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Crystal structure of 2-{1-[(1-(2-pyridinio)ethylidene)hydrazono]ethyl} pyridinium diperchlorate, the product of template condensation in the presence of Cr(III)
dc.creator | Radanović, Dušanka | |
dc.creator | Kalucrossed, D Signerović G. | |
dc.creator | Gómez-Ruiz, S. | |
dc.creator | Sladić, Dušan | |
dc.creator | Šumar-Ristović, Maja | |
dc.creator | Brčeski, Ilija | |
dc.creator | Anđelković, Katarina | |
dc.date.accessioned | 2019-01-30T17:21:39Z | |
dc.date.available | 2019-01-30T17:21:39Z | |
dc.date.issued | 2009 | |
dc.identifier.issn | 1074-1542 | |
dc.identifier.uri | https://cer.ihtm.bg.ac.rs/handle/123456789/602 | |
dc.description.abstract | In an attempt to synthesize a Cr(III) complex of 2′-[1-(2-pyridinyl) ethylidene]oxamohydrazide an azine product 2-{1-[(1-(2-pyridinio)ethylidene) hydrazono]ethyl}pyridinium diperchlorate was obtained by an electrophilic acyl substitution catalyzed by Cr(III). Its structure was determined by X-ray crystal analysis and showed significant changes in comparison to the corresponding unprotonated compound. The 2-{1-[(1-(2-pyridinio)ethylidene)hydrazono]ethyl} pyridinium diperchlorate crystallizes in the space group P21/n of the monoclinic crystal system with unit cell parameters a = 14.3809(3) Å, b = 24.1516(5) Å, c = 15.4471(3) Å, β = 99.930(2)°, V = 5284.74(19) Å3 and Z = 12, i.e. three molecules per asymmetric unit. | en |
dc.relation | info:eu-repo/grantAgreement/MESTD/MPN2006-2010/14026/RS// | |
dc.rights | restrictedAccess | |
dc.source | Journal of Chemical Crystallography | |
dc.subject | Azines | en |
dc.subject | Template synthesis | en |
dc.subject | X-ray structure determination | en |
dc.title | Crystal structure of 2-{1-[(1-(2-pyridinio)ethylidene)hydrazono]ethyl} pyridinium diperchlorate, the product of template condensation in the presence of Cr(III) | en |
dc.type | article | |
dc.rights.license | ARR | |
dcterms.abstract | Брчески, И.; Aнђелковић, Катарина; Шумар-Ристовић, М.; Гóмез-Руиз, С.; Радановић, Душанка; Калуцроссед, Д Сигнеровић Г.; Сладић, Д.; | |
dc.citation.volume | 39 | |
dc.citation.issue | 2 | |
dc.citation.spage | 138 | |
dc.citation.epage | 142 | |
dc.citation.other | 39(2): 138-142 | |
dc.citation.rank | M23 | |
dc.identifier.doi | 10.1007/s10870-008-9443-6 | |
dc.identifier.scopus | 2-s2.0-59849119841 | |
dc.identifier.wos | 000263056300012 | |
dc.type.version | publishedVersion |