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Experimental investigation and thermodynamic calculations of the Bi-Ni-Pb phase diagram

Eksperimentalno ispitivanje i termodinamička analiza Bi-Ni-Pb faznog dijagrama

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2019
1450-53391900024M.pdf (2.151Mb)
Authors
Minić, D.
Premović, Milena
Tošković, N.
Manasijević, Dragan
Ćosović, Vladan
Janaćković, M.
Tomović, Milica
Article (Published version)
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Abstract
The article presents an experimental study of a phase diagram of a ternary Bi-Ni-Pb system using differential thermal analysis (DTA), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS), and X-ray powder diffraction (XRD) analysis. The investigated ternary alloys were selected from three vertical sections (x(Bi)=0.75, x(Ni)=0.1 and x(Pb)=0.9) and two isothermal sections at 100 and at 300°C. The obtained experimental results were compared with the thermodynamically extrapolated phase diagram of the Bi-Ni-Pb ternary system based on the thermodynamic parameters for the constitutive binary systems available in literature. Reasonably close agreement between the experimental data and the calculated phase diagram was obtained.
U ovom radu je predstavljeno eksperimentalno ispitivanje faznog dijagrama Bi-Ni-Pb ternarnog sistema uz pomoć diferencijalne termijske analize (DTA), skenirajućeg elektronskog mikroskopa (SEM) sa energijsko disperzivno spektrometrijom (EDS) i rentgenskom difrakcijom praha (XRD). Ispitivane ternarne legure su izabrane iz tri vertikalna preseka (x(Bi)=0.75, x(Ni)=0.1 i x(Pb)=0.9), i dva izotermalna preseka na 100 i 300°C. Rezultati eksperimenta su upoređeni sa termodinamički ekstrapolisanim faznim dijagramom Bi-Ni-Pb ternarnog sistema na osnovu termodinamičkih parametara sastavnih binarnih sistema koji su dostupni u literaturi. Utvrđeno je dobro slaganje između eksperimentalnih rezultata i proračunatog faznog dijagrama.
Keywords:
Bi–Ni-Pb system / Vertical sections x(Bi)=0.75, x(Ni)=0.1 and x(Pb)=0.9 / Isothermal sections at 100 and at 300 °C / Thermal analysis / Thermodynamic prediction / Vertikalni preseci (x(Bi)=0.75, x(Ni)=0.1 i x(Pb)=0.9) / Izoterermalni preseci na 100 i 300°C / Termijska analiza / Termodinamičko predviđanje
Source:
Journal of Mining and Metallurgy, Section B: Metallurgy, 2019, 55, 2, 157-166
Publisher:
  • Beograd : Univerzitet u Beogradu - Tehnički fakultet u Boru
Funding / projects:
  • Advanced multicomponent metal systems and nanostructured materials with diverse functional properties (RS-172037)
  • Advanced multicomponent metal systems and nanostructured materials with diverse functional properties (RS-172037)

