Radak, Bojan

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orcid::0000-0003-2065-7926
  • Radak, Bojan (2)
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Author's Bibliography

Optimization of injected radiotracer volume for flow meter calibration in closed conduits

Pavlović, Miroslav; Bartl, Pavel; Pantović Pavlović, Marijana; Stevanović, Jasmina; Radak, Bojan

(Warsaw, Poland : Instytut Chemii i Techniki Jądrowej, 2020)

TY  - CONF
AU  - Pavlović, Miroslav
AU  - Bartl, Pavel
AU  - Pantović Pavlović, Marijana
AU  - Stevanović, Jasmina
AU  - Radak, Bojan
PY  - 2020
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/6559
AB  - In chemical processes it is of essential for flow in the process to be accurate and well defined. 
Fluid velocity measurements are important for fluid flow quality performance in the systems. 
This study focuses on determination of volumetric flow rate measurement and on calibration 
of conventional flowmeter using industrial radiotracer approach. In this work, the application 
of radiotracer method for RTD measurement in flow meter calibration for chemical industry 
is described. The experiments in pilot-scale flow rig were performed using Technetium-99 m 
(
99mTc) as a radiotracer in the form of pertechnetate ion (99mTcO4
-
) to calibrate flow meter. The 
data were evaluated using plug flow with axial dispersion model of RTD software.
The optimization of the parameters included input signal of radiotracer, concentration of 
radiotracer and position of detectors. The measured data were analyzed, and precision of 
experimental setup was investigated under two different approaches. A plug flow with axial 
dispersion was used to simulate the measured RTD curves and investigate flow dynamics of 
the flowing water. The results of the study, showed that there might be an optimum injection 
volume range of the tracer for each specific application.
The optimum range in this study was determined from 300 to 700 µL. In this range, relative 
standard deviation was around 1% for both calculation methods, which is lower than with 
other available injection volumes. Bias of the initial flow rate was lower using summation 
approximation, resulting in ca 9% in the area of interest. In case of RTD software, bias values 
were between 10 and 11%. For the first time the variation of standard deviation of calculated 
flow rate with injection volume and activity of radiotracer was determined. The results of the 
study may help in injection volume optimization as well as give a guide on how to process 
data without RTD software, as the results obtained by both methods were in great agreement. 
They also revealed a slight dependency of the precision of output results on the injection 
volume as well as similar results for manual and specialized RTD software data processing. The 
study that investigated the change of standard deviation of calculated flow rate with injection 
volume and activity of used radiotracer was conducted for the first time in literature.
PB  - Warsaw, Poland : Instytut Chemii i Techniki Jądrowej
C3  - Conference abstracts & programme - International Conference on Development and Applications of Nuclear Technologies – NUTECH 2020, October 4-7, Warsaw, Poland
T1  - Optimization of injected radiotracer volume for flow meter calibration in closed conduits
SP  - 80
EP  - 80
UR  - https://hdl.handle.net/21.15107/rcub_cer_6559
ER  - 
@conference{
author = "Pavlović, Miroslav and Bartl, Pavel and Pantović Pavlović, Marijana and Stevanović, Jasmina and Radak, Bojan",
year = "2020",
abstract = "In chemical processes it is of essential for flow in the process to be accurate and well defined. 
Fluid velocity measurements are important for fluid flow quality performance in the systems. 
This study focuses on determination of volumetric flow rate measurement and on calibration 
of conventional flowmeter using industrial radiotracer approach. In this work, the application 
of radiotracer method for RTD measurement in flow meter calibration for chemical industry 
is described. The experiments in pilot-scale flow rig were performed using Technetium-99 m 
(
99mTc) as a radiotracer in the form of pertechnetate ion (99mTcO4
-
) to calibrate flow meter. The 
data were evaluated using plug flow with axial dispersion model of RTD software.
The optimization of the parameters included input signal of radiotracer, concentration of 
radiotracer and position of detectors. The measured data were analyzed, and precision of 
experimental setup was investigated under two different approaches. A plug flow with axial 
dispersion was used to simulate the measured RTD curves and investigate flow dynamics of 
the flowing water. The results of the study, showed that there might be an optimum injection 
volume range of the tracer for each specific application.
The optimum range in this study was determined from 300 to 700 µL. In this range, relative 
standard deviation was around 1% for both calculation methods, which is lower than with 
other available injection volumes. Bias of the initial flow rate was lower using summation 
approximation, resulting in ca 9% in the area of interest. In case of RTD software, bias values 
were between 10 and 11%. For the first time the variation of standard deviation of calculated 
flow rate with injection volume and activity of radiotracer was determined. The results of the 
study may help in injection volume optimization as well as give a guide on how to process 
data without RTD software, as the results obtained by both methods were in great agreement. 
They also revealed a slight dependency of the precision of output results on the injection 
volume as well as similar results for manual and specialized RTD software data processing. The 
study that investigated the change of standard deviation of calculated flow rate with injection 
volume and activity of used radiotracer was conducted for the first time in literature.",
publisher = "Warsaw, Poland : Instytut Chemii i Techniki Jądrowej",
journal = "Conference abstracts & programme - International Conference on Development and Applications of Nuclear Technologies – NUTECH 2020, October 4-7, Warsaw, Poland",
title = "Optimization of injected radiotracer volume for flow meter calibration in closed conduits",
pages = "80-80",
url = "https://hdl.handle.net/21.15107/rcub_cer_6559"
}
Pavlović, M., Bartl, P., Pantović Pavlović, M., Stevanović, J.,& Radak, B.. (2020). Optimization of injected radiotracer volume for flow meter calibration in closed conduits. in Conference abstracts & programme - International Conference on Development and Applications of Nuclear Technologies – NUTECH 2020, October 4-7, Warsaw, Poland
Warsaw, Poland : Instytut Chemii i Techniki Jądrowej., 80-80.
https://hdl.handle.net/21.15107/rcub_cer_6559
Pavlović M, Bartl P, Pantović Pavlović M, Stevanović J, Radak B. Optimization of injected radiotracer volume for flow meter calibration in closed conduits. in Conference abstracts & programme - International Conference on Development and Applications of Nuclear Technologies – NUTECH 2020, October 4-7, Warsaw, Poland. 2020;:80-80.
https://hdl.handle.net/21.15107/rcub_cer_6559 .
Pavlović, Miroslav, Bartl, Pavel, Pantović Pavlović, Marijana, Stevanović, Jasmina, Radak, Bojan, "Optimization of injected radiotracer volume for flow meter calibration in closed conduits" in Conference abstracts & programme - International Conference on Development and Applications of Nuclear Technologies – NUTECH 2020, October 4-7, Warsaw, Poland (2020):80-80,
https://hdl.handle.net/21.15107/rcub_cer_6559 .

