Nićetin, Milica

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orcid::0000-0003-4958-5129
  • Nićetin, Milica (1)
  • Nićetin, Milica R. (1)
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Author's Bibliography

Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses

Nićetin, Milica; Pezo, Lato; Pergal, Marija; Lončar, Biljana; Filipović, Vladimir; Knežević, Violeta; Demir, Hande; Filipović, Jelena; Manojlović, Dragan

(MDPI, 2022)

TY  - JOUR
AU  - Nićetin, Milica
AU  - Pezo, Lato
AU  - Pergal, Marija
AU  - Lončar, Biljana
AU  - Filipović, Vladimir
AU  - Knežević, Violeta
AU  - Demir, Hande
AU  - Filipović, Jelena
AU  - Manojlović, Dragan
PY  - 2022
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/5582
AB  - The osmotic dehydration (OD) of celery root in sugar beet molasses was studied at three temperatures (20, 35, and 50 °C) and three immersion periods (1, 3, and 5 h) in order to examine the changes in antioxidant potential and phenolic profile of celery root throughout the process. The antioxidant capacity (AOC) of dehydrated samples was evaluated by spectrophotometric and polarographic assays, the total phenolic content by the Folin-Ciocalteu method, and the individual phenolic compounds by HPLC-DAD. As a result of OD in molasses, the AOC and phenols content in samples increased proportionally to the augmentation of temperature and the immersion time. Vanillic acid, syringic acid, and catechin were detected in dehydrated samples as a result of transfer from molasses. Compared to fresh celery root, the content of identified phenols in osmodehydrated samples was improved from 1.5 to 6.2 times. Strong correlations between applied assays were obtained, except for the DPPH. Based on the correlation analysis chlorogenic acid, gallic acid, chrysin, catechin, and kaempferol showed the greatest contribution to the overall AOC of osmodehydrated celery root. Molasses, an agro-industrial waste from sugar production, could be valorized as a valuable osmotic solution.
PB  - MDPI
T2  - Foods
T1  - Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses
VL  - 11
IS  - 13
SP  - 1945
DO  - 10.3390/foods11131945
ER  - 
@article{
author = "Nićetin, Milica and Pezo, Lato and Pergal, Marija and Lončar, Biljana and Filipović, Vladimir and Knežević, Violeta and Demir, Hande and Filipović, Jelena and Manojlović, Dragan",
year = "2022",
abstract = "The osmotic dehydration (OD) of celery root in sugar beet molasses was studied at three temperatures (20, 35, and 50 °C) and three immersion periods (1, 3, and 5 h) in order to examine the changes in antioxidant potential and phenolic profile of celery root throughout the process. The antioxidant capacity (AOC) of dehydrated samples was evaluated by spectrophotometric and polarographic assays, the total phenolic content by the Folin-Ciocalteu method, and the individual phenolic compounds by HPLC-DAD. As a result of OD in molasses, the AOC and phenols content in samples increased proportionally to the augmentation of temperature and the immersion time. Vanillic acid, syringic acid, and catechin were detected in dehydrated samples as a result of transfer from molasses. Compared to fresh celery root, the content of identified phenols in osmodehydrated samples was improved from 1.5 to 6.2 times. Strong correlations between applied assays were obtained, except for the DPPH. Based on the correlation analysis chlorogenic acid, gallic acid, chrysin, catechin, and kaempferol showed the greatest contribution to the overall AOC of osmodehydrated celery root. Molasses, an agro-industrial waste from sugar production, could be valorized as a valuable osmotic solution.",
publisher = "MDPI",
journal = "Foods",
title = "Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses",
volume = "11",
number = "13",
pages = "1945",
doi = "10.3390/foods11131945"
}
Nićetin, M., Pezo, L., Pergal, M., Lončar, B., Filipović, V., Knežević, V., Demir, H., Filipović, J.,& Manojlović, D.. (2022). Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses. in Foods
MDPI., 11(13), 1945.
https://doi.org/10.3390/foods11131945
Nićetin M, Pezo L, Pergal M, Lončar B, Filipović V, Knežević V, Demir H, Filipović J, Manojlović D. Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses. in Foods. 2022;11(13):1945.
doi:10.3390/foods11131945 .
Nićetin, Milica, Pezo, Lato, Pergal, Marija, Lončar, Biljana, Filipović, Vladimir, Knežević, Violeta, Demir, Hande, Filipović, Jelena, Manojlović, Dragan, "Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses" in Foods, 11, no. 13 (2022):1945,
https://doi.org/10.3390/foods11131945 . .
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Evaluation of water, sucrose and minerals effective diffusivities during osmotic treatment of pork in sugar beet molasses

Nićetin, Milica R.; Pezo, Lato; Lončar, Biljana; Filipović, Vladimir S.; Šuput, Danijela Z.; Zlatanović, Snežana; Dojčinović, Biljana

(Association of Chemical Engineers of Serbia, 2015)

