Veličković, Milovan M.

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Volatile compounds in medlar fruit (Mespilus germanica L.) at two ripening stages

Veličković, Milovan M.; Radivojević, Dragan D.; Oparnica, Čedo Đ.; Nikićević, Ninoslav; Živković, Marijana; Đorđević, Neda O.; Vajs, Vlatka; Tešević, Vele

(Assoc Chemists & Chemical Engineers Of Serbia, Belgrade, 2013)

TY  - JOUR
AU  - Veličković, Milovan M.
AU  - Radivojević, Dragan D.
AU  - Oparnica, Čedo Đ.
AU  - Nikićević, Ninoslav
AU  - Živković, Marijana
AU  - Đorđević, Neda O.
AU  - Vajs, Vlatka
AU  - Tešević, Vele
PY  - 2013
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/1164
AB  - Medlar is the fruit of Mespilus germanica L. in the family of Rosaceae. The fruit can be eaten only if "bletted" (softened by frost or longer storage). The effect of the maturation stages on the volatile compounds of the medlar fruit was investigated during two different stages. Volatile flavour substances were isolated from the minced pulp of unripe and full ripe medlar fruits by simultaneous steam distillation extraction (SDE) with methylene chloride as the extracting solvent. The concentrate was analyzed by GC-FID-MS. Hexanoic and hexadecanoic acids were the predominant acids, hexanal and (E)-2-hexenal were the predominant aldehydes, (Z)-3-hexenol and hexanol were the predominant alcohols, with p-cymene, terpinen-4-ol, and γ-terpinene (the terpenes responsible for the characteristic medlar flavour) being also present. The C6 aliphatic compounds, such as hexanal and (E)-2-hexenal, were observed as the major volatile constituents in the green stage. In contrast, hexanol and (Z)-3-hexenol were the main volatiles in ripe fruits.
AB  - Mušmula (Mespilus germanica L) je voće iz porodice ruža (Rosaceae). Zeleni plodovi mušmule nisu jestivi već treba da ugnile (omekšaju usled mraza ili tokom čuvanja) pre nego što se koriste u ishrani. Efekat procesa sazrevanja na isparljive komponente ploda mušmule ispitivan je u dve različite faze njegove zrelosti. Isparljiva jedinjenja su izolovana iz izmrvljene pulpe nezrelih i zrelih plodova mušmule pomoću simultane destilacije vodenom parom i ekstrakcije metilen-hloridom. Koncentrovani uzorak je analiziran kombinacijom metoda GC-FID-MS. Heksanska i palmitinska kiselina su najzastupljenije kiseline, heksanal i (E)-2-heksenal su najzastupljeniji aldehidi, (Z)-3-heksenol i heksanol su najzastupljeniji alkoholi i p-cimen, terpinen-4-ol i γ-terpinen, terpeni odgovorni za karakterističnu aromu ploda mušmule, takođe su prisutni. C6 alifatična jedinjenja, kao što su heksanal i (E)-2-heksenal su nađeni kao glavne isparljive komponente zelenih mušmula. Za razliku od njih, heksanol, (Z)-3-heksenol su glavne komponente zrelih plodova mušmule.
PB  - Assoc Chemists & Chemical Engineers Of Serbia, Belgrade
T2  - Hemijska industrija
T1  - Volatile compounds in medlar fruit (Mespilus germanica L.) at two ripening stages
T1  - Isparljiva jedinjenja iz ploda mušmule (Mespilus germanica L.) u dve faze zrenja
VL  - 67
IS  - 3
SP  - 437
EP  - 441
DO  - 10.2298/HEMIND120611085V
ER  - 
@article{
author = "Veličković, Milovan M. and Radivojević, Dragan D. and Oparnica, Čedo Đ. and Nikićević, Ninoslav and Živković, Marijana and Đorđević, Neda O. and Vajs, Vlatka and Tešević, Vele",
year = "2013",
