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Hydride reduction of B-norcholestane 5α,6α-epoxide

Hidridna redukcija B-norholestan 5α,6α-epoksida

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2002
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Authors
Bjelaković, Mira
Pavlović, Vladimir D.
Lorenc, Ljubinka
Article (Published version)
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Abstract
B-Norcholestane epoxide 2 is reduced with lithium aluminium hydride to give either the 3β,6α-diol 3 or the corresponding 3β,5α-diol 4, depending on the quality of the reducing reagent employed. Aplausible mechanistic explanation of the obtained results is suggested.
Redukcijom B-norholestan-epoksida 2 pomoću litijum-aluminijum-hidrida dobijeni su odgovarajući 3β,6α-diol 3 ili 3β,5α-diol 4, u zavisnosti od kvaliteta upotrebljenog redukcionog reagensa. Predloženo je verovatno mehanističko tumačenje dobijenih rezultata.
Keywords:
5α,6α-epoxy-B-norcholestan-3β-yl acetate / 5α-hydroxy-B-norcholestan-3β-yl acetate / 6α-hydroxy-B-nor-5β-cholestan-3β-yl acetate / lithium aluminium hydride / lithium triethylborohydride
Source:
Journal of the Serbian Chemical Society, 2002, 67, 2, 69-75
Publisher:
  • Serbian Chemical Society
Projects:
  • Project MESTD

DOI: 10.2298/JSC0202069B

ISSN: 0352-5139

WoS: 000173995100001

Scopus: 2-s2.0-0036003604
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URI
http://cer.ihtm.bg.ac.rs/handle/123456789/60
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