Validacija metode za određivanje sadržaja citrata u bagremovom medu jonskom hromatografijom
Method validation for determining the citrate content in acacia honey by ion chromatography
Аутори
Simić, AleksandarTosti, Tomislav
Dramićanin, Aleksandra M.
Šegan, Sandra
Milojković-Opsenica, Dušanka
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
Sadržaj limunske kiseline u medu može da pruži informacije za procenu autenticnosti
meda. Me utim, važeci Codexalimentarius kao i Pravilnik o kvalitetu meda ne pružaju
informacije o sadržaju limunske kiseline u medu. Imajuci to u vidu, predmet ovog rada je
razvoj i validacija metode za odre ivanje citrata u medu. Analiza citrata ura ena je
primenom jonske hromatografijesa konduktometrijskom detekcijom na DIONEX AS 15
analitickoj koloni uz upotrebu 30 mM kalijum-hidroksida kao mobilne faze.Validovana
metoda se može primeniti za odre ivanje sadržaja citrata u medu u intervalu 1 – 100 mg/kg
s agranicom detekcije od 0,36 mg/kg igranicomkvantifikacije 1,20 mg/kg.Tacnost metode
je proverena testom obogacenja (95 – 101%), a preciznost ponovljenim analizama u toku
više dana. Metoda je proverena analizom 25 uzoraka bagremovog meda pri cemu je
sadržaj citrata bio u opsegu 10,82 – 55,74 mg/kg. Parametri validacije metode potvr uju
mogucnost primene jonskehromatografije sa konduktometri...jskom detekcijom za brzo i
tacno odre ivanje citrata u uzorcima bagremovog meda.
The citric acid content can give useful information about honey authenticity. However, Codex Alimentarius and the Serbian regulation do not provide information on the content of citric acid in honey. Hence,the object of this paper is the method development and validation for the determination of citrate content in honey. The concentration of citrate in honey was determined by ion chromatography with conductivity detection on DIONEX AS 15 column and 30 mM potassium-hydroxide as mobile phase. The method validation revealed that method can be used for determination of citrate in acaciahoney from 1 to100 mg/kg. The limit of detection was 0.36 mg/kg and limit of quantification 1.20 mg/kg. The accuracy was determined with recovery test (95–101%), and precision with repeat analysis during few days. Analysis of 25 acacia honey samples confirmed applicability of method and revealed that amount of citrate was10.82 – 55.74 mg/kg. The statistical parameters of method validation pointed out that th...e ion chromatography with conductometry detection enabled rapid and accurate determination of citrate in acacia honey.
Кључне речи:
citric acid / honey authenticity / method validationИзвор:
Kratki izvodi radova, knjiga radova - 58. Savetovanje Srpskog hemijskog društva, 9. i 10. jun 2022. godine, Beograd / Book of Abstracts, Proceedings - 58th Meeting of the Serbian Chemical Society, June 9-10, 2023, Belgrade, Serbia, 2022, 56-56Издавач:
- Belgrade : Serbian Chemical Society
Институција/група
IHTMTY - CONF AU - Simić, Aleksandar AU - Tosti, Tomislav AU - Dramićanin, Aleksandra M. AU - Šegan, Sandra AU - Milojković-Opsenica, Dušanka PY - 2022 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/6735 AB - Sadržaj limunske kiseline u medu može da pruži informacije za procenu autenticnosti meda. Me utim, važeci Codexalimentarius kao i Pravilnik o kvalitetu meda ne pružaju informacije o sadržaju limunske kiseline u medu. Imajuci to u vidu, predmet ovog rada je razvoj i validacija metode za odre ivanje citrata u medu. Analiza citrata ura ena je primenom jonske hromatografijesa konduktometrijskom detekcijom na DIONEX AS 15 analitickoj koloni uz upotrebu 30 mM kalijum-hidroksida kao mobilne faze.Validovana metoda se može primeniti za odre ivanje sadržaja citrata u medu u intervalu 1 – 100 mg/kg s agranicom detekcije od 0,36 mg/kg igranicomkvantifikacije 1,20 mg/kg.Tacnost metode je proverena testom obogacenja (95 – 101%), a preciznost ponovljenim analizama u toku više dana. Metoda je proverena analizom 25 uzoraka bagremovog meda pri cemu je sadržaj citrata bio u opsegu 10,82 – 55,74 mg/kg. Parametri validacije metode potvr uju mogucnost primene jonskehromatografije sa konduktometrijskom detekcijom za brzo i tacno odre ivanje citrata u uzorcima bagremovog meda. AB - The citric acid content can give useful information about honey authenticity. However, Codex Alimentarius and the Serbian regulation do not provide information on the content of citric acid in honey. Hence,the object of this paper is the method development and validation for the determination of citrate content in honey. The concentration of citrate in honey was determined by ion chromatography with conductivity detection on DIONEX AS 15 column and 30 mM potassium-hydroxide as mobile phase. The method validation revealed that method can be used for determination of citrate in acaciahoney from 1 to100 mg/kg. The limit of detection was 0.36 mg/kg and limit of quantification 1.20 mg/kg. The accuracy was determined with recovery test (95–101%), and precision with repeat analysis during few days. Analysis of 25 acacia honey samples confirmed applicability of method and revealed that amount of citrate was10.82 – 55.74 mg/kg. The statistical parameters of method validation pointed out that the ion chromatography with conductometry detection enabled rapid and accurate determination of citrate in acacia honey. PB - Belgrade : Serbian Chemical Society C3 - Kratki izvodi radova, knjiga radova - 58. Savetovanje Srpskog hemijskog društva, 9. i 10. jun 2022. godine, Beograd / Book of Abstracts, Proceedings - 58th Meeting of the Serbian Chemical Society, June 9-10, 2023, Belgrade, Serbia T1 - Validacija metode za određivanje sadržaja citrata u bagremovom medu jonskom hromatografijom T1 - Method validation for determining the citrate content in acacia honey by ion chromatography SP - 56 EP - 56 UR - https://hdl.handle.net/21.15107/rcub_cer_6735 ER -
