
Petrovic, R.
Orlovic, A.
Janaćković, Đorđe
Article (Published version)
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Abstract
Submicron carbon spherical particles were obtained by polycondensation of resorcinol and formaldehyde in a solution and subsequent ultrasonic spray pyrolysis of the prepared sol. Microscopic characterization indicates the regular spherical shape of the obtained particles and sphere diameters in 200-700 nm range. The carbon spheres are amorphous as confirmed by electron diffraction, EELS, XRD and HREM characterization. Activation procedure was performed with H2O in a nitrogen flow for 15 and 30 min at 800 degrees C. The activation procedure preserved the initial spherical shapes of the particles while the particle porosity and specific surface area were increased. The amount of surface oxygen functionalities was also increased by activation procedure as indicated by FTIR analysis.
Keywords:
Powder technology / Porosity / Nanomaterials
Source:
Materials Letters, 2010, 64, 20, 2173-2176
Publisher:
  • Elsevier
Funding / projects:
  • Sinteza, struktura, svojstva i primena funkcionalnih nanostrukturnih keramičkih i biokeramičkih materijala (RS-142070)
  • Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy - DE-AC02-05CH11231

DOI: 10.1016/j.matlet.2010.06.066

ISSN: 0167-577X

WoS: 000281997900009

Scopus: 2-s2.0-77955079994
[ Google Scholar ]
10
8
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/715
Collections
  • Radovi istraživača / Researchers' publications
Institution/Community
IHTM
TY  - JOUR
AU  - Jokić, Bojan
AU  - Drmanić, Saša Ž.
AU  - Radetić, Tamara
AU  - Krstić, Jugoslav
AU  - Petrovic, R.
AU  - Orlovic, A.
AU  - Janaćković, Đorđe
PY  - 2010
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/715
AB  - Submicron carbon spherical particles were obtained by polycondensation of resorcinol and formaldehyde in a solution and subsequent ultrasonic spray pyrolysis of the prepared sol. Microscopic characterization indicates the regular spherical shape of the obtained particles and sphere diameters in 200-700 nm range. The carbon spheres are amorphous as confirmed by electron diffraction, EELS, XRD and HREM characterization. Activation procedure was performed with H2O in a nitrogen flow for 15 and 30 min at 800 degrees C. The activation procedure preserved the initial spherical shapes of the particles while the particle porosity and specific surface area were increased. The amount of surface oxygen functionalities was also increased by activation procedure as indicated by FTIR analysis.
PB  - Elsevier
T2  - Materials Letters
T1  - Synthesis of submicron carbon spheres by the ultrasonic spray pyrolysis method
VL  - 64
IS  - 20
SP  - 2173
EP  - 2176
DO  - 10.1016/j.matlet.2010.06.066
ER  - 
@article{
author = "Jokić, Bojan and Drmanić, Saša Ž. and Radetić, Tamara and Krstić, Jugoslav and Petrovic, R. and Orlovic, A. and Janaćković, Đorđe",
year = "2010",
abstract = "Submicron carbon spherical particles were obtained by polycondensation of resorcinol and formaldehyde in a solution and subsequent ultrasonic spray pyrolysis of the prepared sol. Microscopic characterization indicates the regular spherical shape of the obtained particles and sphere diameters in 200-700 nm range. The carbon spheres are amorphous as confirmed by electron diffraction, EELS, XRD and HREM characterization. Activation procedure was performed with H2O in a nitrogen flow for 15 and 30 min at 800 degrees C. The activation procedure preserved the initial spherical shapes of the particles while the particle porosity and specific surface area were increased. The amount of surface oxygen functionalities was also increased by activation procedure as indicated by FTIR analysis.",
publisher = "Elsevier",
journal = "Materials Letters",
title = "Synthesis of submicron carbon spheres by the ultrasonic spray pyrolysis method",
volume = "64",
number = "20",
pages = "2173-2176",
doi = "10.1016/j.matlet.2010.06.066"
}
Jokić, B., Drmanić, S. Ž., Radetić, T., Krstić, J., Petrovic, R., Orlovic, A.,& Janaćković, Đ.. (2010). Synthesis of submicron carbon spheres by the ultrasonic spray pyrolysis method. in Materials Letters
Elsevier., 64(20), 2173-2176.
https://doi.org/10.1016/j.matlet.2010.06.066
Jokić B, Drmanić SŽ, Radetić T, Krstić J, Petrovic R, Orlovic A, Janaćković Đ. Synthesis of submicron carbon spheres by the ultrasonic spray pyrolysis method. in Materials Letters. 2010;64(20):2173-2176.
doi:10.1016/j.matlet.2010.06.066 .
Jokić, Bojan, Drmanić, Saša Ž., Radetić, Tamara, Krstić, Jugoslav, Petrovic, R., Orlovic, A., Janaćković, Đorđe, "Synthesis of submicron carbon spheres by the ultrasonic spray pyrolysis method" in Materials Letters, 64, no. 20 (2010):2173-2176,
https://doi.org/10.1016/j.matlet.2010.06.066 . .

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