DOI: 10.2298/JMMB181128024M

ISSN: 1450-5339; 2217-7175

WoS: 000473285100003

Scopus: 2-s2.0-85069494972
[ Google Scholar ]
1
1
URI
https://cer.ihtm.bg.ac.rs/handle/123456789/3210
Collections
  • Radovi istraživača / Researchers' publications
Institution/Community
IHTM
TY  - JOUR
AU  - Minić, D.
AU  - Premović, Milena
AU  - Tošković, N.
AU  - Manasijević, Dragan
AU  - Ćosović, Vladan
AU  - Janaćković, M.
AU  - Tomović, Milica
PY  - 2019
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/3210
AB  - The article presents an experimental study of a phase diagram of a ternary Bi-Ni-Pb system using differential thermal analysis (DTA), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS), and X-ray powder diffraction (XRD) analysis. The investigated ternary alloys were selected from three vertical sections (x(Bi)=0.75, x(Ni)=0.1 and x(Pb)=0.9) and two isothermal sections at 100 and at 300°C. The obtained experimental results were compared with the thermodynamically extrapolated phase diagram of the Bi-Ni-Pb ternary system based on the thermodynamic parameters for the constitutive binary systems available in literature. Reasonably close agreement between the experimental data and the calculated phase diagram was obtained.
AB  - U ovom radu je predstavljeno eksperimentalno ispitivanje faznog dijagrama Bi-Ni-Pb ternarnog sistema uz pomoć diferencijalne termijske analize (DTA), skenirajućeg elektronskog mikroskopa (SEM) sa energijsko disperzivno spektrometrijom (EDS) i rentgenskom difrakcijom praha (XRD). Ispitivane ternarne legure su izabrane iz tri vertikalna preseka (x(Bi)=0.75, x(Ni)=0.1 i x(Pb)=0.9), i dva izotermalna preseka na 100 i 300°C. Rezultati eksperimenta su upoređeni sa termodinamički ekstrapolisanim faznim dijagramom Bi-Ni-Pb ternarnog sistema na osnovu termodinamičkih parametara sastavnih binarnih sistema koji su dostupni u literaturi. Utvrđeno je dobro slaganje između eksperimentalnih rezultata i proračunatog faznog dijagrama.
PB  - Beograd : Univerzitet u Beogradu - Tehnički fakultet u Boru
T2  - Journal of Mining and Metallurgy, Section B: Metallurgy
T1  - Experimental investigation and thermodynamic calculations of the Bi-Ni-Pb phase diagram
T1  - Eksperimentalno ispitivanje i termodinamička analiza Bi-Ni-Pb faznog dijagrama
VL  - 55
IS  - 2
SP  - 157
EP  - 166
DO  - 10.2298/JMMB181128024M
ER  - 
@article{
author = "Minić, D. and Premović, Milena and Tošković, N. and Manasijević, Dragan and Ćosović, Vladan and Janaćković, M. and Tomović, Milica",
year = "2019",
abstract = "The article presents an experimental study of a phase diagram of a ternary Bi-Ni-Pb system using differential thermal analysis (DTA), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS), and X-ray powder diffraction (XRD) analysis. The investigated ternary alloys were selected from three vertical sections (x(Bi)=0.75, x(Ni)=0.1 and x(Pb)=0.9) and two isothermal sections at 100 and at 300°C. The obtained experimental results were compared with the thermodynamically extrapolated phase diagram of the Bi-Ni-Pb ternary system based on the thermodynamic parameters for the constitutive binary systems available in literature. Reasonably close agreement between the experimental data and the calculated phase diagram was obtained., U ovom radu je predstavljeno eksperimentalno ispitivanje faznog dijagrama Bi-Ni-Pb ternarnog sistema uz pomoć diferencijalne termijske analize (DTA), skenirajućeg elektronskog mikroskopa (SEM) sa energijsko disperzivno spektrometrijom (EDS) i rentgenskom difrakcijom praha (XRD). Ispitivane ternarne legure su izabrane iz tri vertikalna preseka (x(Bi)=0.75, x(Ni)=0.1 i x(Pb)=0.9), i dva izotermalna preseka na 100 i 300°C. Rezultati eksperimenta su upoređeni sa termodinamički ekstrapolisanim faznim dijagramom Bi-Ni-Pb ternarnog sistema na osnovu termodinamičkih parametara sastavnih binarnih sistema koji su dostupni u literaturi. Utvrđeno je dobro slaganje između eksperimentalnih rezultata i proračunatog faznog dijagrama.",
publisher = "Beograd : Univerzitet u Beogradu - Tehnički fakultet u Boru",
journal = "Journal of Mining and Metallurgy, Section B: Metallurgy",
title = "Experimental investigation and thermodynamic calculations of the Bi-Ni-Pb phase diagram, Eksperimentalno ispitivanje i termodinamička analiza Bi-Ni-Pb faznog dijagrama",
volume = "55",
number = "2",
pages = "157-166",
doi = "10.2298/JMMB181128024M"
}
Minić, D., Premović, M., Tošković, N., Manasijević, D., Ćosović, V., Janaćković, M.,& Tomović, M.. (2019). Experimental investigation and thermodynamic calculations of the Bi-Ni-Pb phase diagram. in Journal of Mining and Metallurgy, Section B: Metallurgy
Beograd : Univerzitet u Beogradu - Tehnički fakultet u Boru., 55(2), 157-166.
https://doi.org/10.2298/JMMB181128024M
Minić D, Premović M, Tošković N, Manasijević D, Ćosović V, Janaćković M, Tomović M. Experimental investigation and thermodynamic calculations of the Bi-Ni-Pb phase diagram. in Journal of Mining and Metallurgy, Section B: Metallurgy. 2019;55(2):157-166.
doi:10.2298/JMMB181128024M .
Minić, D., Premović, Milena, Tošković, N., Manasijević, Dragan, Ćosović, Vladan, Janaćković, M., Tomović, Milica, "Experimental investigation and thermodynamic calculations of the Bi-Ni-Pb phase diagram" in Journal of Mining and Metallurgy, Section B: Metallurgy, 55, no. 2 (2019):157-166,
https://doi.org/10.2298/JMMB181128024M . .

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