TY  - JOUR
AU  - Nićetin, Milica R.
AU  - Pezo, Lato
AU  - Lončar, Biljana
AU  - Filipović, Vladimir S.
AU  - Šuput, Danijela Z.
AU  - Zlatanović, Snežana
AU  - Dojčinović, Biljana
PY  - 2015
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/1641
AB  - Effective diffusivities of water, sucrose and minerals in osmotic treatment of pork cubes (M. triceps brachii) were calculated using Response Surface Methodology (RSM), with respect to temperature (20, 35 and 50°C) and concentration of sugar beet molasses, (60, 70 and 80 mass%). The numerical solution of Fick's law for unsteady-state mass transfer in a perfect cube configuration was used to calculate the effective diffusivities of water, sucrose and minerals (Na, K, Ca and Mg). Zugarramurdi and Lupin's model was used to predict the equilibrium condition, which has shown to be appropriate for water loss and solute uptake during osmotic treatment. Effective diffusivity of water was found to be in the range of 6.95×10-10-8.03×10-10 m2 s-1, the sucrose effective diffusivity was between 6.39×10-10 and 8.25×10-10 m2 s-1, while diffusivities for minerals (m2 s-1) were in the range: 6.34×10-10-8.82×10-10 for Na, 6.27×10-10-7.43×10-10 for K, 6.44×10-10-8.94×10-10 for Ca and 3.47×10-10-5.66×10-10 for Mg.
AB  - Metoda odzivne površine (Response Surface Methodology - RSM) je korišćena pri matematičkom modelovanju i izračunavanju vrednosti prividne (efektivne) difuzije vode, saharoze i minerala tokom osmotskog tretmana kockica svinjskog mesa (M. triceps brachii), na temperaturi 20, 35 i 50°C i pri koncentracijama osmotskog rastvora (melasa šećerne repe) od 60, 70 i 80 mas.%. Numeričko rešavanje Fikovog (Fick) zakona o prenosu mase, pri nestacionarnim uslovima, za idealnu kocku je korišćeno za izračunavanje efektivnog koeficijenta difuzije vode, saharoze i minerala (Na, K, Ca and Mg). Sadržaj vlage i minerala je izmeren u tri ponavljanja. Korišćen je model Cuguramurdija (Zugarramurdi) i Lupina (Lupin) za predviđanje ravnotežnih uslova i ispostavilo se da je taj model pogodan za izračunavanje gubitka vlage i priraštaja suve materije tokom procesa osmotskog tretmana. Metoda odzivnih površina, koje se široko koristi za modelovanje i kontrolu procesa u prehrambenoj industriji, a u ovom radu je korišćena za predviđanje efektivnog koeficijenta difuzije vode, saharoze i minerala, pri određenoj temperaturi imerzije i koncentraciji melase šećerne repe. Matematički modeli koji su dobijeni na osnovu eksperimentalnih podataka obrađuju kompleksne nelinearne relacije sa interakcijama između procesnih promenljivih. Dobijene vrednosti efektivne difuzivnosti (m2 s-1) za vodu bili su u rasponu od 6,95×10-10 do 8,03×10-10, za efektivnu difuzivnost saharoze bili su između 6,39×10-10 i 8,25×10-10, dok su difuzivnosti za minerale bile u opsezima: 6,34×10-10-8,82×10-10 (Na), 6,27×10-10- -7,43×10-10 (K), 6,44×10-10-8,94×10-10 (Ca) i 3,47×10-10-5,66×10-10 (Mg). Korišćenjem razvijenih matematičkih modela dobijene su vrednosti efektivnih koeficijenata difuzije, sa tačnošću izraženom preko koeficijenata determinacije (r2) za Dw, DSuc, DNa. DK, DCa i DMg, i to: 0,993; 0,998; 0,999; 0,992; 0,999 i 0,998, redom. Širok opseg procesnih promenljivih veličina razmatranih u formiranju ovih modela, kao i njihova laka implementacija u tabelarnim proračunima, čini ove modele veoma praktičnim za projektovanje i kontrolu procesa.
PB  - Association of Chemical Engineers of Serbia
T2  - Hemijska industrija
T1  - Evaluation of water, sucrose and minerals effective diffusivities during osmotic treatment of pork in sugar beet molasses
T1  - Prividni koeficijenti difuzije vode, saharoze i minerala pri osmotskom tretmanu svinjskog mesa u melasi šećerne repe
VL  - 69
IS  - 3
SP  - 241
EP  - 251
DO  - 10.2298/HEMIND131003037N
ER  - 
@article{
author = "Nićetin, Milica R. and Pezo, Lato and Lončar, Biljana and Filipović, Vladimir S. and Šuput, Danijela Z. and Zlatanović, Snežana and Dojčinović, Biljana",
year = "2015",
