Nanocrystalline Ni-ferrite was synthesized by modified precipitation method in which soluble starch is used as dispersing agent and Na2CO 3 as a precipitating agent. NiSO4-6H2O and Fe(NO3)3-9H2O were used as precursors for nickel and ferric oxide, respectively. The obtained nanocrystalline Ni-ferrite was analysed and discussed through structural, compositional and magnetic characterization. Formation of pure NiFe2O4 phase with average crystallite size of 21 nm has been con rmed by X-ray di raction analysis (XRD). The determined phase composition was additionally supported by results of 57Fe Mössbauer phase (MS) analysis and material's nanocrystalline structure by field emission scanning electron microscopy (FE-SEM). Thermomagnetic behaviour was studied up to 800 C. The obtained room temperature magnetic hysteresis loop, recorded by means of a vibrating sample magnetometer (VSM), exhibits characteristic "S" shape of the soft magnetic material with the measured coercivity of about 10 kA/...m and the specific moment up to 40 Am2/kg.
TY - CONF
AU - Žak, Tomas
AU - David, B.
AU - Ćosović, A.
AU - Ćosović, Vladan
AU - Živković, Dragana
AU - Talijan, Nadežda M.
PY - 2014
UR - https://cer.ihtm.bg.ac.rs/handle/123456789/1602
AB - Nanocrystalline Ni-ferrite was synthesized by modified precipitation method in which soluble starch is used as dispersing agent and Na2CO 3 as a precipitating agent. NiSO4-6H2O and Fe(NO3)3-9H2O were used as precursors for nickel and ferric oxide, respectively. The obtained nanocrystalline Ni-ferrite was analysed and discussed through structural, compositional and magnetic characterization. Formation of pure NiFe2O4 phase with average crystallite size of 21 nm has been con rmed by X-ray di raction analysis (XRD). The determined phase composition was additionally supported by results of 57Fe Mössbauer phase (MS) analysis and material's nanocrystalline structure by field emission scanning electron microscopy (FE-SEM). Thermomagnetic behaviour was studied up to 800 C. The obtained room temperature magnetic hysteresis loop, recorded by means of a vibrating sample magnetometer (VSM), exhibits characteristic "S" shape of the soft magnetic material with the measured coercivity of about 10 kA/m and the specific moment up to 40 Am2/kg.
PB - Polish Academy of Sciences
C3 - Acta Physica Polonica A
T1 - Structure and magnetic properties of nanocrystalline NiFe2O 4 prepared via precipitation route
VL - 126
IS - 1
SP - 142
EP - 143
DO - 10.12693/APhysPolA.126.142
ER -
@conference{
author = "Žak, Tomas and David, B. and Ćosović, A. and Ćosović, Vladan and Živković, Dragana and Talijan, Nadežda M.",
year = "2014",
abstract = "Nanocrystalline Ni-ferrite was synthesized by modified precipitation method in which soluble starch is used as dispersing agent and Na2CO 3 as a precipitating agent. NiSO4-6H2O and Fe(NO3)3-9H2O were used as precursors for nickel and ferric oxide, respectively. The obtained nanocrystalline Ni-ferrite was analysed and discussed through structural, compositional and magnetic characterization. Formation of pure NiFe2O4 phase with average crystallite size of 21 nm has been con rmed by X-ray di raction analysis (XRD). The determined phase composition was additionally supported by results of 57Fe Mössbauer phase (MS) analysis and material's nanocrystalline structure by field emission scanning electron microscopy (FE-SEM). Thermomagnetic behaviour was studied up to 800 C. The obtained room temperature magnetic hysteresis loop, recorded by means of a vibrating sample magnetometer (VSM), exhibits characteristic "S" shape of the soft magnetic material with the measured coercivity of about 10 kA/m and the specific moment up to 40 Am2/kg.",
publisher = "Polish Academy of Sciences",
journal = "Acta Physica Polonica A",
title = "Structure and magnetic properties of nanocrystalline NiFe2O 4 prepared via precipitation route",
volume = "126",
number = "1",
pages = "142-143",
doi = "10.12693/APhysPolA.126.142"
}
Žak, T., David, B., Ćosović, A., Ćosović, V., Živković, D.,& Talijan, N. M.. (2014). Structure and magnetic properties of nanocrystalline NiFe2O 4 prepared via precipitation route. in Acta Physica Polonica A
Polish Academy of Sciences., 126(1), 142-143.
https://doi.org/10.12693/APhysPolA.126.142
Žak T, David B, Ćosović A, Ćosović V, Živković D, Talijan NM. Structure and magnetic properties of nanocrystalline NiFe2O 4 prepared via precipitation route. in Acta Physica Polonica A. 2014;126(1):142-143.
doi:10.12693/APhysPolA.126.142 .
Žak, Tomas, David, B., Ćosović, A., Ćosović, Vladan, Živković, Dragana, Talijan, Nadežda M., "Structure and magnetic properties of nanocrystalline NiFe2O 4 prepared via precipitation route" in Acta Physica Polonica A, 126, no. 1 (2014):142-143,
https://doi.org/10.12693/APhysPolA.126.142 . .
