Crystal Structure and Solid State Conformation of 5‐Hydroxy‐8,9‐Dioxo‐8,9‐Seco‐α‐Cholestan‐3β‐yl Acetate
Samo za registrovane korisnike
1993
Autori
Tinant, BernardDeclercq, J P
Dabović, Milan
Krstić, Natalija
Lorenc, Ljubinka
Mihailović, Milhailo Lj.
Članak u časopisu (Objavljena verzija)
,
Elsevier B.V.
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
The molecular structure of the title compound, which might be a possible intermediate in the synthesis of 5,10:8,9‐diseco‐steroids (=steroklastanes), was determined by X‐ray analysis. Hydrogen bonding between the 5α‐hydroxyl group and the 9‐oxo function attached to the ten‐membered ring, and the presence of two conformational forms of the side‐chain in the solid state structure of 2 are established. Copyright © 1993 Wiley‐VCH Verlag GmbH & Co. KGaA, Weinheim
Izvor:
Bulletin des Sociétés Chimiques Belges, 1993, 102, 8, 539-544Izdavač:
- Comltb van Beheer van het Bulletin V.Z.W.
Finansiranje / projekti:
- F.N.R.S. Belgium
- Serbian Academy of Sciences and Arts
- Serbian Research Fund
Institucija/grupa
IHTMTY - JOUR AU - Tinant, Bernard AU - Declercq, J P AU - Dabović, Milan AU - Krstić, Natalija AU - Lorenc, Ljubinka AU - Mihailović, Milhailo Lj. PY - 1993 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/2704 AB - The molecular structure of the title compound, which might be a possible intermediate in the synthesis of 5,10:8,9‐diseco‐steroids (=steroklastanes), was determined by X‐ray analysis. Hydrogen bonding between the 5α‐hydroxyl group and the 9‐oxo function attached to the ten‐membered ring, and the presence of two conformational forms of the side‐chain in the solid state structure of 2 are established. Copyright © 1993 Wiley‐VCH Verlag GmbH & Co. KGaA, Weinheim PB - Comltb van Beheer van het Bulletin V.Z.W. T2 - Bulletin des Sociétés Chimiques Belges T1 - Crystal Structure and Solid State Conformation of 5‐Hydroxy‐8,9‐Dioxo‐8,9‐Seco‐α‐Cholestan‐3β‐yl Acetate VL - 102 IS - 8 SP - 539 EP - 544 DO - 10.1002/bscb.19931020806 ER -
@article{ author = "Tinant, Bernard and Declercq, J P and Dabović, Milan and Krstić, Natalija and Lorenc, Ljubinka and Mihailović, Milhailo Lj.", year = "1993", abstract = "The molecular structure of the title compound, which might be a possible intermediate in the synthesis of 5,10:8,9‐diseco‐steroids (=steroklastanes), was determined by X‐ray analysis. Hydrogen bonding between the 5α‐hydroxyl group and the 9‐oxo function attached to the ten‐membered ring, and the presence of two conformational forms of the side‐chain in the solid state structure of 2 are established. Copyright © 1993 Wiley‐VCH Verlag GmbH & Co. KGaA, Weinheim", publisher = "Comltb van Beheer van het Bulletin V.Z.W.", journal = "Bulletin des Sociétés Chimiques Belges", title = "Crystal Structure and Solid State Conformation of 5‐Hydroxy‐8,9‐Dioxo‐8,9‐Seco‐α‐Cholestan‐3β‐yl Acetate", volume = "102", number = "8", pages = "539-544", doi = "10.1002/bscb.19931020806" }
Tinant, B., Declercq, J. P., Dabović, M., Krstić, N., Lorenc, L.,& Mihailović, M. Lj.. (1993). Crystal Structure and Solid State Conformation of 5‐Hydroxy‐8,9‐Dioxo‐8,9‐Seco‐α‐Cholestan‐3β‐yl Acetate. in Bulletin des Sociétés Chimiques Belges Comltb van Beheer van het Bulletin V.Z.W.., 102(8), 539-544. https://doi.org/10.1002/bscb.19931020806
Tinant B, Declercq JP, Dabović M, Krstić N, Lorenc L, Mihailović ML. Crystal Structure and Solid State Conformation of 5‐Hydroxy‐8,9‐Dioxo‐8,9‐Seco‐α‐Cholestan‐3β‐yl Acetate. in Bulletin des Sociétés Chimiques Belges. 1993;102(8):539-544. doi:10.1002/bscb.19931020806 .
Tinant, Bernard, Declercq, J P, Dabović, Milan, Krstić, Natalija, Lorenc, Ljubinka, Mihailović, Milhailo Lj., "Crystal Structure and Solid State Conformation of 5‐Hydroxy‐8,9‐Dioxo‐8,9‐Seco‐α‐Cholestan‐3β‐yl Acetate" in Bulletin des Sociétés Chimiques Belges, 102, no. 8 (1993):539-544, https://doi.org/10.1002/bscb.19931020806 . .