TY  - JOUR
AU  - Maksimović, Vesna M.
AU  - Pavlović, L.J.
AU  - Pavlović, Miomir
AU  - Tomić, Milorad V.
PY  - 2009
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/615
AB  - Technological properties of powders depend on their granulometry and morphology. Very often one method is inadequate for characterization of powder particles. This article studied different methods intended for clear definition of the copper powder granulometric and morphological properties. Quantitative microstructural analysis, sieve analysis, and XRD analysis of copper powder as well as scanning electron microscopy analysis of the copper powder particles were performed. It was determined that selected stereological parameters, such as area, perimeter, and shape factor (roundness) show a linear decreasing dependence of current density, while the morphology was changed from massive to branched 3D dendrites. XRD analysis indicated that the crystallite sizes shows a linearly increasing dependence on current density. The shape factor could be a useful parameter for description of powder morphologies deposited by different regimes.
T2  - Journal of Applied Electrochemistry
T1  - Characterization of copper powder particles obtained by electrodeposition as function of different current densities
VL  - 39
IS  - 12
SP  - 2545
EP  - 2552
DO  - 10.1007/s10800-009-9950-y
ER  - 

@article{
author = "Maksimović, Vesna M. and Pavlović, L.J. and Pavlović, Miomir and Tomić, Milorad V.",
year = "2009",
abstract = "Technological properties of powders depend on their granulometry and morphology. Very often one method is inadequate for characterization of powder particles. This article studied different methods intended for clear definition of the copper powder granulometric and morphological properties. Quantitative microstructural analysis, sieve analysis, and XRD analysis of copper powder as well as scanning electron microscopy analysis of the copper powder particles were performed. It was determined that selected stereological parameters, such as area, perimeter, and shape factor (roundness) show a linear decreasing dependence of current density, while the morphology was changed from massive to branched 3D dendrites. XRD analysis indicated that the crystallite sizes shows a linearly increasing dependence on current density. The shape factor could be a useful parameter for description of powder morphologies deposited by different regimes.",
journal = "Journal of Applied Electrochemistry",
title = "Characterization of copper powder particles obtained by electrodeposition as function of different current densities",
volume = "39",
number = "12",
pages = "2545-2552",
doi = "10.1007/s10800-009-9950-y"
}

Maksimović, V. M., Pavlović, L.J., Pavlović, M.,& Tomić, M. V.. (2009). Characterization of copper powder particles obtained by electrodeposition as function of different current densities. in Journal of Applied Electrochemistry, 39(12), 2545-2552.
https://doi.org/10.1007/s10800-009-9950-y

Maksimović VM, Pavlović L, Pavlović M, Tomić MV. Characterization of copper powder particles obtained by electrodeposition as function of different current densities. in Journal of Applied Electrochemistry. 2009;39(12):2545-2552.
doi:10.1007/s10800-009-9950-y .

Maksimović, Vesna M., Pavlović, L.J., Pavlović, Miomir, Tomić, Milorad V., "Characterization of copper powder particles obtained by electrodeposition as function of different current densities" in Journal of Applied Electrochemistry, 39, no. 12 (2009):2545-2552,
https://doi.org/10.1007/s10800-009-9950-y . .

TY  - CHAP
AU  - Nikolić, Nebojša D.
AU  - Krstić, Snežana B.
AU  - Pavlović, L.J.
AU  - Pavlović, Miomir
AU  - Popov, Konstantin I.
PY  - 2008
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/482
AB  - The papers dealing with the effects of electrodeposition conditions on the decisive characteristics of electrolytic copper powder and their mutual relations are reviewed, and a semiquantitative theory based on them is presented. Also, the method for the estimation of the surface energy of disperse deposit formation based on the estimation of a surface area of deposits at different overpotentials is proposed. Then, the values of the surface energy of disperse deposit formation estimated in this way are used for the correlation of the specific surface of a powder to the electrodeposition conditions. The good agreement between the values of the specific surface of a powder determined in this way and those found in the literature is obtained. The apparent density of a powder as one of the decisive characteristics of metal powders is also correlated to the specific surface, and hence, to the electrodeposition conditions. In this chapter, the size of representative powder particle having the same specific surface as a powder is defined and the shape of the particle size distribution curve is analyzed. The problems concerning the effect of the particle shape and structure on the flowability of electrolytically formed copper powder are also discussed.© 2009 by Nova Science Publishers, Inc. All rights reserved.
PB  - Nova Science Publishers, Inc.
T2  - Electroanalytical Chemistry Research Trends
T1  - The mutual relation of decisive characteristics of electrolytic copper powder and effect of deposition conditions on them
SP  - 185
EP  - 209
UR  - https://hdl.handle.net/21.15107/rcub_cer_482
ER  - 

@inbook{
author = "Nikolić, Nebojša D. and Krstić, Snežana B. and Pavlović, L.J. and Pavlović, Miomir and Popov, Konstantin I.",
year = "2008",
abstract = "The papers dealing with the effects of electrodeposition conditions on the decisive characteristics of electrolytic copper powder and their mutual relations are reviewed, and a semiquantitative theory based on them is presented. Also, the method for the estimation of the surface energy of disperse deposit formation based on the estimation of a surface area of deposits at different overpotentials is proposed. Then, the values of the surface energy of disperse deposit formation estimated in this way are used for the correlation of the specific surface of a powder to the electrodeposition conditions. The good agreement between the values of the specific surface of a powder determined in this way and those found in the literature is obtained. The apparent density of a powder as one of the decisive characteristics of metal powders is also correlated to the specific surface, and hence, to the electrodeposition conditions. In this chapter, the size of representative powder particle having the same specific surface as a powder is defined and the shape of the particle size distribution curve is analyzed. The problems concerning the effect of the particle shape and structure on the flowability of electrolytically formed copper powder are also discussed.© 2009 by Nova Science Publishers, Inc. All rights reserved.",
publisher = "Nova Science Publishers, Inc.",
journal = "Electroanalytical Chemistry Research Trends",
booktitle = "The mutual relation of decisive characteristics of electrolytic copper powder and effect of deposition conditions on them",
pages = "185-209",
url = "https://hdl.handle.net/21.15107/rcub_cer_482"
}

Nikolić, N. D., Krstić, S. B., Pavlović, L.J., Pavlović, M.,& Popov, K. I.. (2008). The mutual relation of decisive characteristics of electrolytic copper powder and effect of deposition conditions on them. in Electroanalytical Chemistry Research Trends
Nova Science Publishers, Inc.., 185-209.
https://hdl.handle.net/21.15107/rcub_cer_482

Nikolić ND, Krstić SB, Pavlović L, Pavlović M, Popov KI. The mutual relation of decisive characteristics of electrolytic copper powder and effect of deposition conditions on them. in Electroanalytical Chemistry Research Trends. 2008;:185-209.
https://hdl.handle.net/21.15107/rcub_cer_482 .

Nikolić, Nebojša D., Krstić, Snežana B., Pavlović, L.J., Pavlović, Miomir, Popov, Konstantin I., "The mutual relation of decisive characteristics of electrolytic copper powder and effect of deposition conditions on them" in Electroanalytical Chemistry Research Trends (2008):185-209,
https://hdl.handle.net/21.15107/rcub_cer_482 .