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Hydride reduction of B-norcholestane 5α,6α-epoxide

Hidridna redukcija B-norholestan 5α,6α-epoksida

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2002
58.pdf (97.43Kb)
Authors
Bjelaković, Mira
Pavlović, Vladimir D.
Lorenc, Ljubinka
Article (Published version)
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Abstract
B-Norcholestane epoxide 2 is reduced with lithium aluminium hydride to give either the 3β,6α-diol 3 or the corresponding 3β,5α-diol 4, depending on the quality of the reducing reagent employed. Aplausible mechanistic explanation of the obtained results is suggested.
Redukcijom B-norholestan-epoksida 2 pomoću litijum-aluminijum-hidrida dobijeni su odgovarajući 3β,6α-diol 3 ili 3β,5α-diol 4, u zavisnosti od kvaliteta upotrebljenog redukcionog reagensa. Predloženo je verovatno mehanističko tumačenje dobijenih rezultata.
Keywords:
5α,6α-epoxy-B-norcholestan-3β-yl acetate / 5α-hydroxy-B-norcholestan-3β-yl acetate / 6α-hydroxy-B-nor-5β-cholestan-3β-yl acetate / lithium aluminium hydride / lithium triethylborohydride
Source:
Journal of the Serbian Chemical Society, 2002, 67, 2, 69-75
Publisher:
  • Serbian Chemical Society
Funding / projects:
  • Project MESTD

DOI: 10.2298/JSC0202069B

ISSN: 0352-5139

WoS: 000173995100001

Scopus: 2-s2.0-0036003604
[ Google Scholar ]
6
4
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/60
Collections
  • Radovi istraživača / Researchers' publications
Institution/Community
IHTM
TY  - JOUR
AU  - Bjelaković, Mira
AU  - Pavlović, Vladimir D.
AU  - Lorenc, Ljubinka
PY  - 2002
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/60
AB  - B-Norcholestane epoxide 2 is reduced with lithium aluminium hydride to give either the 3β,6α-diol 3 or the corresponding 3β,5α-diol 4, depending on the quality of the reducing reagent employed. Aplausible mechanistic explanation of the obtained results is suggested.
AB  - Redukcijom B-norholestan-epoksida 2 pomoću litijum-aluminijum-hidrida dobijeni su odgovarajući 3β,6α-diol 3 ili 3β,5α-diol 4, u zavisnosti od kvaliteta upotrebljenog redukcionog reagensa. Predloženo je verovatno mehanističko tumačenje dobijenih rezultata.
PB  - Serbian Chemical Society
T2  - Journal of the Serbian Chemical Society
T1  - Hydride reduction of B-norcholestane 5α,6α-epoxide
T1  - Hidridna redukcija B-norholestan 5α,6α-epoksida
VL  - 67
IS  - 2
SP  - 69
EP  - 75
DO  - 10.2298/JSC0202069B
ER  - 
@article{
author = "Bjelaković, Mira and Pavlović, Vladimir D. and Lorenc, Ljubinka",
year = "2002",
abstract = "B-Norcholestane epoxide 2 is reduced with lithium aluminium hydride to give either the 3β,6α-diol 3 or the corresponding 3β,5α-diol 4, depending on the quality of the reducing reagent employed. Aplausible mechanistic explanation of the obtained results is suggested., Redukcijom B-norholestan-epoksida 2 pomoću litijum-aluminijum-hidrida dobijeni su odgovarajući 3β,6α-diol 3 ili 3β,5α-diol 4, u zavisnosti od kvaliteta upotrebljenog redukcionog reagensa. Predloženo je verovatno mehanističko tumačenje dobijenih rezultata.",
publisher = "Serbian Chemical Society",
journal = "Journal of the Serbian Chemical Society",
title = "Hydride reduction of B-norcholestane 5α,6α-epoxide, Hidridna redukcija B-norholestan 5α,6α-epoksida",
volume = "67",
number = "2",
pages = "69-75",
doi = "10.2298/JSC0202069B"
}
Bjelaković, M., Pavlović, V. D.,& Lorenc, L.. (2002). Hydride reduction of B-norcholestane 5α,6α-epoxide. in Journal of the Serbian Chemical Society
Serbian Chemical Society., 67(2), 69-75.
https://doi.org/10.2298/JSC0202069B
Bjelaković M, Pavlović VD, Lorenc L. Hydride reduction of B-norcholestane 5α,6α-epoxide. in Journal of the Serbian Chemical Society. 2002;67(2):69-75.
doi:10.2298/JSC0202069B .
Bjelaković, Mira, Pavlović, Vladimir D., Lorenc, Ljubinka, "Hydride reduction of B-norcholestane 5α,6α-epoxide" in Journal of the Serbian Chemical Society, 67, no. 2 (2002):69-75,
https://doi.org/10.2298/JSC0202069B . .

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