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Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics

Uticaj vremena sinterovanja na gustinu i SEM analiza kordijeritne keramike

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2021
Djordjevic_9_MKOIEE.pdf (1.059Mb)
Authors
Đorđević, Nataša
Peleš, Adriana
Obradović, Nina
Vlahović, Milica
Mihajlović, Slavica
Martinović, Sanja
Conference object (Published version)
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Abstract
The mechanical activation of the starting mixtures of cordierite (2MgO*2Al2O3*5SiO2) with 5.00 mass % TiO2 was performed in a high energy ball mill during 10-80 min. The applied compaction pressure before the sintering process was 2t/cm2. The sintering process was performed at 1350°C for 2h and 4h in air atmosphere. Scanning electron microscopy was performed to analyze the microstructure of both compacted and sintered samples. Atomic force microscope was used to investigate the surface of the sintered samples. This paper investigates the influence of prolonged sintering time on the densities of the sintered samples, along with electrical properties.
Mehanička aktivacija početnih smeša kordierita (2MgO*2Al2O3*5SiO2) sa 5.00 mas. % TiO2 izvršena je u visokoenergetskom mlinu sa kuglama tokom 10-80 min. Primenjeni pritisak presovanja pre procesa sinterovanja bio je 2 t/cm2. Proces sinterovanja je izveden na 1350 °C tokom 2h i 4h u vazdušnoj atmosferi. Skenirajuća elektronska mikroskopija je izvršena u cilju analize mikrostrukture presovanih i sinterovanih uzoraka. Za ispitivanje površine sinterovanih uzoraka korišćen je mikroskop atomskih sila. Ovaj rad istražuje uticaj produženog vremena sinterovanja na gustinu sinterovanih uzoraka zajedno sa električnim svojstvima.
Keywords:
mechanical activation / density / SEM / cordierite
Source:
Zbornik radova / 9. Međunarodna konferencija o obnovljivim izvorima električne energije, Beograd, 15. oktobar 2021 = Proceedings / 9th International Conference on Renewable Electrical Power Sources, Belgrade, October 15, 2021, 2021, 265-268
Publisher:
  • Beograd : Savez mašinskih i elektrotehničkih inženjera i tehničara Srbije - SMEITS
Funding / projects:
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200023 (Institute of Technology of Nuclear and Other Mineral Row Materials - ITNMS, Belgrade) (RS-200023)
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200026 (University of Belgrade, Institute of Chemistry, Technology and Metallurgy - IChTM) (RS-200026)
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200131 (University of Belgrade, Technical Faculty, Bor) (RS-200131)

