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/Title ({Synthesis, structure and thermogravimetric analysis of a,w-telechelic polydimethylsiloxanes of low molecular weight})
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2017-12-30T14:35:47+01:00
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2017-12
{Synthesis, structure and thermogravimetric analysis of a,w-telechelic polydimethylsiloxanes of low molecular weight}
bibtex/number/12
bibtex/file/:C$backslash$:/Users/Dekanski/AppData/Local/Mendeley Ltd./Mendeley Desktop/Downloaded/Tasic et al. - 2017 - Synthesis, structure and thermogravimetric analysis of a,w-telechelic polydimethylsiloxanes of low molecular weigh.pdf;:06_5067_5049.pdf:PDF
bibtex/journal/Journal of the Serbian Chemical Society
bibtex/pages/1395--1416
bibtex/url/http://www.doiserbia.nb.rs/Article.aspx?ID=0352-51391700082T
bibtex/volume/82
bibtex/bibtexkey/Tasic2017
Aleksandra Tasic
Marija Pergal
Malisa Antic
Vesna Antic
A series of a,w-telechelic polydimethylsiloxanes (PDMS), with predetermined molecular weights of about 2500 g mol -1 , was synthesized by siloxane equilibration reaction. Syntheses were performed using octamethylcyclotetrasiloxane (D 4 ) and various disiloxanes: hexamethyldisiloxane (HMDS), tetramethyldisiloxane (TMDS), 1,3-divinyltetramethyl-disiloxane (DVTMDS), 1,3- bis (3-carboxypropyl)tetramethyldisiloxane (DCPTMDS) and 1,3- bis (3-aminopropyl)tetramethyldisiloxane (DAPTMDS). The role of disiloxane was to introduce terminal functional groups at the end of polymer chains and to control molecular weight of the polymers. Polymers with trimethyl, hydrido, vinyl, carboxypropyl and aminopropyl end-groups were obtained in this way. The structure of a,w-telechelic PDMSs was confirmed by NMR and IR spectroscopy. Molecular weights of the polymers were determined by 1 H NMR, gel-permeation chromatography(GPC) and viscometry of dilute solutions. Thermogravimetric analysis(TGA) in nitrogen and air showed that the type of terminal groups significantly influences thermal and thermo-oxidative stability, as well as the degradation mechanism of a,w-telechelic PDMSs.
10.2298/JSC170427082T
application/pdf
Article
Aleksandra Tasic
Marija Pergal
Malisa Antic
Vesna Antic
Tasic2017
10.2298/JSC170427082T
:C$backslash$:/Users/Dekanski/AppData/Local/Mendeley Ltd./Mendeley Desktop/Downloaded/Tasic et al. - 2017 - Synthesis, structure and thermogravimetric analysis of a,w-telechelic polydimethylsiloxanes of low molecular weigh.pdf;:06_5067_5049.pdf:PDF
Journal of the Serbian Chemical Society
dec
12
1395--1416
{Synthesis, structure and thermogravimetric analysis of a,w-telechelic polydimethylsiloxanes of low molecular weight}
http://www.doiserbia.nb.rs/Article.aspx?ID=0352-51391700082T
82
2017
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