abstract = "Medlar is the fruit of Mespilus germanica L. in the family of Rosaceae. The fruit can be eaten only if "bletted" (softened by frost or longer storage). The effect of the maturation stages on the volatile compounds of the medlar fruit was investigated during two different stages. Volatile flavour substances were isolated from the minced pulp of unripe and full ripe medlar fruits by simultaneous steam distillation extraction (SDE) with methylene chloride as the extracting solvent. The concentrate was analyzed by GC-FID-MS. Hexanoic and hexadecanoic acids were the predominant acids, hexanal and (E)-2-hexenal were the predominant aldehydes, (Z)-3-hexenol and hexanol were the predominant alcohols, with p-cymene, terpinen-4-ol, and γ-terpinene (the terpenes responsible for the characteristic medlar flavour) being also present. The C6 aliphatic compounds, such as hexanal and (E)-2-hexenal, were observed as the major volatile constituents in the green stage. In contrast, hexanol and (Z)-3-hexenol were the main volatiles in ripe fruits., Mušmula (Mespilus germanica L) je voće iz porodice ruža (Rosaceae). Zeleni plodovi mušmule nisu jestivi već treba da ugnile (omekšaju usled mraza ili tokom čuvanja) pre nego što se koriste u ishrani. Efekat procesa sazrevanja na isparljive komponente ploda mušmule ispitivan je u dve različite faze njegove zrelosti. Isparljiva jedinjenja su izolovana iz izmrvljene pulpe nezrelih i zrelih plodova mušmule pomoću simultane destilacije vodenom parom i ekstrakcije metilen-hloridom. Koncentrovani uzorak je analiziran kombinacijom metoda GC-FID-MS. Heksanska i palmitinska kiselina su najzastupljenije kiseline, heksanal i (E)-2-heksenal su najzastupljeniji aldehidi, (Z)-3-heksenol i heksanol su najzastupljeniji alkoholi i p-cimen, terpinen-4-ol i γ-terpinen, terpeni odgovorni za karakterističnu aromu ploda mušmule, takođe su prisutni. C6 alifatična jedinjenja, kao što su heksanal i (E)-2-heksenal su nađeni kao glavne isparljive komponente zelenih mušmula. Za razliku od njih, heksanol, (Z)-3-heksenol su glavne komponente zrelih plodova mušmule.",
publisher = "Assoc Chemists & Chemical Engineers Of Serbia, Belgrade",
journal = "Hemijska industrija",
title = "Volatile compounds in medlar fruit (Mespilus germanica L.) at two ripening stages, Isparljiva jedinjenja iz ploda mušmule (Mespilus germanica L.) u dve faze zrenja",
volume = "67",
number = "3",
pages = "437-441",
doi = "10.2298/HEMIND120611085V"
}
Veličković, M. M., Radivojević, D. D., Oparnica, Č. Đ., Nikićević, N., Živković, M., Đorđević, N. O., Vajs, V.,& Tešević, V.. (2013). Volatile compounds in medlar fruit (Mespilus germanica L.) at two ripening stages. in Hemijska industrija
Assoc Chemists & Chemical Engineers Of Serbia, Belgrade., 67(3), 437-441.
https://doi.org/10.2298/HEMIND120611085V
Veličković MM, Radivojević DD, Oparnica ČĐ, Nikićević N, Živković M, Đorđević NO, Vajs V, Tešević V. Volatile compounds in medlar fruit (Mespilus germanica L.) at two ripening stages. in Hemijska industrija. 2013;67(3):437-441.
doi:10.2298/HEMIND120611085V .
Veličković, Milovan M., Radivojević, Dragan D., Oparnica, Čedo Đ., Nikićević, Ninoslav, Živković, Marijana, Đorđević, Neda O., Vajs, Vlatka, Tešević, Vele, "Volatile compounds in medlar fruit (Mespilus germanica L.) at two ripening stages" in Hemijska industrija, 67, no. 3 (2013):437-441,
https://doi.org/10.2298/HEMIND120611085V . .
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The determination of quantitative jugolone content dynamics and the antioxidant activity in the extract of green walnut (Juglans regia L.) fruits