@conference{ author = "Simić, Aleksandar and Tosti, Tomislav and Dramićanin, Aleksandra M. and Šegan, Sandra and Milojković-Opsenica, Dušanka", year = "2022", abstract = "Sadržaj limunske kiseline u medu može da pruži informacije za procenu autenticnosti meda. Me utim, važeci Codexalimentarius kao i Pravilnik o kvalitetu meda ne pružaju informacije o sadržaju limunske kiseline u medu. Imajuci to u vidu, predmet ovog rada je razvoj i validacija metode za odre ivanje citrata u medu. Analiza citrata ura ena je primenom jonske hromatografijesa konduktometrijskom detekcijom na DIONEX AS 15 analitickoj koloni uz upotrebu 30 mM kalijum-hidroksida kao mobilne faze.Validovana metoda se može primeniti za odre ivanje sadržaja citrata u medu u intervalu 1 – 100 mg/kg s agranicom detekcije od 0,36 mg/kg igranicomkvantifikacije 1,20 mg/kg.Tacnost metode je proverena testom obogacenja (95 – 101%), a preciznost ponovljenim analizama u toku više dana. Metoda je proverena analizom 25 uzoraka bagremovog meda pri cemu je sadržaj citrata bio u opsegu 10,82 – 55,74 mg/kg. Parametri validacije metode potvr uju mogucnost primene jonskehromatografije sa konduktometrijskom detekcijom za brzo i tacno odre ivanje citrata u uzorcima bagremovog meda., The citric acid content can give useful information about honey authenticity. However, Codex Alimentarius and the Serbian regulation do not provide information on the content of citric acid in honey. Hence,the object of this paper is the method development and validation for the determination of citrate content in honey. The concentration of citrate in honey was determined by ion chromatography with conductivity detection on DIONEX AS 15 column and 30 mM potassium-hydroxide as mobile phase. The method validation revealed that method can be used for determination of citrate in acaciahoney from 1 to100 mg/kg. The limit of detection was 0.36 mg/kg and limit of quantification 1.20 mg/kg. The accuracy was determined with recovery test (95–101%), and precision with repeat analysis during few days. Analysis of 25 acacia honey samples confirmed applicability of method and revealed that amount of citrate was10.82 – 55.74 mg/kg. The statistical parameters of method validation pointed out that the ion chromatography with conductometry detection enabled rapid and accurate determination of citrate in acacia honey.", publisher = "Belgrade : Serbian Chemical Society", journal = "Kratki izvodi radova, knjiga radova - 58. Savetovanje Srpskog hemijskog društva, 9. i 10. jun 2022. godine, Beograd / Book of Abstracts, Proceedings - 58th Meeting of the Serbian Chemical Society, June 9-10, 2023, Belgrade, Serbia", title = "Validacija metode za određivanje sadržaja citrata u bagremovom medu jonskom hromatografijom, Method validation for determining the citrate content in acacia honey by ion chromatography", pages = "56-56", url = "https://hdl.handle.net/21.15107/rcub_cer_6735" }
Simić, A., Tosti, T., Dramićanin, A. M., Šegan, S.,& Milojković-Opsenica, D.. (2022). Validacija metode za određivanje sadržaja citrata u bagremovom medu jonskom hromatografijom. in Kratki izvodi radova, knjiga radova - 58. Savetovanje Srpskog hemijskog društva, 9. i 10. jun 2022. godine, Beograd / Book of Abstracts, Proceedings - 58th Meeting of the Serbian Chemical Society, June 9-10, 2023, Belgrade, Serbia Belgrade : Serbian Chemical Society., 56-56. https://hdl.handle.net/21.15107/rcub_cer_6735
Simić A, Tosti T, Dramićanin AM, Šegan S, Milojković-Opsenica D. Validacija metode za određivanje sadržaja citrata u bagremovom medu jonskom hromatografijom. in Kratki izvodi radova, knjiga radova - 58. Savetovanje Srpskog hemijskog društva, 9. i 10. jun 2022. godine, Beograd / Book of Abstracts, Proceedings - 58th Meeting of the Serbian Chemical Society, June 9-10, 2023, Belgrade, Serbia. 2022;:56-56. https://hdl.handle.net/21.15107/rcub_cer_6735 .
Simić, Aleksandar, Tosti, Tomislav, Dramićanin, Aleksandra M., Šegan, Sandra, Milojković-Opsenica, Dušanka, "Validacija metode za određivanje sadržaja citrata u bagremovom medu jonskom hromatografijom" in Kratki izvodi radova, knjiga radova - 58. Savetovanje Srpskog hemijskog društva, 9. i 10. jun 2022. godine, Beograd / Book of Abstracts, Proceedings - 58th Meeting of the Serbian Chemical Society, June 9-10, 2023, Belgrade, Serbia (2022):56-56, https://hdl.handle.net/21.15107/rcub_cer_6735 .