SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor

2013
Authors
Dimitrijević, R.Cvetković, Olga

Miodragović, Zoran
Simić, M.
Manojlović, Dragan

Jović, Vesna

Article (Published version)
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The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.
Keywords:
Ag nanoparticles / sphere shaped / chemical deposition / XRD technique / SEM/EDX analysisSource:
Journal of Mining and Metallurgy B: Metallurgy, 2013, 49, 1, 91-95Publisher:
- Technical Faculty, Bor-Serbia, Bor
Funding / projects:
- Application of advanced oxidation processes and nanostructured oxide materials for the removal of pollutants from the environment, development and optimisation of instrumental techniques for efficiency monitoring (RS-172030)
- Geochemical investigations of sedimentary rocks - fossil fuels and environmental pollutants (RS-176006)
- Micro- Nanosystems and Sensors for Electric Power and Process Industry and Environmental Protection (RS-32008)
DOI: 10.2298/JMMB120111041D
ISSN: 1450-5339
WoS: 000328704500014
Scopus: 2-s2.0-84880975200
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Institution/Community
IHTMTY - JOUR AU - Dimitrijević, R. AU - Cvetković, Olga AU - Miodragović, Zoran AU - Simić, M. AU - Manojlović, Dragan AU - Jović, Vesna PY - 2013 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/1169 AB - The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard. PB - Technical Faculty, Bor-Serbia, Bor T2 - Journal of Mining and Metallurgy B: Metallurgy T1 - SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor VL - 49 IS - 1 SP - 91 EP - 95 DO - 10.2298/JMMB120111041D ER -
@article{ author = "Dimitrijević, R. and Cvetković, Olga and Miodragović, Zoran and Simić, M. and Manojlović, Dragan and Jović, Vesna", year = "2013", abstract = "The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.", publisher = "Technical Faculty, Bor-Serbia, Bor", journal = "Journal of Mining and Metallurgy B: Metallurgy", title = "SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor", volume = "49", number = "1", pages = "91-95", doi = "10.2298/JMMB120111041D" }
Dimitrijević, R., Cvetković, O., Miodragović, Z., Simić, M., Manojlović, D.,& Jović, V.. (2013). SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor. in Journal of Mining and Metallurgy B: Metallurgy Technical Faculty, Bor-Serbia, Bor., 49(1), 91-95. https://doi.org/10.2298/JMMB120111041D
Dimitrijević R, Cvetković O, Miodragović Z, Simić M, Manojlović D, Jović V. SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor. in Journal of Mining and Metallurgy B: Metallurgy. 2013;49(1):91-95. doi:10.2298/JMMB120111041D .
Dimitrijević, R., Cvetković, Olga, Miodragović, Zoran, Simić, M., Manojlović, Dragan, Jović, Vesna, "SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor" in Journal of Mining and Metallurgy B: Metallurgy, 49, no. 1 (2013):91-95, https://doi.org/10.2298/JMMB120111041D . .