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dc.creatorPopa, A.
dc.creatorHolclajtner-Antunovic, I.
dc.creatorVasiljević-Radović, Dana
dc.creatorSasca, V.
dc.date.accessioned2019-01-30T17:19:45Z
dc.date.available2019-01-30T17:19:45Z
dc.date.issued2009
dc.identifier.issn1454-4164
dc.identifier.urihttps://cer.ihtm.bg.ac.rs/handle/123456789/511
dc.description.abstractHeteropolyacids (HPAS) H(3)PMo(12)O(40) (HPM) and H(4)PVMo(11)O(40) (HPVM) supported on mesoporous pure-silica and Al, Fe modified molecular sieve MCM-41 and SBA-15 have been prepared and characterized by atomic force microscopy (AFM) and scanning electron microscopy (SEM) with EDS. All supported HPAs were prepared by impregnation using the incipient wetness techniques with a mixture of water: ethanol = 1:1. AFM features show that nanoclusters of HPA-molecular sieves composites of various heights were formed on the surface. The morphology of the pure molecular sieves and HPA-molecular sieves composites surface, respectively, has an island-like structure. SEM studies confirmed the uniformity of the distribution of active phase in the supported samples. It is found that most of HPM and HPVM (active phases) in supported samples are well dispersed on all supports. HPAs supported on MCM-41 ans SBA-15 have still kept their Keggin structure. A relatively uniform distribution of active phase in the supports pores was confirmed by EDS analysis.en
dc.publisherNatl Inst Optoelectronics, Bucharest-Magurele
dc.rightsrestrictedAccess
dc.sourceJournal of Optoelectronics and Advanced Materials
dc.subjectmolecular sievesen
dc.subjectheteropolyacidsen
dc.subjectATMen
dc.subjectSEM-EDSen
dc.titleAFM and SEM-EDS examination of highly dispersed heteropolyacids supported on MCM 41 and SBA 15 mesoporous materialsen
dc.typearticle
dc.rights.licenseARR
dcterms.abstractХолцлајтнер-Aнтуновиц, И.; Васиљевић-Радовић, Дана; Попа, A.; Сасца, В.;
dc.citation.volume11
dc.citation.issue8
dc.citation.spage1185
dc.citation.epage1190
dc.citation.other11(8): 1185-1190
dc.citation.rankM23
dc.identifier.rcubhttps://hdl.handle.net/21.15107/rcub_cer_511
dc.identifier.rcubConv_2466
dc.identifier.scopus2-s2.0-75949097959
dc.identifier.wos000269724200022
dc.type.versionpublishedVersion


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