Veličković, Milovan M.; Vulić, Todor; Oparnica, Čedo; Radivojević, Dragan; Đorđević, Boban; Tešević, Vele; Jadranin, Milka

(2007)

TY  - JOUR
AU  - Veličković, Milovan M.
AU  - Vulić, Todor
AU  - Oparnica, Čedo
AU  - Radivojević, Dragan
AU  - Đorđević, Boban
AU  - Tešević, Vele
AU  - Jadranin, Milka
PY  - 2007
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/321
AB  - Fruits from three walnut cultivars were picked in three terms with the aim to determine the optimal harvesting time of green walnut fruits for the improvement fruit brandies. Quantity of juglone and its antioxidant activity was determined in the picked fruits. Juglone quantity was the highest in fruits weighing between 4.5 g and 6.5 g (harvesting time around June 1), and varied from 209.60 mg up to 735.00 mg in the cultivar Sheinovo, from 388.50 mg up to 418.60 mg in the cultivar Geisenheim 139 and from 325.50 mg up to 499.40 mg in the cultivar Geisenheim 251, in a sample of 100 fruits. In this phase, walnut fruits had the highest antioxidant activity, too. .
AB  - Tehnikom visokoefikasne tečne hromatografije određivan je sadržaj juglona (5-hidroxi-1,4-naftohinona) u uzorcima mladog oraha različitih sorti i različite zrelosti berbi 2005. i 2006. godine. Pored toga određena je anatioksidativna aktivnost metanolnih ekstrakata uzoraka plodova. Koncentracije juglona se nalaze u opsegu 0,03-0,24 % za berbu 2005. i 0,03-0,08 % za berbu 2006. Svi uzorci su pokazali značajnu antioksidativnu aktivnost. .
T2  - Journal of Scientific Agricultural Research
T1  - The determination of quantitative jugolone content dynamics and the antioxidant activity in the extract of green walnut (Juglans regia L.) fruits
T1  - Određivanje dinamike kvantitativnog sadržaja juglona i antioksidativne aktivnosti u ekstraktu ploda mladog oraha (Juglans regia)
VL  - 68
IS  - 1
SP  - 59
EP  - 68
UR  - https://hdl.handle.net/21.15107/rcub_cer_321
ER  - 
@article{
author = "Veličković, Milovan M. and Vulić, Todor and Oparnica, Čedo and Radivojević, Dragan and Đorđević, Boban and Tešević, Vele and Jadranin, Milka",
year = "2007",
abstract = "Fruits from three walnut cultivars were picked in three terms with the aim to determine the optimal harvesting time of green walnut fruits for the improvement fruit brandies. Quantity of juglone and its antioxidant activity was determined in the picked fruits. Juglone quantity was the highest in fruits weighing between 4.5 g and 6.5 g (harvesting time around June 1), and varied from 209.60 mg up to 735.00 mg in the cultivar Sheinovo, from 388.50 mg up to 418.60 mg in the cultivar Geisenheim 139 and from 325.50 mg up to 499.40 mg in the cultivar Geisenheim 251, in a sample of 100 fruits. In this phase, walnut fruits had the highest antioxidant activity, too. ., Tehnikom visokoefikasne tečne hromatografije određivan je sadržaj juglona (5-hidroxi-1,4-naftohinona) u uzorcima mladog oraha različitih sorti i različite zrelosti berbi 2005. i 2006. godine. Pored toga određena je anatioksidativna aktivnost metanolnih ekstrakata uzoraka plodova. Koncentracije juglona se nalaze u opsegu 0,03-0,24 % za berbu 2005. i 0,03-0,08 % za berbu 2006. Svi uzorci su pokazali značajnu antioksidativnu aktivnost. .",
journal = "Journal of Scientific Agricultural Research",
title = "The determination of quantitative jugolone content dynamics and the antioxidant activity in the extract of green walnut (Juglans regia L.) fruits, Određivanje dinamike kvantitativnog sadržaja juglona i antioksidativne aktivnosti u ekstraktu ploda mladog oraha (Juglans regia)",
volume = "68",
number = "1",
pages = "59-68",
url = "https://hdl.handle.net/21.15107/rcub_cer_321"
}
Veličković, M. M., Vulić, T., Oparnica, Č., Radivojević, D., Đorđević, B., Tešević, V.,& Jadranin, M.. (2007). The determination of quantitative jugolone content dynamics and the antioxidant activity in the extract of green walnut (Juglans regia L.) fruits. in Journal of Scientific Agricultural Research, 68(1), 59-68.
https://hdl.handle.net/21.15107/rcub_cer_321
Veličković MM, Vulić T, Oparnica Č, Radivojević D, Đorđević B, Tešević V, Jadranin M. The determination of quantitative jugolone content dynamics and the antioxidant activity in the extract of green walnut (Juglans regia L.) fruits. in Journal of Scientific Agricultural Research. 2007;68(1):59-68.
https://hdl.handle.net/21.15107/rcub_cer_321 .
Veličković, Milovan M., Vulić, Todor, Oparnica, Čedo, Radivojević, Dragan, Đorđević, Boban, Tešević, Vele, Jadranin, Milka, "The determination of quantitative jugolone content dynamics and the antioxidant activity in the extract of green walnut (Juglans regia L.) fruits" in Journal of Scientific Agricultural Research, 68, no. 1 (2007):59-68,
https://hdl.handle.net/21.15107/rcub_cer_321 .