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dc.creatorPeleš, Adriana
dc.creatorPavlović, Vera P.
dc.creatorFilipović, Suzana
dc.creatorObradovic, Nina
dc.creatorMančić, Lidija
dc.creatorKrstić, Jugoslav
dc.creatorMitrić, Miodrag
dc.creatorVlahovic, B
dc.creatorRasic, G
dc.creatorKosanovic, D
dc.creatorPavlović, Vladimir B.
dc.date.accessioned2019-11-14T10:17:43Z
dc.date.available2017-07-08
dc.date.issued2015
dc.identifier.issn0925-8388
dc.identifier.urihttp://cer.ihtm.bg.ac.rs/handle/123456789/3208
dc.description.abstractCommercially available ZnO powder was mechanically activated in a planetary ball mill. In order to investigate the specific surface area, pore volume and microstructure of non-activated and mechanically activated ZnO powders the authors performed N-2 physisorption, SEM and TEM. Crystallite size and lattice microstrain were analyzed by X-ray diffraction method. XRD patterns indicate that peak intensities are getting lower and expend with activation time. The reduction in crystallite size and increasing of lattice microstrain with prolonged milling time were determined applying the Rietveld's method. The difference between non-activated and the activated powder has been also observed by X-ray photoelectron spectroscopy (XPS). XPS is used for investigating the chemical bonding of ZnO powder by analyzing the energy of photoelectrons. The lattice vibration spectra were obtained using Raman spectroscopy. In Raman spectra some changes along with atypical resonant scattering were noticed, which were caused by mechanical activation.en
dc.publisherElsevier
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172057/RS//
dc.relationNSF CREST - HRD-0833184
dc.relationNASA - NNX09AV07A
dc.relationSerbian Academy of Science and Arts - F/198
dc.rightsembargoedAccess
dc.sourceJournal of Alloys and Compounds
dc.subjectmechanical activationen
dc.subjectN-2 physisorptionen
dc.subjectXRDen
dc.subjectXPSen
dc.subjectSEMen
dc.subjectTEMen
dc.subjectRaman spectroscopyen
dc.subjectZnOen
dc.titleStructural investigation of mechanically activated ZnO powderen
dc.typearticle
dc.rights.licenseBY-NC-ND
dcterms.abstractПавловић, Вера П.; Пелеш, Aдриана; Обрадовиц, Нина; Влаховиц, Б; Крстић, Југослав; Расиц, Г; Косановиц, Д; Митрић, Миодраг; Павловић, Владимир Б.; Манчић, Лидија; Филиповић, Сузана;
dc.citation.volume648
dc.citation.spage971
dc.citation.epage979
dc.citation.other648: 971-979
dc.citation.rankaM21
dc.description.otherThis is peer-reviewed version of the artcle: A. Peleš, V.P. Pavlović, S. Filipović, N. Obradović, L. Mančić, J. Krstić, M. Mitrić, B. Vlahović, G. Rašić, D. Kosanović, V.B. Pavlović, Structural investigation of mechanically activated ZnO powder, J. Alloys Compd. 648 (2015) 971–979 [https://doi.org/10.1016/j.jallcom.2015.06.247]
dc.description.otherPublished version: [http://cer.ihtm.bg.ac.rs/handle/123456789/1715]
dc.identifier.doi10.1016/j.jallcom.2015.06.247
dc.identifier.rcubConv_3413
dc.identifier.fulltexthttp://cer.ihtm.bg.ac.rs/bitstream/id/15406/pele2015.pdf
dc.identifier.scopus2-s2.0-84937238971
dc.identifier.wos000361158300139
dc.type.versionacceptedVersion


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