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Hardness and assessment of adhesion of monolayer and multilayer nickel thin films electrochemically deposited on silicon substrates with and without the ultrasonic agitation

Lamovec, Jelena; Jović, Vesna; Jaćimovski, Stevo; Jovanov, Goran; Radojević, Vesna; Šetrajčić, Jovan

(Belgrade : Academy of Criminalistic and Police Studies, 2019)

TY  - JOUR
AU  - Lamovec, Jelena
AU  - Jović, Vesna
AU  - Jaćimovski, Stevo
AU  - Jovanov, Goran
AU  - Radojević, Vesna
AU  - Šetrajčić, Jovan
PY  - 2019
UR  - http://jakov.kpu.edu.rs/handle/123456789/929
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/2904
AB  - Composite systems of monolayer and multilayer nickel films electrochemically deposited on single crystal (100)-oriented silicon wafers were fabricated with and without the ultrasonic agitation. The hardness and adhesion behaviour of these composite structures were characterized by Vickers microindentation test. The dependence of composite microhardness and film adhesion on the structure of the film and mixing conditions of electrolyte were analysed. Mathematical models of Chicot-Lesage and Chen-Gao were applied to experimental data in order to obtain the film hardness and adhesion parameter respectively. It is confirmed that the mechanical properties of composite systems of nickel thin films on silicon substrate can be enhanced by formation of multilayer film structure by ultrasound-assisted electrodeposition and by reducing the layer thickness in the multilayer film.
AB  - Formirani su kompozitni sistemi od jednoslojnih i višeslojnih filmova nikla elektrohemijski deponovanih sa i bez ultrazvučnog mešanja na pločicama od monokristalnog silicijuma orijentacije (100). Tvrdoća i adhezija tih kompozitnih struktura su okarakterisane testom mikrotvrdoće po Vikersu. Analizirana je zavisnost mikrotvrdoće kompozita i adhezije filma od strukture filma i uslova mešanja elektrolita. Matematički modeli Šiko-Lezaža i Čen-Gaoa su primenjeni na eksperimentalne podatke kako bi se dobile vrednosti tvrdoće filma i parametra adhezije. Potvrđeno je da se mehanička svojstva kompozit-nih sistema sastavljenih od tankih filmova nikla na silicijumskoj podlozi mogu poboljšati formiranjem višeslojne strukture filmova, primenom ultrazvučnog mešanja pri elektrodepoziciji i smanjenjem debljine sloja u višeslojnom filmu.
PB  - Belgrade : Academy of Criminalistic and Police Studies
T2  - NBP : Journal of Criminalistic and Law : Žurnal za kriminalistiku i pravo
T1  - Hardness and assessment of adhesion of monolayer and multilayer nickel thin films electrochemically deposited on silicon substrates with and without the ultrasonic agitation
T1  - Tvrdoća i procena adhezije jednoslojnih i višeslojnih tankih filmova nikla elektrohemijski deponovanih na silicijumskim podlogama sa i bez ultrazvučnog mešanja
VL  - 24
IS  - 1
SP  - 17
EP  - 29
DO  - 10.5937/nabepo24-19682
ER  - 
@article{
author = "Lamovec, Jelena and Jović, Vesna and Jaćimovski, Stevo and Jovanov, Goran and Radojević, Vesna and Šetrajčić, Jovan",
year = "2019",
abstract = "Composite systems of monolayer and multilayer nickel films electrochemically deposited on single crystal (100)-oriented silicon wafers were fabricated with and without the ultrasonic agitation. The hardness and adhesion behaviour of these composite structures were characterized by Vickers microindentation test. The dependence of composite microhardness and film adhesion on the structure of the film and mixing conditions of electrolyte were analysed. Mathematical models of Chicot-Lesage and Chen-Gao were applied to experimental data in order to obtain the film hardness and adhesion parameter respectively. It is confirmed that the mechanical properties of composite systems of nickel thin films on silicon substrate can be enhanced by formation of multilayer film structure by ultrasound-assisted electrodeposition and by reducing the layer thickness in the multilayer film., Formirani su kompozitni sistemi od jednoslojnih i višeslojnih filmova nikla elektrohemijski deponovanih sa i bez ultrazvučnog mešanja na pločicama od monokristalnog silicijuma orijentacije (100). Tvrdoća i adhezija tih kompozitnih struktura su okarakterisane testom mikrotvrdoće po Vikersu. Analizirana je zavisnost mikrotvrdoće kompozita i adhezije filma od strukture filma i uslova mešanja elektrolita. Matematički modeli Šiko-Lezaža i Čen-Gaoa su primenjeni na eksperimentalne podatke kako bi se dobile vrednosti tvrdoće filma i parametra adhezije. Potvrđeno je da se mehanička svojstva kompozit-nih sistema sastavljenih od tankih filmova nikla na silicijumskoj podlozi mogu poboljšati formiranjem višeslojne strukture filmova, primenom ultrazvučnog mešanja pri elektrodepoziciji i smanjenjem debljine sloja u višeslojnom filmu.",
publisher = "Belgrade : Academy of Criminalistic and Police Studies",
journal = "NBP : Journal of Criminalistic and Law : Žurnal za kriminalistiku i pravo",
title = "Hardness and assessment of adhesion of monolayer and multilayer nickel thin films electrochemically deposited on silicon substrates with and without the ultrasonic agitation, Tvrdoća i procena adhezije jednoslojnih i višeslojnih tankih filmova nikla elektrohemijski deponovanih na silicijumskim podlogama sa i bez ultrazvučnog mešanja",
volume = "24",
number = "1",
pages = "17-29",
doi = "10.5937/nabepo24-19682"
}
Lamovec, J., Jović, V., Jaćimovski, S., Jovanov, G., Radojević, V.,& Šetrajčić, J.. (2019). Hardness and assessment of adhesion of monolayer and multilayer nickel thin films electrochemically deposited on silicon substrates with and without the ultrasonic agitation. in NBP : Journal of Criminalistic and Law : Žurnal za kriminalistiku i pravo
Belgrade : Academy of Criminalistic and Police Studies., 24(1), 17-29.
https://doi.org/10.5937/nabepo24-19682
Lamovec J, Jović V, Jaćimovski S, Jovanov G, Radojević V, Šetrajčić J. Hardness and assessment of adhesion of monolayer and multilayer nickel thin films electrochemically deposited on silicon substrates with and without the ultrasonic agitation. in NBP : Journal of Criminalistic and Law : Žurnal za kriminalistiku i pravo. 2019;24(1):17-29.
doi:10.5937/nabepo24-19682 .
Lamovec, Jelena, Jović, Vesna, Jaćimovski, Stevo, Jovanov, Goran, Radojević, Vesna, Šetrajčić, Jovan, "Hardness and assessment of adhesion of monolayer and multilayer nickel thin films electrochemically deposited on silicon substrates with and without the ultrasonic agitation" in NBP : Journal of Criminalistic and Law : Žurnal za kriminalistiku i pravo, 24, no. 1 (2019):17-29,
https://doi.org/10.5937/nabepo24-19682 . .