Synthesis of fluorapatite nanopowders by a surfactant-assisted microwave method under isothermal conditions

2018
Authors
Stanić, Vojislav Dj.
Adnađević, Borivoj K.

Dimitrijević, Suzana I.

Dimović, Slavko

Mitrić, Miodrag

Zmejkovski, Bojana

Smiljanić, Slavko
Article (Published version)
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Fluorapatite nanopowders with different amounts of fluoride ions were prepared using the surfactant-assisted microwave method under isothermal conditions. Microwave irradiation was applied for the rapid formation of crystals. A micellar solution of polyoxyethylene (23) lauryl ether was used as a regulator of nucleation and crystal growth. Characterization studies from X-ray diffraction, field-emission scaning electron microscopy and Fourier(-)transform infrared spectra showed that crystals have an apatite structure and particles of all samples are nano size, with an average length of 50 mn and about 15-25 nm in diameter. Antimicrobial studies have demonstrated that synthesized fluorapatite nanopowders exhibit activity against tested pathogens: Eseherichia coli, Staphylococcus aureus and Candida albicans. Activity increased with the amount of fluoride ions. The synthesized fluorapatite nanomaterials are promising as materials in environmental protection and medicine for orthopedics and ...dental restorations.
Keywords:
fluorapatite / microwave processing / nanopowder / environmental protectionSource:
Nuclear Technology & Radiation Protection, 2018, 33, 2, 180-187Publisher:
- Belgrade : Vinča Institute of Nuclear Sciences
Funding / projects:
DOI: 10.2298/NTRP1802180S
ISSN: 1451-3994
WoS: 000444067500006
Scopus: 2-s2.0-85053233415
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IHTMTY - JOUR AU - Stanić, Vojislav Dj. AU - Adnađević, Borivoj K. AU - Dimitrijević, Suzana I. AU - Dimović, Slavko AU - Mitrić, Miodrag AU - Zmejkovski, Bojana AU - Smiljanić, Slavko PY - 2018 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/2453 AB - Fluorapatite nanopowders with different amounts of fluoride ions were prepared using the surfactant-assisted microwave method under isothermal conditions. Microwave irradiation was applied for the rapid formation of crystals. A micellar solution of polyoxyethylene (23) lauryl ether was used as a regulator of nucleation and crystal growth. Characterization studies from X-ray diffraction, field-emission scaning electron microscopy and Fourier(-)transform infrared spectra showed that crystals have an apatite structure and particles of all samples are nano size, with an average length of 50 mn and about 15-25 nm in diameter. Antimicrobial studies have demonstrated that synthesized fluorapatite nanopowders exhibit activity against tested pathogens: Eseherichia coli, Staphylococcus aureus and Candida albicans. Activity increased with the amount of fluoride ions. The synthesized fluorapatite nanomaterials are promising as materials in environmental protection and medicine for orthopedics and dental restorations. PB - Belgrade : Vinča Institute of Nuclear Sciences T2 - Nuclear Technology & Radiation Protection T1 - Synthesis of fluorapatite nanopowders by a surfactant-assisted microwave method under isothermal conditions VL - 33 IS - 2 SP - 180 EP - 187 DO - 10.2298/NTRP1802180S ER -
@article{ author = "Stanić, Vojislav Dj. and Adnađević, Borivoj K. and Dimitrijević, Suzana I. and Dimović, Slavko and Mitrić, Miodrag and Zmejkovski, Bojana and Smiljanić, Slavko", year = "2018", abstract = "Fluorapatite nanopowders with different amounts of fluoride ions were prepared using the surfactant-assisted microwave method under isothermal conditions. Microwave irradiation was applied for the rapid formation of crystals. A micellar solution of polyoxyethylene (23) lauryl ether was used as a regulator of nucleation and crystal growth. Characterization studies from X-ray diffraction, field-emission scaning electron microscopy and Fourier(-)transform infrared spectra showed that crystals have an apatite structure and particles of all samples are nano size, with an average length of 50 mn and about 15-25 nm in diameter. Antimicrobial studies have demonstrated that synthesized fluorapatite nanopowders exhibit activity against tested pathogens: Eseherichia coli, Staphylococcus aureus and Candida albicans. Activity increased with the amount of fluoride ions. The synthesized fluorapatite nanomaterials are promising as materials in environmental protection and medicine for orthopedics and dental restorations.", publisher = "Belgrade : Vinča Institute of Nuclear Sciences", journal = "Nuclear Technology & Radiation Protection", title = "Synthesis of fluorapatite nanopowders by a surfactant-assisted microwave method under isothermal conditions", volume = "33", number = "2", pages = "180-187", doi = "10.2298/NTRP1802180S" }
Stanić, V. Dj., Adnađević, B. K., Dimitrijević, S. I., Dimović, S., Mitrić, M., Zmejkovski, B.,& Smiljanić, S.. (2018). Synthesis of fluorapatite nanopowders by a surfactant-assisted microwave method under isothermal conditions. in Nuclear Technology & Radiation Protection Belgrade : Vinča Institute of Nuclear Sciences., 33(2), 180-187. https://doi.org/10.2298/NTRP1802180S
Stanić VD, Adnađević BK, Dimitrijević SI, Dimović S, Mitrić M, Zmejkovski B, Smiljanić S. Synthesis of fluorapatite nanopowders by a surfactant-assisted microwave method under isothermal conditions. in Nuclear Technology & Radiation Protection. 2018;33(2):180-187. doi:10.2298/NTRP1802180S .
Stanić, Vojislav Dj., Adnađević, Borivoj K., Dimitrijević, Suzana I., Dimović, Slavko, Mitrić, Miodrag, Zmejkovski, Bojana, Smiljanić, Slavko, "Synthesis of fluorapatite nanopowders by a surfactant-assisted microwave method under isothermal conditions" in Nuclear Technology & Radiation Protection, 33, no. 2 (2018):180-187, https://doi.org/10.2298/NTRP1802180S . .