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Supplementary material for: "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge"

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2015
gnpl_a_991929_sm9346.pdf (1.025Mb)
Authors
Vlajic, Marina D
Trifunović, Snežana
Simić, Milena R.
Vujisić, Ljubodrag V.
Vučković, Ivan
Novaković, Miroslav
Nikolic-Mandic, Snezana D
Tešević, Vele
Vajs, Vlatka
Milosavljević, Slobodan
Mandić, Boris
Dataset (Published version)
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Abstract
Experimental details relating to the article: Mandić, B., Vlajic, M. D., Trifunović, S., Simić, M. R., Vujisić, L. V., Vučković, I., Novaković, M., Nikolic-Mandic, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. (2015). Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge. Natural Product Research, 29(9), 887-890. https://doi.org/10.1080/14786419.2014.991929. Figure S1. Structures of monitored PAs from R. umbellata (1 - 6). Figure S2. Yields of PAs in relation to days of maceration in the methanol. Figure S3. Yields of PAs extracted with methanol, ethanol and sulphuric acid during four days at dark place and room temperature. Figure S4. Yields of PAs (1-6) in relation to molarity of sulphuric acid used for their extraction. Figure S5. Yields of PAs (1-6) in relation to days of maceration with 1 M sulphuric acid, at room temperature. Figure S6. Yields of PAs (1-6) in relation to days of ultrasonic assisted extraction with 1 M sulphuric acid. Figu...re S7. Yields of PAs (1-6) in relation to days of extraction with 1 M sulphuric acid by overhead rotary mixer. Figure S8. Comparison of yields of PAs (1-6) accomplished after four days of maceration, three days of extraction by ultrasonic bath and overhead rotary mixer assisted extractions of plant material with 1M sulphuric acid. Figure S9. Yields of PAs (1-6) isolated from 1.00 g of the plant material (with 1M sulphuric acid during the extraction by overhead rotary mixer for three days) in relation to the volume (ml) of sulphuric acid. Figure S10. Yields of isolated PAs (1-6) in relation to pH values of aqueous solutions for alkaline extraction of PAs with CH2Cl2. Figure S11. Yields of isolated PAs in relation to the number of continuous alkaline re-extractions with CH2Cl2 at pH 9.

Keywords:
isolation / GC-MS / pyrrolizidine alkaloids / Rindera umellata Bunge
Source:
Natural Product Research, 2015
Publisher:
  • Taylor & Francis
Funding / projects:
  • Natural products of wild, cultivated and edible plants: structure and bioactivity determination (RS-172053)
Note:
  • This is the supplementary material for: Mandić, B., Vlajic, M. D., Trifunović, S., Simić, M. R., Vujisić, L. V., Vučković, I., Novaković, M., Nikolic-Mandic, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. (2015). Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge. Natural Product Research, Taylor & Francis, 29(9), 887-890. https://doi.org/10.1080/14786419.2014.991929
  • Published version of the article: https://cer.ihtm.bg.ac.rs/handle/123456789/1780
Related info:
  • Referenced by
    https://doi.org/10.1080/14786419.2014.991929
  • Referenced by
    https://cer.ihtm.bg.ac.rs/handle/123456789/1780

