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dc.creatorTešević, Vele
dc.creatorAljančić, Ivana
dc.creatorVajs, Vlatka
dc.creatorŽivković, Marijana
dc.creatorNikićević, Ninoslav
dc.creatorUrosevic, Ivan
dc.creatorVujisić, Ljubodrag V.
dc.date.accessioned2019-01-30T17:40:40Z
dc.date.available2019-01-30T17:40:40Z
dc.date.issued2014
dc.identifier.issn0352-5139
dc.identifier.urihttp://cer.ihtm.bg.ac.rs/handle/123456789/1489
dc.description.abstractAn ultra-performance liquid chromatographic triple quadrupole mass spectrometric (UPLC-QqQ-MS/MS) method with a multiple reactions monitoring mode (MRM) was developed and validated for the quantification of vanillin and syringaldehyde in plum brandy. The method showed good linearity (0.05 to 10 mg L-1) and low limits of detection and quantification (the LOD and LOQ values were 11.6 and 38.2 mu g L-1 for vanillin, and 12.7 and 42.0 mu g L-1 for syringaldehyde, respectively). The overall intra-day and inter-day variations were less than 4.21 % and the overall recovery was over 93.0 %. The correlation coefficients (R-2) of the calibration curves were higher than 0.9999. In order to evaluate whether the method was suitable for use as a routine analytical tool, vanillin and syringaldehyde were determined in 31 samples of Serbian plum brandy.en
dc.publisherSerbian Chemical Soc, Belgrade
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172053/RS//
dc.rightsopenAccess
dc.sourceJournal of the Serbian Chemical Society
dc.subjectvanillinen
dc.subjectsyringaldehydeen
dc.subjectplum brandyen
dc.subjectLC-MS/MSen
dc.titleDevelopment and validation of an LC-MS/MS method with a multiple reactions monitoring mode for the quantification of vanillin and syringaldehyde in plum brandiesen
dc.typearticle
dc.rights.licenseBY-NC-ND
dcterms.abstractТесевиц, Веле; Aљанчић, Ивана С.; Вајс, Влатка; Никицевиц, Нинослав; Уросевиц, Иван; Вујисиц, Љубодраг; Живковић, Маријана;
dc.citation.volume79
dc.citation.issue12
dc.citation.spage1537
dc.citation.epage1543
dc.citation.other79(12): 1537-1543
dc.citation.rankM23
dc.identifier.doi10.2298/JSC140225079T
dc.identifier.rcubConv_3279
dc.identifier.fulltexthttp://cer.ihtm.bg.ac.rs//bitstream/id/7960/1487.pdf
dc.identifier.scopus2-s2.0-84920836911
dc.identifier.wos000348749400008
dc.type.versionpublishedVersion


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