Optimization of injected radiotracer volume for flow rate measurement in closed conduits

Pavlović, Miroslav M.; Pantović Pavlović, Marijana; Bartl, Pavel; Stevanović, Jasmina; Radak, Bojan

(Belgrade : Association of the Chemical Engineers of Serbia, 2020)

TY  - JOUR
AU  - Pavlović, Miroslav M.
AU  - Pantović Pavlović, Marijana
AU  - Bartl, Pavel
AU  - Stevanović, Jasmina
AU  - Radak, Bojan
PY  - 2020
UR  - https://cer.ihtm.bg.ac.rs/handle/123456789/4017
AB  - In chemical processes it is essential that the flow in the process is accurately defined. Fluid velocity measurements are important for fluid flow quality performance in flow systems. This study focuses on determination of the volumetric flow rate and its standard (relative) deviation for calibration of conventional flow meters by using a radiotracer approach. The measurements for flow meter calibration were performed at a pilot-scale flow rig using Technetium-99 m (99mTc) as a radiotracer in the form of pertechnetate ion (99mTcO4-). The measured data were analyzed, and precision of the experimental setup was investigated under two different approaches – IAEA’s RTD software and sum approximation of raw data. For the first time, the variation of standard deviation of calculated flow rate with the injection volume and activity of the radiotracer was determined. Plug flow with axial dispersion was used to simulate the measured RTD curves and investigate the flow dynamics of the flowing water. The results of the study have shown the possibility of in situ calibration of flow meters with a relative error lower than 1 %. They also revealed a slight dependency of the precision of output results on the injection volume as well as similar results for manual and specialized RTD software data processing.
AB  - U hemijskim procesima od suštinskog značaja je tačno definisan i precizan protok. Merenja brzine fluida su važna za karakterizaciju kvaliteta protoka tečnosti u sistemima. Ova studija se fokusira na određivanje zapreminskog protoka i standardnog (relativnog) odstupanja izmerenih vrednosti u cilju kalibracije konvencionalnih merača protoka korišćenjem metode radioaktivnog obeleživača. Merenja potrebna za kalibraciju merača protoka izvedena su na pilot postrojenju korišćenjem Tehnecijuma-99m (99mTc) kao radiotrejsera u obliku pertehnetatnog jona (99mTcO4-). Izmereni podaci su analizirani, a preciznost eksperimentalne postavke je ispitivana pomoću dva različita pristupa: upotrebom softvera za određivanje raspodele vremena zadržavanja (eng. residence time distribution, RTD) koga je razvila Međunarodna agencija za atomsku energiju i zbirne aproksimacije neobrađenih podataka. Po prvi put je utvrđena varijacija standardne devijacije izračunatog protoka u odnosu na zapreminu i u odnosu na aktivnost ubrizganog radioaktivnog obeleživača. Model protoka sa aksijalnom disperzijom je korišćen za simulaciju izmerenih RTD krivih i istraživanje dinamike protoka vode. Rezultati studije su pokazali mogućnost in situ kalibracije merača protoka sa relativnom greškom manjom od 1%. Takođe su pokazali malu zavisnost preciznosti izlaznih rezultata od količine ubrizganog obeleživača, kao i slične rezultate za manuelnu obradu i specijalizovanu obradu podataka upotrebom RTD softvera.
PB  - Belgrade : Association of the Chemical Engineers of Serbia
T2  - Hemijska industrija
T1  - Optimization of injected radiotracer volume for flow rate measurement in closed conduits
T1  - Optimizacija zapremine radioaktivnog obeleživača pri merenju zapreminskog protoka u zatvorenim cevovodima
VL  - 74
IS  - 5
SP  - 305
EP  - 312
DO  - 10.2298/HEMIND20050325P
ER  - 
@article{
author = "Pavlović, Miroslav M. and Pantović Pavlović, Marijana and Bartl, Pavel and Stevanović, Jasmina and Radak, Bojan",
year = "2020",
