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The synthesis of single phase WC nanoparticles/C composite by solid state reaction involving nitrogen-rich carbonized polyaniline

Authorized Users Only
2013
Authors
Gavrilov, Nemanja M.
Pasti, Igor
Krstić, Jugoslav
Mitrić, Miodrag
Ciric-Marjanovic, Gordana
Mentus, Slavko
Article (Published version)
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Abstract
Single phase tungsten carbide nanoparticles (WC-NPs), (mean particle diameter 5.4 nm), distributed over carbonized polyaniline (C-PANT) nanotubes/nanosheets were synthesized by a solid state reaction between WO3 and nitrogen-rich carbonized polyaniline at 1000 degrees C in a reducing atmosphere. The resulting composite was characterized by X-ray diffractometry, electron microscopy, thermogravimetry in oxidizing and reduction atmospheres and elemental analysis. We suggested that the synthesis of WC as a single phase was facilitated by reactive C atoms with dangling bonds, formed upon nitrogen removal.
Keywords:
Nanocomposite / Tungsten carbide / Nitrogen depletion / Carbonized polyaniline
Source:
Ceramics International, 2013, 39, 8, 8761-8765
Publisher:
  • Elsevier Sci Ltd, Oxford
Projects:
  • Lithium-ion batteries and fuel cells - research and development (RS-45014)
  • Electroconducting and redox-active polymers and oligomers: synthesis, structure, properties and applications (RS-172043)
  • Nanostructured Functional and Composite Materials in Catalytic and Sorption Processes (RS-45001)
  • Serbian Academy of Sciences and Arts

DOI: 10.1016/j.ceramint.2013.04.062

ISSN: 0272-8842

WoS: 000325835100026

Scopus: 2-s2.0-84883749039
[ Google Scholar ]
10
10
URI
http://cer.ihtm.bg.ac.rs/handle/123456789/1261
Collections
  • Radovi istraživača / Researchers' publications
Institution
IHTM
TY  - JOUR
AU  - Gavrilov, Nemanja M.
AU  - Pasti, Igor
AU  - Krstić, Jugoslav
AU  - Mitrić, Miodrag
AU  - Ciric-Marjanovic, Gordana
AU  - Mentus, Slavko
PY  - 2013
UR  - http://cer.ihtm.bg.ac.rs/handle/123456789/1261
AB  - Single phase tungsten carbide nanoparticles (WC-NPs), (mean particle diameter 5.4 nm), distributed over carbonized polyaniline (C-PANT) nanotubes/nanosheets were synthesized by a solid state reaction between WO3 and nitrogen-rich carbonized polyaniline at 1000 degrees C in a reducing atmosphere. The resulting composite was characterized by X-ray diffractometry, electron microscopy, thermogravimetry in oxidizing and reduction atmospheres and elemental analysis. We suggested that the synthesis of WC as a single phase was facilitated by reactive C atoms with dangling bonds, formed upon nitrogen removal.
PB  - Elsevier Sci Ltd, Oxford
T2  - Ceramics International
T1  - The synthesis of single phase WC nanoparticles/C composite by solid state reaction involving nitrogen-rich carbonized polyaniline
VL  - 39
IS  - 8
SP  - 8761
EP  - 8765
DO  - 10.1016/j.ceramint.2013.04.062
ER  - 
@article{
author = "Gavrilov, Nemanja M. and Pasti, Igor and Krstić, Jugoslav and Mitrić, Miodrag and Ciric-Marjanovic, Gordana and Mentus, Slavko",
year = "2013",
url = "http://cer.ihtm.bg.ac.rs/handle/123456789/1261",
abstract = "Single phase tungsten carbide nanoparticles (WC-NPs), (mean particle diameter 5.4 nm), distributed over carbonized polyaniline (C-PANT) nanotubes/nanosheets were synthesized by a solid state reaction between WO3 and nitrogen-rich carbonized polyaniline at 1000 degrees C in a reducing atmosphere. The resulting composite was characterized by X-ray diffractometry, electron microscopy, thermogravimetry in oxidizing and reduction atmospheres and elemental analysis. We suggested that the synthesis of WC as a single phase was facilitated by reactive C atoms with dangling bonds, formed upon nitrogen removal.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "The synthesis of single phase WC nanoparticles/C composite by solid state reaction involving nitrogen-rich carbonized polyaniline",
volume = "39",
number = "8",
pages = "8761-8765",
doi = "10.1016/j.ceramint.2013.04.062"
}
Gavrilov NM, Pasti I, Krstić J, Mitrić M, Ciric-Marjanovic G, Mentus S. The synthesis of single phase WC nanoparticles/C composite by solid state reaction involving nitrogen-rich carbonized polyaniline. Ceramics International. 2013;39(8):8761-8765
Gavrilov, N. M., Pasti, I., Krstić, J., Mitrić, M., Ciric-Marjanovic, G.,& Mentus, S. (2013). The synthesis of single phase WC nanoparticles/C composite by solid state reaction involving nitrogen-rich carbonized polyaniline.
Ceramics InternationalElsevier Sci Ltd, Oxford., 39(8), 8761-8765.
https://doi.org/10.1016/j.ceramint.2013.04.062
Gavrilov Nemanja M., Pasti Igor, Krstić Jugoslav, Mitrić Miodrag, Ciric-Marjanovic Gordana, Mentus Slavko, "The synthesis of single phase WC nanoparticles/C composite by solid state reaction involving nitrogen-rich carbonized polyaniline" 39, no. 8 (2013):8761-8765,
https://doi.org/10.1016/j.ceramint.2013.04.062 .

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