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Synthesis and characterization of Ag-loaded hematite nanocomposites

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2021
bitstream_24500.pdf (819.0Kb)
Authors
Vrbica, Boško
Šuljagić, Marija
Jeremić, Dejan
Anđelković, Ljubica
Milenković, Milica R.
Conference object (Published version)
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Abstract
Hematite (α-Fe2O3) nanoparticles have been synthesized by thermal decomposition of iron(III)acetylacetonate precursor. The structure and morphology of the resulting powder were investigated by X-ray powder diffraction (XRPD), Fourier transformation IR (FTIR), scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDS). Hematite-loading with silver was conducted using the reduction of silver nitrate by ascorbic acid realized by three different synthetic procedures – simple reduction process, ultrasonically supported reduction, and reduction after pre-treatment of hematite in Lugol's iodine. All synthesized hematite/silver samples were characterized withSEM, supported by EDS maps. Silver content was determined by Inductively Coupled Plasma Optical Emission spectroscopy (ICP-OES). The development of Ag-doped hematite nanocomposites, hetero-structures containing Ag and magnetic iron oxide,is indispensable in orderto take advantage of Ag containing nanocomposites in... the field of biomedicine.

Source:
Program and the Book of Abstracts, The Nineth Serbian Ceramic Society Conference Advanced Ceramics and Application, September 20-21, 2021, 2021, 53-53
Publisher:
  • Belgrade: Serbian Ceramic Society
Funding / projects:
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200026 (University of Belgrade, Institute of Chemistry, Technology and Metallurgy - IChTM) (RS-200026)
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200168 (University of Belgrade, Faculty of Chemistry) (RS-200168)
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200288 (Innovation Center of the Faculty of Chemistry) (RS-200288)

ISBN: 978-86-915627-8-6

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_cer_5911
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/5911
Collections
  • Radovi istraživača / Researchers' publications
Institution/Community
IHTM
TY  - CONF
AU  - Vrbica, Boško
AU  - Šuljagić, Marija
AU  - Jeremić, Dejan
AU  - Anđelković, Ljubica
AU  - Milenković, Milica R.
PY  - 2021
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/5911
AB  - Hematite (α-Fe2O3) nanoparticles have been synthesized by thermal decomposition of iron(III)acetylacetonate precursor. The structure and morphology of the resulting powder  were investigated by X-ray powder diffraction (XRPD), Fourier transformation IR (FTIR),  scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDS). Hematite-loading with silver was conducted using the reduction of silver nitrate by ascorbic acid realized by three different synthetic procedures – simple reduction process, ultrasonically supported reduction, and reduction after pre-treatment of hematite in Lugol's iodine. All synthesized hematite/silver samples were characterized withSEM, supported by EDS maps. Silver content was determined by Inductively Coupled Plasma Optical Emission spectroscopy (ICP-OES). The development of Ag-doped hematite nanocomposites, hetero-structures containing Ag and magnetic iron oxide,is indispensable in orderto take advantage of Ag containing nanocomposites in the field of biomedicine.
PB  - Belgrade: Serbian Ceramic Society
C3  - Program and the Book of Abstracts, The Nineth Serbian Ceramic Society Conference Advanced Ceramics and Application, September 20-21, 2021
T1  - Synthesis and characterization of Ag-loaded hematite nanocomposites
SP  - 53
EP  - 53
UR  - https://hdl.handle.net/21.15107/rcub_cer_5911
ER  - 
@conference{
author = "Vrbica, Boško and Šuljagić, Marija and Jeremić, Dejan and Anđelković, Ljubica and Milenković, Milica R.",
year = "2021",
abstract = "Hematite (α-Fe2O3) nanoparticles have been synthesized by thermal decomposition of iron(III)acetylacetonate precursor. The structure and morphology of the resulting powder  were investigated by X-ray powder diffraction (XRPD), Fourier transformation IR (FTIR),  scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDS). Hematite-loading with silver was conducted using the reduction of silver nitrate by ascorbic acid realized by three different synthetic procedures – simple reduction process, ultrasonically supported reduction, and reduction after pre-treatment of hematite in Lugol's iodine. All synthesized hematite/silver samples were characterized withSEM, supported by EDS maps. Silver content was determined by Inductively Coupled Plasma Optical Emission spectroscopy (ICP-OES). The development of Ag-doped hematite nanocomposites, hetero-structures containing Ag and magnetic iron oxide,is indispensable in orderto take advantage of Ag containing nanocomposites in the field of biomedicine.",
publisher = "Belgrade: Serbian Ceramic Society",
journal = "Program and the Book of Abstracts, The Nineth Serbian Ceramic Society Conference Advanced Ceramics and Application, September 20-21, 2021",
title = "Synthesis and characterization of Ag-loaded hematite nanocomposites",
pages = "53-53",
url = "https://hdl.handle.net/21.15107/rcub_cer_5911"
}
Vrbica, B., Šuljagić, M., Jeremić, D., Anđelković, L.,& Milenković, M. R.. (2021). Synthesis and characterization of Ag-loaded hematite nanocomposites. in Program and the Book of Abstracts, The Nineth Serbian Ceramic Society Conference Advanced Ceramics and Application, September 20-21, 2021
Belgrade: Serbian Ceramic Society., 53-53.
https://hdl.handle.net/21.15107/rcub_cer_5911
Vrbica B, Šuljagić M, Jeremić D, Anđelković L, Milenković MR. Synthesis and characterization of Ag-loaded hematite nanocomposites. in Program and the Book of Abstracts, The Nineth Serbian Ceramic Society Conference Advanced Ceramics and Application, September 20-21, 2021. 2021;:53-53.
https://hdl.handle.net/21.15107/rcub_cer_5911 .
Vrbica, Boško, Šuljagić, Marija, Jeremić, Dejan, Anđelković, Ljubica, Milenković, Milica R., "Synthesis and characterization of Ag-loaded hematite nanocomposites" in Program and the Book of Abstracts, The Nineth Serbian Ceramic Society Conference Advanced Ceramics and Application, September 20-21, 2021 (2021):53-53,
https://hdl.handle.net/21.15107/rcub_cer_5911 .

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