SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor

Dimitrijević, R.; Cvetković, Olga; Miodragović, Zoran; Simić, M.; Manojlović, Dragan; Jović, Vesna

doi:10.2298/JMMB120111041D

2013

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Authors

Dimitrijević, R.
Cvetković, Olga

Miodragović, Zoran
Simić, M.
Manojlović, Dragan

Jović, Vesna

Article (Published version)

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Abstract

The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.

Keywords:

Ag nanoparticles / sphere shaped / chemical deposition / XRD technique / SEM/EDX analysis

Source:
Journal of Mining and Metallurgy B: Metallurgy, 2013, 49, 1, 91-95

Publisher:

Technical Faculty, Bor-Serbia, Bor

Funding / projects:

DOI: 10.2298/JMMB120111041D

ISSN: 1450-5339

WoS: 000328704500014

Scopus: 2-s2.0-84880975200

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	23

TY  - JOUR
AU  - Dimitrijević, R.
AU  - Cvetković, Olga
AU  - Miodragović, Zoran
AU  - Simić, M.
AU  - Manojlović, Dragan
AU  - Jović, Vesna
PY  - 2013
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/1169
AB  - The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.
PB  - Technical Faculty, Bor-Serbia, Bor
T2  - Journal of Mining and Metallurgy B: Metallurgy
T1  - SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor
VL  - 49
IS  - 1
SP  - 91
EP  - 95
DO  - 10.2298/JMMB120111041D
ER  -

@article{
author = "Dimitrijević, R. and Cvetković, Olga and Miodragović, Zoran and Simić, M. and Manojlović, Dragan and Jović, Vesna",
year = "2013",
abstract = "The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.",
publisher = "Technical Faculty, Bor-Serbia, Bor",
journal = "Journal of Mining and Metallurgy B: Metallurgy",
title = "SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor",
volume = "49",
number = "1",
pages = "91-95",
doi = "10.2298/JMMB120111041D"
}

Dimitrijević, R., Cvetković, O., Miodragović, Z., Simić, M., Manojlović, D.,& Jović, V.. (2013). SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor. in Journal of Mining and Metallurgy B: Metallurgy
Technical Faculty, Bor-Serbia, Bor., 49(1), 91-95.
https://doi.org/10.2298/JMMB120111041D

Dimitrijević R, Cvetković O, Miodragović Z, Simić M, Manojlović D, Jović V. SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor. in Journal of Mining and Metallurgy B: Metallurgy. 2013;49(1):91-95.
doi:10.2298/JMMB120111041D .

Dimitrijević, R., Cvetković, Olga, Miodragović, Zoran, Simić, M., Manojlović, Dragan, Jović, Vesna, "SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor" in Journal of Mining and Metallurgy B: Metallurgy, 49, no. 1 (2013):91-95,
https://doi.org/10.2298/JMMB120111041D . .