SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor
2013
Аутори
Dimitrijević, R.Cvetković, Olga
Miodragović, Zoran
Simić, M.
Manojlović, Dragan
Jović, Vesna
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.
Кључне речи:
Ag nanoparticles / sphere shaped / chemical deposition / XRD technique / SEM/EDX analysisИзвор:
Journal of Mining and Metallurgy B: Metallurgy, 2013, 49, 1, 91-95Издавач:
- Technical Faculty, Bor-Serbia, Bor
Финансирање / пројекти:
- Примена унапређених оксидационих процеса и наноструктурисаних оксидних материјала за уклањање загађивача из животне средине, развој и оптимизација инструменталних техника за праћење ефикасности (RS-MESTD-Basic Research (BR or ON)-172030)
- Геохемијска испитивања седиментних стена - фосилна горива и загађивачи животне средине (RS-MESTD-Basic Research (BR or ON)-176006)
- Микро, нано-системи и сензори за примену у електропривреди, процесној индустрији и заштити животне средине (RS-MESTD-Technological Development (TD or TR)-32008)
DOI: 10.2298/JMMB120111041D
ISSN: 1450-5339
WoS: 000328704500014
Scopus: 2-s2.0-84880975200
Институција/група
IHTMTY - JOUR AU - Dimitrijević, R. AU - Cvetković, Olga AU - Miodragović, Zoran AU - Simić, M. AU - Manojlović, Dragan AU - Jović, Vesna PY - 2013 UR - https://cer.ihtm.bg.ac.rs/handle/123456789/1169 AB - The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard. PB - Technical Faculty, Bor-Serbia, Bor T2 - Journal of Mining and Metallurgy B: Metallurgy T1 - SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor VL - 49 IS - 1 SP - 91 EP - 95 DO - 10.2298/JMMB120111041D ER -
@article{ author = "Dimitrijević, R. and Cvetković, Olga and Miodragović, Zoran and Simić, M. and Manojlović, Dragan and Jović, Vesna", year = "2013", abstract = "The Ag nano-structured thin films prepared on flat glass substrates have been studied. The ball-like silver nanoparticles have been synthesized in large quantity by using a modified method of hydrolytic decomposition of silver complexes with amino types ligands formed in ethanol aqueous solution. SEM analysis revealed that Ag nanoparticles are all sphere shaped with bimodal size (40 and 70 nm) distribution. The results of XRD powder pattern examination show that Ag nanoparticles are pure phase, well crystallized. The unit cell dimensions measured on synthesized Ag nano films show small but frequent contraction in comparison to Ag metal standard.", publisher = "Technical Faculty, Bor-Serbia, Bor", journal = "Journal of Mining and Metallurgy B: Metallurgy", title = "SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor", volume = "49", number = "1", pages = "91-95", doi = "10.2298/JMMB120111041D" }
Dimitrijević, R., Cvetković, O., Miodragović, Z., Simić, M., Manojlović, D.,& Jović, V.. (2013). SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor. in Journal of Mining and Metallurgy B: Metallurgy Technical Faculty, Bor-Serbia, Bor., 49(1), 91-95. https://doi.org/10.2298/JMMB120111041D
Dimitrijević R, Cvetković O, Miodragović Z, Simić M, Manojlović D, Jović V. SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor. in Journal of Mining and Metallurgy B: Metallurgy. 2013;49(1):91-95. doi:10.2298/JMMB120111041D .
Dimitrijević, R., Cvetković, Olga, Miodragović, Zoran, Simić, M., Manojlović, Dragan, Jović, Vesna, "SEM/EDX and XRD characterization of silver nanocrystalline thin film prepared from organometallic solution precursor" in Journal of Mining and Metallurgy B: Metallurgy, 49, no. 1 (2013):91-95, https://doi.org/10.2298/JMMB120111041D . .