DOI: 10.6084/m9.figshare.1276004.v2

[ Google Scholar ]
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/4466
Collections
  • Istraživački podaci / Research data
Institution/Community
IHTM
TY  - DATA
AU  - Vlajic, Marina D
AU  - Trifunović, Snežana
AU  - Simić, Milena R.
AU  - Vujisić, Ljubodrag V.
AU  - Vučković, Ivan
AU  - Novaković, Miroslav
AU  - Nikolic-Mandic, Snezana D
AU  - Tešević, Vele
AU  - Vajs, Vlatka
AU  - Milosavljević, Slobodan
AU  - Mandić, Boris
PY  - 2015
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/4466
AB  - Experimental details relating to the article: Mandić, B., Vlajic, M. D., Trifunović, S., Simić, M. R., Vujisić, L. V., Vučković, I., Novaković, M., Nikolic-Mandic, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. (2015). Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge. Natural Product Research, 29(9), 887-890. https://doi.org/10.1080/14786419.2014.991929. Figure S1. Structures of monitored PAs from R. umbellata (1 - 6). Figure S2. Yields of PAs in relation to days of maceration in the methanol. Figure S3. Yields of PAs extracted with methanol, ethanol and sulphuric acid during four days at dark place and room temperature. Figure S4. Yields of PAs (1-6) in relation to molarity of sulphuric acid used for their extraction. Figure S5. Yields of PAs (1-6) in relation to days of maceration with 1 M sulphuric acid, at room temperature. Figure S6. Yields of PAs (1-6) in relation to days of ultrasonic assisted extraction with 1 M sulphuric acid. Figure S7. Yields of PAs (1-6) in relation to days of extraction with 1 M sulphuric acid by overhead rotary mixer.  Figure S8. Comparison of yields of PAs (1-6) accomplished after four days of maceration, three days of extraction by ultrasonic bath and overhead rotary mixer assisted extractions of plant material with 1M sulphuric acid. Figure S9. Yields of PAs (1-6) isolated from 1.00 g of the plant material (with 1M sulphuric acid during the extraction by overhead rotary mixer for three days) in relation to the volume (ml) of sulphuric acid. Figure S10. Yields of isolated PAs (1-6) in relation to pH values of aqueous solutions for alkaline extraction of PAs with CH2Cl2. Figure S11. Yields of isolated PAs in relation to the number of continuous alkaline re-extractions with CH2Cl2 at pH 9.
PB  - Taylor & Francis
T2  - Natural Product Research
T1  - Supplementary material for: "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge"
DO  - 10.6084/m9.figshare.1276004.v2
ER  - 
@misc{
author = "Vlajic, Marina D and Trifunović, Snežana and Simić, Milena R. and Vujisić, Ljubodrag V. and Vučković, Ivan and Novaković, Miroslav and Nikolic-Mandic, Snezana D and Tešević, Vele and Vajs, Vlatka and Milosavljević, Slobodan and Mandić, Boris",
year = "2015",
abstract = "Experimental details relating to the article: Mandić, B., Vlajic, M. D., Trifunović, S., Simić, M. R., Vujisić, L. V., Vučković, I., Novaković, M., Nikolic-Mandic, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. (2015). Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge. Natural Product Research, 29(9), 887-890. https://doi.org/10.1080/14786419.2014.991929. Figure S1. Structures of monitored PAs from R. umbellata (1 - 6). Figure S2. Yields of PAs in relation to days of maceration in the methanol. Figure S3. Yields of PAs extracted with methanol, ethanol and sulphuric acid during four days at dark place and room temperature. Figure S4. Yields of PAs (1-6) in relation to molarity of sulphuric acid used for their extraction. Figure S5. Yields of PAs (1-6) in relation to days of maceration with 1 M sulphuric acid, at room temperature. Figure S6. Yields of PAs (1-6) in relation to days of ultrasonic assisted extraction with 1 M sulphuric acid. Figure S7. Yields of PAs (1-6) in relation to days of extraction with 1 M sulphuric acid by overhead rotary mixer.  Figure S8. Comparison of yields of PAs (1-6) accomplished after four days of maceration, three days of extraction by ultrasonic bath and overhead rotary mixer assisted extractions of plant material with 1M sulphuric acid. Figure S9. Yields of PAs (1-6) isolated from 1.00 g of the plant material (with 1M sulphuric acid during the extraction by overhead rotary mixer for three days) in relation to the volume (ml) of sulphuric acid. Figure S10. Yields of isolated PAs (1-6) in relation to pH values of aqueous solutions for alkaline extraction of PAs with CH2Cl2. Figure S11. Yields of isolated PAs in relation to the number of continuous alkaline re-extractions with CH2Cl2 at pH 9.",
publisher = "Taylor & Francis",
journal = "Natural Product Research",
title = "Supplementary material for: "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge"",
doi = "10.6084/m9.figshare.1276004.v2"
}
Vlajic, M. D., Trifunović, S., Simić, M. R., Vujisić, L. V., Vučković, I., Novaković, M., Nikolic-Mandic, S. D., Tešević, V., Vajs, V., Milosavljević, S.,& Mandić, B.. (2015). Supplementary material for: "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge". in Natural Product Research
Taylor & Francis..
https://doi.org/10.6084/m9.figshare.1276004.v2
Vlajic MD, Trifunović S, Simić MR, Vujisić LV, Vučković I, Novaković M, Nikolic-Mandic SD, Tešević V, Vajs V, Milosavljević S, Mandić B. Supplementary material for: "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge". in Natural Product Research. 2015;.
doi:10.6084/m9.figshare.1276004.v2 .
Vlajic, Marina D, Trifunović, Snežana, Simić, Milena R., Vujisić, Ljubodrag V., Vučković, Ivan, Novaković, Miroslav, Nikolic-Mandic, Snezana D, Tešević, Vele, Vajs, Vlatka, Milosavljević, Slobodan, Mandić, Boris, "Supplementary material for: "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge"" in Natural Product Research (2015),
https://doi.org/10.6084/m9.figshare.1276004.v2 . .

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