Optimization of reaction parameters for preparation of MXene-based polymer nanocomposites
Samo za registrovane korisnike
2023
Autori
Pešić, IvanRašljić-Rafajilović, Milena
Vasiljević-Radović, Dana
Ostojić, Sanja
Petrović, Miloš
Radojević, Vesna
Pergal, Marija
Konferencijski prilog (Objavljena verzija)
,
IEEE
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
The present study reports on the preparation of nanocomposites consisting of polyurethane (PU) as the matrix and Ti 3 C 2 T x MXene as the nanofiller, utilizing an in-situ polymerization method. The synthesis parameters of polyurethane remained constant, while the method of adding and preparing MXene was varied. The MXene content was maintained at 1 wt.% for all prepared nanocomposites, and the soft segment content was held constant as well. For the characterization of our materials, FTIR, SEM, TGA and tensile tests were employed. Also, the properties of the prepared nanocomposites were compared to pure PU. FTIR spectra confirmed the formation of urethane bonds. SEM images demonstrated the dispersion state of MXene in the polymer matrix. TGA revealed higher thermal stability of the prepared nanocomposites compared to pure PU. Moreover, the Young’s modulus and tensile strength increased for all prepared nanocomposites.
Ključne reči:
polymer / MXene / nanocomposite / optimization / characterizationIzvor:
10th International Conference on Electrical, Electronic and Computing Engineering (IcETRAN), 05-08 June 2023, East Sarajevo, Bosnia and Herzegovina, 2023, 23488337-Izdavač:
- Institute of Electrical and Electronics Engineers (IEEE)
Finansiranje / projekti:
- Ministarstvo nauke, tehnološkog razvoja i inovacija Republike Srbije, institucionalno finansiranje - 200026 (Univerzitet u Beogradu, Institut za hemiju, tehnologiju i metalurgiju - IHTM) (RS-MESTD-inst-2020-200026)
DOI: 10.1109/IcETRAN59631.2023.10192211
ISBN: 979-8-3503-0711-5
Scopus: 2-s2.0-85168419170
Institucija/grupa
IHTMTY - CONF AU - Pešić, Ivan AU - Rašljić-Rafajilović, Milena AU - Vasiljević-Radović, Dana AU - Ostojić, Sanja AU - Petrović, Miloš AU - Radojević, Vesna AU - Pergal, Marija PY - 2023 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/6690 AB - The present study reports on the preparation of nanocomposites consisting of polyurethane (PU) as the matrix and Ti 3 C 2 T x MXene as the nanofiller, utilizing an in-situ polymerization method. The synthesis parameters of polyurethane remained constant, while the method of adding and preparing MXene was varied. The MXene content was maintained at 1 wt.% for all prepared nanocomposites, and the soft segment content was held constant as well. For the characterization of our materials, FTIR, SEM, TGA and tensile tests were employed. Also, the properties of the prepared nanocomposites were compared to pure PU. FTIR spectra confirmed the formation of urethane bonds. SEM images demonstrated the dispersion state of MXene in the polymer matrix. TGA revealed higher thermal stability of the prepared nanocomposites compared to pure PU. Moreover, the Young’s modulus and tensile strength increased for all prepared nanocomposites. PB - Institute of Electrical and Electronics Engineers (IEEE) C3 - 10th International Conference on Electrical, Electronic and Computing Engineering (IcETRAN), 05-08 June 2023, East Sarajevo, Bosnia and Herzegovina T1 - Optimization of reaction parameters for preparation of MXene-based polymer nanocomposites SP - 23488337 DO - 10.1109/IcETRAN59631.2023.10192211 ER -
@conference{ author = "Pešić, Ivan and Rašljić-Rafajilović, Milena and Vasiljević-Radović, Dana and Ostojić, Sanja and Petrović, Miloš and Radojević, Vesna and Pergal, Marija", year = "2023", abstract = "The present study reports on the preparation of nanocomposites consisting of polyurethane (PU) as the matrix and Ti 3 C 2 T x MXene as the nanofiller, utilizing an in-situ polymerization method. The synthesis parameters of polyurethane remained constant, while the method of adding and preparing MXene was varied. The MXene content was maintained at 1 wt.% for all prepared nanocomposites, and the soft segment content was held constant as well. For the characterization of our materials, FTIR, SEM, TGA and tensile tests were employed. Also, the properties of the prepared nanocomposites were compared to pure PU. FTIR spectra confirmed the formation of urethane bonds. SEM images demonstrated the dispersion state of MXene in the polymer matrix. TGA revealed higher thermal stability of the prepared nanocomposites compared to pure PU. Moreover, the Young’s modulus and tensile strength increased for all prepared nanocomposites.", publisher = "Institute of Electrical and Electronics Engineers (IEEE)", journal = "10th International Conference on Electrical, Electronic and Computing Engineering (IcETRAN), 05-08 June 2023, East Sarajevo, Bosnia and Herzegovina", title = "Optimization of reaction parameters for preparation of MXene-based polymer nanocomposites", pages = "23488337", doi = "10.1109/IcETRAN59631.2023.10192211" }
Pešić, I., Rašljić-Rafajilović, M., Vasiljević-Radović, D., Ostojić, S., Petrović, M., Radojević, V.,& Pergal, M.. (2023). Optimization of reaction parameters for preparation of MXene-based polymer nanocomposites. in 10th International Conference on Electrical, Electronic and Computing Engineering (IcETRAN), 05-08 June 2023, East Sarajevo, Bosnia and Herzegovina Institute of Electrical and Electronics Engineers (IEEE)., 23488337. https://doi.org/10.1109/IcETRAN59631.2023.10192211
Pešić I, Rašljić-Rafajilović M, Vasiljević-Radović D, Ostojić S, Petrović M, Radojević V, Pergal M. Optimization of reaction parameters for preparation of MXene-based polymer nanocomposites. in 10th International Conference on Electrical, Electronic and Computing Engineering (IcETRAN), 05-08 June 2023, East Sarajevo, Bosnia and Herzegovina. 2023;:23488337. doi:10.1109/IcETRAN59631.2023.10192211 .
Pešić, Ivan, Rašljić-Rafajilović, Milena, Vasiljević-Radović, Dana, Ostojić, Sanja, Petrović, Miloš, Radojević, Vesna, Pergal, Marija, "Optimization of reaction parameters for preparation of MXene-based polymer nanocomposites" in 10th International Conference on Electrical, Electronic and Computing Engineering (IcETRAN), 05-08 June 2023, East Sarajevo, Bosnia and Herzegovina (2023):23488337, https://doi.org/10.1109/IcETRAN59631.2023.10192211 . .