TY  - JOUR
AU  - Krstić, Jugoslav
AU  - Vukelić, Nikola
AU  - Nedić, Zoran
AU  - Milutinović Nikolić, Aleksandra
AU  - Sucurovic, A
AU  - Jovanović, Dušan M.
PY  - 2005
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/175
AB  - The aim of this paper was the investigation of the influence of synthesis parameters, as well as the order of synthesis steps, in procedure of chemical precipitation, on the properties of synthesized nickel precursor. The starting materials were always the same aqueous solutions of Ni(NO3)(2)(.)6H(2)O and Mg(NO3)(2)(.)6H(2)O of constant molar ratio, 2% solution Of SiO2 in the form of sodium silicate solution (module SiO2/Na2O = 3.0) and 10% solution of Na2CO3, while synthesis steps and addition modes were varied. Complete pH and temperature monitoring was performed during entire synthesis at 90 degrees C. The formed precipitate aged 30 minutes at synthesis temperature. By changing the order and conditions of adding SiO2 and Na2CO3 solutions and keeping the treatment of precipitates the same (rinsing with hot distilled water followed by drying at 110 degrees C for 24 hours) six different precursors were obtained. Samples characterizations were performed using different experimental techniques: XRD analysis, IR spectroscopy, reflection spectroscopy, TG analysis, N-2 physisorption. The relation between synthesis procedure and precursor properties was established.
PB  - Trans Tech Publications Ltd, Zurich-Uetikon
T2  - Current Research in Advanced Materials and Processes
T1  - Nickel/silica precursor from sodium silicate solution - Synthesis and characterization
VL  - 494
SP  - 333
EP  - 338
DO  - 10.4028/www.scientific.net/MSF.494.333
ER  - 

@article{
author = "Krstić, Jugoslav and Vukelić, Nikola and Nedić, Zoran and Milutinović Nikolić, Aleksandra and Sucurovic, A and Jovanović, Dušan M.",
year = "2005",
abstract = "The aim of this paper was the investigation of the influence of synthesis parameters, as well as the order of synthesis steps, in procedure of chemical precipitation, on the properties of synthesized nickel precursor. The starting materials were always the same aqueous solutions of Ni(NO3)(2)(.)6H(2)O and Mg(NO3)(2)(.)6H(2)O of constant molar ratio, 2% solution Of SiO2 in the form of sodium silicate solution (module SiO2/Na2O = 3.0) and 10% solution of Na2CO3, while synthesis steps and addition modes were varied. Complete pH and temperature monitoring was performed during entire synthesis at 90 degrees C. The formed precipitate aged 30 minutes at synthesis temperature. By changing the order and conditions of adding SiO2 and Na2CO3 solutions and keeping the treatment of precipitates the same (rinsing with hot distilled water followed by drying at 110 degrees C for 24 hours) six different precursors were obtained. Samples characterizations were performed using different experimental techniques: XRD analysis, IR spectroscopy, reflection spectroscopy, TG analysis, N-2 physisorption. The relation between synthesis procedure and precursor properties was established.",
publisher = "Trans Tech Publications Ltd, Zurich-Uetikon",
journal = "Current Research in Advanced Materials and Processes",
title = "Nickel/silica precursor from sodium silicate solution - Synthesis and characterization",
volume = "494",
pages = "333-338",
doi = "10.4028/www.scientific.net/MSF.494.333"
}

Krstić, J., Vukelić, N., Nedić, Z., Milutinović Nikolić, A., Sucurovic, A.,& Jovanović, D. M.. (2005). Nickel/silica precursor from sodium silicate solution - Synthesis and characterization. in Current Research in Advanced Materials and Processes
Trans Tech Publications Ltd, Zurich-Uetikon., 494, 333-338.
https://doi.org/10.4028/www.scientific.net/MSF.494.333

Krstić J, Vukelić N, Nedić Z, Milutinović Nikolić A, Sucurovic A, Jovanović DM. Nickel/silica precursor from sodium silicate solution - Synthesis and characterization. in Current Research in Advanced Materials and Processes. 2005;494:333-338.
doi:10.4028/www.scientific.net/MSF.494.333 .

Krstić, Jugoslav, Vukelić, Nikola, Nedić, Zoran, Milutinović Nikolić, Aleksandra, Sucurovic, A, Jovanović, Dušan M., "Nickel/silica precursor from sodium silicate solution - Synthesis and characterization" in Current Research in Advanced Materials and Processes, 494 (2005):333-338,
https://doi.org/10.4028/www.scientific.net/MSF.494.333 . .