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dc.creatorPetrović, Srđan
dc.creatorRožić, Ljiljana
dc.creatorJović, Vesna
dc.creatorStojadinović, Stevan
dc.creatorGrbić, Boško
dc.creatorRadić, Nenad
dc.creatorLamovec, Jelena
dc.creatorVasilić, Rastko
dc.date.accessioned2019-01-30T18:00:50Z
dc.date.available2019-01-30T18:00:50Z
dc.date.issued2018
dc.identifier.issn0921-8831
dc.identifier.urihttps://cer.ihtm.bg.ac.rs/handle/123456789/2454
dc.description.abstractNanocrystalline TiO2-CeO2 powders were synthesized from their TiO2 and CeO2 oxides using mechanical ball milling process. The response surface method is applied to identify optimal parameters for the synthesis of TiO2-CeO2 photocatalyst. Analysis of variance and main effect plot are used to determine the significant parameters and set the optimal level for each parameter. Regression analysis showed good agreement of experimental data with the second-order polynomial model with a coefficients of determination: R-2 = 0.991, R-Adj(2). = 0.940 and R-Pred(2). = 0.983. Under optimal experimental conditions of TiO2:CeO2 weight percentage ratio 71: 29, milling speed 200 rpm, and milling time 115 min the highest photodegradation efficiency was achieved. On the basis of the above statistical analysis, it was found that the band gap energy of TiO2-CeO2 nanoparticles decreases with the increase of the milling speed and milling time with constant TiO2:CeO2 weight percentage ratio. Obtained results suggest that mechanical ball milling process is a rapid, efficient and low energy consumption method to synthesize TiO2-CeO2 photocatalyst.en
dc.publisherElsevier
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172015/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172001/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172022/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172035/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172026/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/Technological Development (TD or TR)/32008/RS//
dc.rightsrestrictedAccess
dc.sourceAdvanced Powder Technology
dc.subjectTiO2-CeO(2)nanopowderen
dc.subjectPlanetary ball millingen
dc.subjectResponse surface methodologyen
dc.subjectPhotocatalytic degradationen
dc.titleOptimization of a nanoparticle ball milling process parameters using the response surface methoden
dc.typearticle
dc.rights.licenseARR
dcterms.abstractГрбић, Бошко; Стојадиновиц, Стеван; Василиц, Растко; Рожић, Љиљана; Радић, Ненад; Ламовец, Јелена; Јовић, Весна; Петровић, Срђан;
dc.citation.volume29
dc.citation.issue9
dc.citation.spage2129
dc.citation.epage2139
dc.citation.other29(9): 2129-2139
dc.citation.rankM21
dc.identifier.doi10.1016/j.apt.2018.05.021
dc.identifier.scopus2-s2.0-85047783874
dc.identifier.wos000437308300018
dc.type.versionpublishedVersion


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