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Synthesis of calcium doped phosphate tungsten bronze

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2018
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Authors
Maksimović, Tijana
Maksimović, Jelena
Stojadinović, Stevan
Tančić, Pavle
Nedić, Zoran
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Abstract
A study is presented of phase transitions of acid CaHPW12O40∙6H2O salt of 12-tungstophosphoric acid and characterized in the temperature range from room temperature to 1093 K. The structure and its phase transformations were characterized by thermal analysis (TGA and DSC), X-ray powder diffraction (XRPD) and Fourier-transform infrared spectra (FTIR). Dehydration processes are finished at about 770 K. Keggin’s anions are transformed by solid-solid recrystallization at about 873 K in calcium doped phosphate tungsten bronze.
Keywords:
phase transitions / thermal analysis / X-ray powder diffraction (XRPD) / Fourier-transform infrared spectra (FTIR)
Source:
Proceedings - 14th International Conference on Fundamental and Applied aspects of Physical Chemistry - Physical Chemistry 2018, September 24-28, 2018 Belgrade, Serbia, 2018, 2, 673-676
Publisher:
  • Society of Physical Chemists of Serbia
Funding / projects:
  • Lithium-ion batteries and fuel cells - research and development (RS-45014)
  • Nanostructured Functional and Composite Materials in Catalytic and Sorption Processes (RS-45001)
  • Dynamics of nonlinear physicochemical and biochemical systems with modeling and predicting of their behavior under nonequilibrium conditions (RS-172015)

ISBN: 978-86-82475-37-8

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_cer_5977
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/5977
Collections
  • Radovi istraživača pre dolaska u IHTM / Researchers' papers before joining ICTM
Institution/Community
IHTM
TY  - CONF
AU  - Maksimović, Tijana
AU  - Maksimović, Jelena
AU  - Stojadinović, Stevan
AU  - Tančić, Pavle
AU  - Nedić, Zoran
PY  - 2018
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/5977
AB  - A study is presented of phase transitions of acid CaHPW12O40∙6H2O salt of 12-tungstophosphoric acid and characterized in the temperature range from room temperature to 1093 K. The structure and its phase transformations were characterized by thermal analysis (TGA and DSC), X-ray powder diffraction (XRPD) and Fourier-transform infrared spectra (FTIR). 
Dehydration processes are finished at about 770 K. Keggin’s anions are transformed by solid-solid recrystallization at about 873 K in calcium doped phosphate tungsten bronze.
PB  - Society of Physical Chemists of Serbia
C3  - Proceedings - 14th International Conference on Fundamental and Applied aspects of Physical Chemistry - Physical Chemistry 2018, September 24-28, 2018 Belgrade, Serbia
T1  - Synthesis of calcium doped phosphate tungsten bronze
VL  - 2
SP  - 673
EP  - 676
UR  - https://hdl.handle.net/21.15107/rcub_cer_5977
ER  - 
@conference{
author = "Maksimović, Tijana and Maksimović, Jelena and Stojadinović, Stevan and Tančić, Pavle and Nedić, Zoran",
year = "2018",
abstract = "A study is presented of phase transitions of acid CaHPW12O40∙6H2O salt of 12-tungstophosphoric acid and characterized in the temperature range from room temperature to 1093 K. The structure and its phase transformations were characterized by thermal analysis (TGA and DSC), X-ray powder diffraction (XRPD) and Fourier-transform infrared spectra (FTIR). 
Dehydration processes are finished at about 770 K. Keggin’s anions are transformed by solid-solid recrystallization at about 873 K in calcium doped phosphate tungsten bronze.",
publisher = "Society of Physical Chemists of Serbia",
journal = "Proceedings - 14th International Conference on Fundamental and Applied aspects of Physical Chemistry - Physical Chemistry 2018, September 24-28, 2018 Belgrade, Serbia",
title = "Synthesis of calcium doped phosphate tungsten bronze",
volume = "2",
pages = "673-676",
url = "https://hdl.handle.net/21.15107/rcub_cer_5977"
}
Maksimović, T., Maksimović, J., Stojadinović, S., Tančić, P.,& Nedić, Z.. (2018). Synthesis of calcium doped phosphate tungsten bronze. in Proceedings - 14th International Conference on Fundamental and Applied aspects of Physical Chemistry - Physical Chemistry 2018, September 24-28, 2018 Belgrade, Serbia
Society of Physical Chemists of Serbia., 2, 673-676.
https://hdl.handle.net/21.15107/rcub_cer_5977
Maksimović T, Maksimović J, Stojadinović S, Tančić P, Nedić Z. Synthesis of calcium doped phosphate tungsten bronze. in Proceedings - 14th International Conference on Fundamental and Applied aspects of Physical Chemistry - Physical Chemistry 2018, September 24-28, 2018 Belgrade, Serbia. 2018;2:673-676.
https://hdl.handle.net/21.15107/rcub_cer_5977 .
Maksimović, Tijana, Maksimović, Jelena, Stojadinović, Stevan, Tančić, Pavle, Nedić, Zoran, "Synthesis of calcium doped phosphate tungsten bronze" in Proceedings - 14th International Conference on Fundamental and Applied aspects of Physical Chemistry - Physical Chemistry 2018, September 24-28, 2018 Belgrade, Serbia, 2 (2018):673-676,
https://hdl.handle.net/21.15107/rcub_cer_5977 .

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