abstract = "In chemical processes it is essential that the flow in the process is accurately defined. Fluid velocity measurements are important for fluid flow quality performance in flow systems. This study focuses on determination of the volumetric flow rate and its standard (relative) deviation for calibration of conventional flow meters by using a radiotracer approach. The measurements for flow meter calibration were performed at a pilot-scale flow rig using Technetium-99 m (99mTc) as a radiotracer in the form of pertechnetate ion (99mTcO4-). The measured data were analyzed, and precision of the experimental setup was investigated under two different approaches – IAEA’s RTD software and sum approximation of raw data. For the first time, the variation of standard deviation of calculated flow rate with the injection volume and activity of the radiotracer was determined. Plug flow with axial dispersion was used to simulate the measured RTD curves and investigate the flow dynamics of the flowing water. The results of the study have shown the possibility of in situ calibration of flow meters with a relative error lower than 1 %. They also revealed a slight dependency of the precision of output results on the injection volume as well as similar results for manual and specialized RTD software data processing., U hemijskim procesima od suštinskog značaja je tačno definisan i precizan protok. Merenja brzine fluida su važna za karakterizaciju kvaliteta protoka tečnosti u sistemima. Ova studija se fokusira na određivanje zapreminskog protoka i standardnog (relativnog) odstupanja izmerenih vrednosti u cilju kalibracije konvencionalnih merača protoka korišćenjem metode radioaktivnog obeleživača. Merenja potrebna za kalibraciju merača protoka izvedena su na pilot postrojenju korišćenjem Tehnecijuma-99m (99mTc) kao radiotrejsera u obliku pertehnetatnog jona (99mTcO4-). Izmereni podaci su analizirani, a preciznost eksperimentalne postavke je ispitivana pomoću dva različita pristupa: upotrebom softvera za određivanje raspodele vremena zadržavanja (eng. residence time distribution, RTD) koga je razvila Međunarodna agencija za atomsku energiju i zbirne aproksimacije neobrađenih podataka. Po prvi put je utvrđena varijacija standardne devijacije izračunatog protoka u odnosu na zapreminu i u odnosu na aktivnost ubrizganog radioaktivnog obeleživača. Model protoka sa aksijalnom disperzijom je korišćen za simulaciju izmerenih RTD krivih i istraživanje dinamike protoka vode. Rezultati studije su pokazali mogućnost in situ kalibracije merača protoka sa relativnom greškom manjom od 1%. Takođe su pokazali malu zavisnost preciznosti izlaznih rezultata od količine ubrizganog obeleživača, kao i slične rezultate za manuelnu obradu i specijalizovanu obradu podataka upotrebom RTD softvera.",
publisher = "Belgrade : Association of the Chemical Engineers of Serbia",
journal = "Hemijska industrija",
title = "Optimization of injected radiotracer volume for flow rate measurement in closed conduits, Optimizacija zapremine radioaktivnog obeleživača pri merenju zapreminskog protoka u zatvorenim cevovodima",
volume = "74",
number = "5",
pages = "305-312",
doi = "10.2298/HEMIND20050325P"
}
Pavlović, M. M., Pantović Pavlović, M., Bartl, P., Stevanović, J.,& Radak, B.. (2020). Optimization of injected radiotracer volume for flow rate measurement in closed conduits. in Hemijska industrija
Belgrade : Association of the Chemical Engineers of Serbia., 74(5), 305-312.
https://doi.org/10.2298/HEMIND20050325P
Pavlović MM, Pantović Pavlović M, Bartl P, Stevanović J, Radak B. Optimization of injected radiotracer volume for flow rate measurement in closed conduits. in Hemijska industrija. 2020;74(5):305-312.
doi:10.2298/HEMIND20050325P .
Pavlović, Miroslav M., Pantović Pavlović, Marijana, Bartl, Pavel, Stevanović, Jasmina, Radak, Bojan, "Optimization of injected radiotracer volume for flow rate measurement in closed conduits" in Hemijska industrija, 74, no. 5 (2020):305-312,
https://doi.org/10.2298/HEMIND20050325P . .
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