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Synthesis of 5-azaandrostane-3β,17β-diol protected at the 17β-hydroxyl group
(Serbian Chemical Society, 2004)
In the present paper, the preparation of 3β-hydroxy-17β-dimethyl- tert-butylsilyloxy-5-azaandrostane (15) in fourteen steps is described. B-nor-17-oxoandrost-5-en-3β-yl acetate (1) 1,2 was used as the starting material, ...