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dc.creatorRadanović, Dušanka
dc.creatorKalucrossed, D Signerović G.
dc.creatorGómez-Ruiz, S.
dc.creatorSladić, Dušan
dc.creatorŠumar-Ristović, M.
dc.creatorBrčeski, I.
dc.creatorAnđelković, Katarina
dc.date.accessioned2019-01-30T17:21:39Z
dc.date.available2019-01-30T17:21:39Z
dc.date.issued2009
dc.identifier.issn1074-1542
dc.identifier.urihttp://cer.ihtm.bg.ac.rs/handle/123456789/602
dc.description.abstractIn an attempt to synthesize a Cr(III) complex of 2′-[1-(2-pyridinyl) ethylidene]oxamohydrazide an azine product 2-{1-[(1-(2-pyridinio)ethylidene) hydrazono]ethyl}pyridinium diperchlorate was obtained by an electrophilic acyl substitution catalyzed by Cr(III). Its structure was determined by X-ray crystal analysis and showed significant changes in comparison to the corresponding unprotonated compound. The 2-{1-[(1-(2-pyridinio)ethylidene)hydrazono]ethyl} pyridinium diperchlorate crystallizes in the space group P21/n of the monoclinic crystal system with unit cell parameters a = 14.3809(3) Å, b = 24.1516(5) Å, c = 15.4471(3) Å, β = 99.930(2)°, V = 5284.74(19) Å3 and Z = 12, i.e. three molecules per asymmetric unit.en
dc.relationinfo:eu-repo/grantAgreement/MESTD/MPN2006-2010/14026/RS//
dc.rightsrestrictedAccess
dc.sourceJournal of Chemical Crystallography
dc.subjectAzinesen
dc.subjectTemplate synthesisen
dc.subjectX-ray structure determinationen
dc.titleCrystal structure of 2-{1-[(1-(2-pyridinio)ethylidene)hydrazono]ethyl} pyridinium diperchlorate, the product of template condensation in the presence of Cr(III)en
dc.typearticle
dc.rights.licenseARR
dcterms.abstractБрчески, И.; Aнђелковић, Катарина; Шумар-Ристовић, М.; Гóмез-Руиз, С.; Радановић, Душанка; Калуцроссед, Д Сигнеровић Г.; Сладић, Д.;
dc.citation.volume39
dc.citation.issue2
dc.citation.spage138
dc.citation.epage142
dc.citation.other39(2): 138-142
dc.citation.rankM23
dc.identifier.doi10.1007/s10870-008-9443-6
dc.identifier.rcubConv_4184
dc.identifier.scopus2-s2.0-59849119841
dc.identifier.wos000263056300012
dc.type.versionpublishedVersion


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