ISBN: 978-86-85535-09-3

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_dais_12354
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/4917
Collections
  • Radovi istraživača / Researchers' publications
Institution/Community
IHTM
TY  - CONF
AU  - Đorđević, Nataša
AU  - Peleš, Adriana
AU  - Obradović, Nina
AU  - Vlahović, Milica
AU  - Mihajlović, Slavica
AU  - Martinović, Sanja
PY  - 2021
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/4917
AB  - The mechanical activation of the starting mixtures of cordierite (2MgO*2Al2O3*5SiO2) with 5.00 mass % TiO2 was performed in a high energy ball mill during 10-80 min. The applied compaction pressure before the sintering process was 2t/cm2. The sintering process was performed at 1350°C for 2h and 4h in air atmosphere. Scanning electron microscopy was performed to analyze the microstructure of both compacted and sintered samples. Atomic force microscope was used to investigate the surface of the sintered samples. This paper investigates the influence of prolonged sintering time on the densities of the sintered samples, along with electrical properties.
AB  - Mehanička aktivacija početnih smeša kordierita (2MgO*2Al2O3*5SiO2) sa 5.00 mas. % TiO2 izvršena je u visokoenergetskom mlinu sa kuglama tokom 10-80 min. Primenjeni pritisak presovanja pre procesa sinterovanja bio je 2 t/cm2. Proces sinterovanja je izveden na 1350 °C tokom 2h i 4h u vazdušnoj atmosferi. Skenirajuća elektronska mikroskopija je izvršena u cilju analize mikrostrukture presovanih i sinterovanih uzoraka. Za ispitivanje površine sinterovanih uzoraka korišćen je mikroskop atomskih sila. Ovaj rad istražuje uticaj produženog vremena sinterovanja na gustinu sinterovanih uzoraka zajedno sa električnim svojstvima.
PB  - Beograd : Savez mašinskih i elektrotehničkih inženjera i tehničara Srbije - SMEITS
C3  - Zbornik radova / 9. Međunarodna konferencija o obnovljivim izvorima električne energije, Beograd, 15. oktobar 2021 = Proceedings / 9th International Conference on Renewable Electrical Power Sources, Belgrade, October 15, 2021
T1  - Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics
T1  - Uticaj vremena sinterovanja na gustinu i SEM analiza kordijeritne keramike
SP  - 265
EP  - 268
UR  - https://hdl.handle.net/21.15107/rcub_dais_12354
ER  - 
@conference{
author = "Đorđević, Nataša and Peleš, Adriana and Obradović, Nina and Vlahović, Milica and Mihajlović, Slavica and Martinović, Sanja",
year = "2021",
abstract = "The mechanical activation of the starting mixtures of cordierite (2MgO*2Al2O3*5SiO2) with 5.00 mass % TiO2 was performed in a high energy ball mill during 10-80 min. The applied compaction pressure before the sintering process was 2t/cm2. The sintering process was performed at 1350°C for 2h and 4h in air atmosphere. Scanning electron microscopy was performed to analyze the microstructure of both compacted and sintered samples. Atomic force microscope was used to investigate the surface of the sintered samples. This paper investigates the influence of prolonged sintering time on the densities of the sintered samples, along with electrical properties., Mehanička aktivacija početnih smeša kordierita (2MgO*2Al2O3*5SiO2) sa 5.00 mas. % TiO2 izvršena je u visokoenergetskom mlinu sa kuglama tokom 10-80 min. Primenjeni pritisak presovanja pre procesa sinterovanja bio je 2 t/cm2. Proces sinterovanja je izveden na 1350 °C tokom 2h i 4h u vazdušnoj atmosferi. Skenirajuća elektronska mikroskopija je izvršena u cilju analize mikrostrukture presovanih i sinterovanih uzoraka. Za ispitivanje površine sinterovanih uzoraka korišćen je mikroskop atomskih sila. Ovaj rad istražuje uticaj produženog vremena sinterovanja na gustinu sinterovanih uzoraka zajedno sa električnim svojstvima.",
publisher = "Beograd : Savez mašinskih i elektrotehničkih inženjera i tehničara Srbije - SMEITS",
journal = "Zbornik radova / 9. Međunarodna konferencija o obnovljivim izvorima električne energije, Beograd, 15. oktobar 2021 = Proceedings / 9th International Conference on Renewable Electrical Power Sources, Belgrade, October 15, 2021",
title = "Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics, Uticaj vremena sinterovanja na gustinu i SEM analiza kordijeritne keramike",
pages = "265-268",
url = "https://hdl.handle.net/21.15107/rcub_dais_12354"
}
Đorđević, N., Peleš, A., Obradović, N., Vlahović, M., Mihajlović, S.,& Martinović, S.. (2021). Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics. in Zbornik radova / 9. Međunarodna konferencija o obnovljivim izvorima električne energije, Beograd, 15. oktobar 2021 = Proceedings / 9th International Conference on Renewable Electrical Power Sources, Belgrade, October 15, 2021
Beograd : Savez mašinskih i elektrotehničkih inženjera i tehničara Srbije - SMEITS., 265-268.
https://hdl.handle.net/21.15107/rcub_dais_12354
Đorđević N, Peleš A, Obradović N, Vlahović M, Mihajlović S, Martinović S. Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics. in Zbornik radova / 9. Međunarodna konferencija o obnovljivim izvorima električne energije, Beograd, 15. oktobar 2021 = Proceedings / 9th International Conference on Renewable Electrical Power Sources, Belgrade, October 15, 2021. 2021;:265-268.
https://hdl.handle.net/21.15107/rcub_dais_12354 .
Đorđević, Nataša, Peleš, Adriana, Obradović, Nina, Vlahović, Milica, Mihajlović, Slavica, Martinović, Sanja, "Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics" in Zbornik radova / 9. Međunarodna konferencija o obnovljivim izvorima električne energije, Beograd, 15. oktobar 2021 = Proceedings / 9th International Conference on Renewable Electrical Power Sources, Belgrade, October 15, 2021 (2021):265-268,
https://hdl.handle.net/21.15107/rcub_dais_12354 .

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