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dc.creatorAvramović, Ljiljana
dc.creatorBugarin, Mile
dc.creatorMilanović, D.
dc.creatorConić, V.
dc.creatorPavlović, Miroslav M.
dc.creatorVuković, M.
dc.creatorNikolić, Nebojša
dc.date.accessioned2019-01-30T17:59:38Z
dc.date.available2019-01-30T17:59:38Z
dc.date.issued2018
dc.identifier.issn1450-5339
dc.identifier.urihttp://cer.ihtm.bg.ac.rs/handle/123456789/2395
dc.description.abstractSilver powders produced by both electrochemical (galvanostatic (DC) and potentiostatic (POT) regimes of electrolysis) and chemical processes were examined by scanning electron microscope, and particle size distribution (PSD) of the obtained particles was done. In the DC regime, the current densities of -14.4 mA cm-2 for the nitrate (NIT; powder denoted with DC(NIT)) and -13.05 mA cm-2 for the ammonium (AM; DC(AM)) electrolytes were applied. In the POT regime, the used overpotentials were -90 mV (NIT(90)) and -150 mV (NIT(150)) for the nitrate, and -625 mV (AM(625)) and -925 mV (AM(925)) for the ammonium electrolytes. Reduction with hydrazine was used for chemical synthesis (powder denoted with HYD). On the basis of SEM and PSD analysis, Ag powders were grouped into three groups. In the first group DC(AM), AM(925) and HYD powders with the (8.4-8.9 %) volume ratios were placed. In the second group were AM(625) and DC(NIT) powders with the (6.5-6.6 %) volume ratios. NIT(90) and NIT(150) powders with the volume ratios of (5.2-5.7 %) made the third group. The obtained volume ratios were correlated with the morphology of synthesized particles in order to perceive advantages and lacks of powder production via electrochemical and chemical routes.en
dc.publisherTechnical Faculty, Bor
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172046/RS//
dc.rightsopenAccess
dc.sourceJournal of Mining and Metallurgy B: Metallurgy
dc.subjectChemical synthesisen
dc.subjectElectrolysisen
dc.subjectElektrolizaen
dc.subjectHemijska sintezaen
dc.subjectPowderen
dc.subjectPrahen
dc.subjectPSDen
dc.subjectPSDen
dc.subjectSEMen
dc.subjectSEMen
dc.subjectSilveren
dc.subjectSrebroen
dc.titleThe particle size distribution (PSD) as criteria for comparison of silver powders obtained by different methods of synthesis and by conditions of electrolysisen
dc.typearticle
dc.rights.licenseBY-SA
dcterms.abstractЦонић, В.; Николић, Небојша; Aврамовић, Л.; Бугарин, Миле; Павловић, Мирослав М.; Вуковић, М.; Милановић, Д.;
dc.citation.volume54
dc.citation.issue3
dc.citation.spage291
dc.citation.epage300
dc.citation.other54(3): 291-300
dc.citation.rankM22
dc.identifier.doi10.2298/JMMB171002020A
dc.identifier.rcubConv_4497
dc.identifier.fulltexthttp://cer.ihtm.bg.ac.rs//bitstream/id/8770/2393.pdf
dc.identifier.scopus2-s2.0-85059594317
dc.identifier.wos000462282900002
dc.type.versionpublishedVersion


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