abstract = "Effective diffusivities of water, sucrose and minerals in osmotic treatment of pork cubes (M. triceps brachii) were calculated using Response Surface Methodology (RSM), with respect to temperature (20, 35 and 50°C) and concentration of sugar beet molasses, (60, 70 and 80 mass%). The numerical solution of Fick's law for unsteady-state mass transfer in a perfect cube configuration was used to calculate the effective diffusivities of water, sucrose and minerals (Na, K, Ca and Mg). Zugarramurdi and Lupin's model was used to predict the equilibrium condition, which has shown to be appropriate for water loss and solute uptake during osmotic treatment. Effective diffusivity of water was found to be in the range of 6.95×10-10-8.03×10-10 m2 s-1, the sucrose effective diffusivity was between 6.39×10-10 and 8.25×10-10 m2 s-1, while diffusivities for minerals (m2 s-1) were in the range: 6.34×10-10-8.82×10-10 for Na, 6.27×10-10-7.43×10-10 for K, 6.44×10-10-8.94×10-10 for Ca and 3.47×10-10-5.66×10-10 for Mg., Metoda odzivne površine (Response Surface Methodology - RSM) je korišćena pri matematičkom modelovanju i izračunavanju vrednosti prividne (efektivne) difuzije vode, saharoze i minerala tokom osmotskog tretmana kockica svinjskog mesa (M. triceps brachii), na temperaturi 20, 35 i 50°C i pri koncentracijama osmotskog rastvora (melasa šećerne repe) od 60, 70 i 80 mas.%. Numeričko rešavanje Fikovog (Fick) zakona o prenosu mase, pri nestacionarnim uslovima, za idealnu kocku je korišćeno za izračunavanje efektivnog koeficijenta difuzije vode, saharoze i minerala (Na, K, Ca and Mg). Sadržaj vlage i minerala je izmeren u tri ponavljanja. Korišćen je model Cuguramurdija (Zugarramurdi) i Lupina (Lupin) za predviđanje ravnotežnih uslova i ispostavilo se da je taj model pogodan za izračunavanje gubitka vlage i priraštaja suve materije tokom procesa osmotskog tretmana. Metoda odzivnih površina, koje se široko koristi za modelovanje i kontrolu procesa u prehrambenoj industriji, a u ovom radu je korišćena za predviđanje efektivnog koeficijenta difuzije vode, saharoze i minerala, pri određenoj temperaturi imerzije i koncentraciji melase šećerne repe. Matematički modeli koji su dobijeni na osnovu eksperimentalnih podataka obrađuju kompleksne nelinearne relacije sa interakcijama između procesnih promenljivih. Dobijene vrednosti efektivne difuzivnosti (m2 s-1) za vodu bili su u rasponu od 6,95×10-10 do 8,03×10-10, za efektivnu difuzivnost saharoze bili su između 6,39×10-10 i 8,25×10-10, dok su difuzivnosti za minerale bile u opsezima: 6,34×10-10-8,82×10-10 (Na), 6,27×10-10- -7,43×10-10 (K), 6,44×10-10-8,94×10-10 (Ca) i 3,47×10-10-5,66×10-10 (Mg). Korišćenjem razvijenih matematičkih modela dobijene su vrednosti efektivnih koeficijenata difuzije, sa tačnošću izraženom preko koeficijenata determinacije (r2) za Dw, DSuc, DNa. DK, DCa i DMg, i to: 0,993; 0,998; 0,999; 0,992; 0,999 i 0,998, redom. Širok opseg procesnih promenljivih veličina razmatranih u formiranju ovih modela, kao i njihova laka implementacija u tabelarnim proračunima, čini ove modele veoma praktičnim za projektovanje i kontrolu procesa.",
publisher = "Association of Chemical Engineers of Serbia",
journal = "Hemijska industrija",
title = "Evaluation of water, sucrose and minerals effective diffusivities during osmotic treatment of pork in sugar beet molasses, Prividni koeficijenti difuzije vode, saharoze i minerala pri osmotskom tretmanu svinjskog mesa u melasi šećerne repe",
volume = "69",
number = "3",
pages = "241-251",
doi = "10.2298/HEMIND131003037N"
}
Nićetin, M. R., Pezo, L., Lončar, B., Filipović, V. S., Šuput, D. Z., Zlatanović, S.,& Dojčinović, B.. (2015). Evaluation of water, sucrose and minerals effective diffusivities during osmotic treatment of pork in sugar beet molasses. in Hemijska industrija
Association of Chemical Engineers of Serbia., 69(3), 241-251.
https://doi.org/10.2298/HEMIND131003037N
Nićetin MR, Pezo L, Lončar B, Filipović VS, Šuput DZ, Zlatanović S, Dojčinović B. Evaluation of water, sucrose and minerals effective diffusivities during osmotic treatment of pork in sugar beet molasses. in Hemijska industrija. 2015;69(3):241-251.
doi:10.2298/HEMIND131003037N .
Nićetin, Milica R., Pezo, Lato, Lončar, Biljana, Filipović, Vladimir S., Šuput, Danijela Z., Zlatanović, Snežana, Dojčinović, Biljana, "Evaluation of water, sucrose and minerals effective diffusivities during osmotic treatment of pork in sugar beet molasses" in Hemijska industrija, 69, no. 3 (2015):241-251,
https://doi.org/10.2298/HEMIND131003037N . .
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